• Title/Summary/Keyword: 미세압출

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Hyper-peritectic Al-Ti Alloys as In-Situ composites through Rapid Solidification (급냉응고법에 의한 In-Situ 복합재료로서의 과포정 Al-10wt%Ti 합금(I))

  • Kim, Hye-Seong;Geum, Dong-Hwa;Kim, Geung-Ho
    • Korean Journal of Materials Research
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    • v.9 no.3
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    • pp.263-268
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    • 1999
  • In this study, a new concept of aluminum-matrix composites and the possibility of in-situ processing are suggested, and preliminary results on AI- Ti system are presented. Fine powders of AI-lO% Ti were prepared by the gas atomization so that fine $Al_3Ti$ formed into flake shape. A 25v/o $Al_3Ti/Al$ composite sample was made by the pow­d er metallurgy process involving hot extrusion. Microstructure and mechanical behavior both at room temperature and high temperatures were analysed by OM, SEM, TEM and tension test. Microstructural characteristics and mechanical properties of the composites exhibited similar behavior to those of $SiC_w/2124$ composites. Merits and drawbacks of the $Al_3Ti/Al$ composites are discussed together with a possibility of further improvement.

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Mechanical Properties of Polypropylene/Talc Composites Prepared via Solid-State Extrusion (고상 압출된 폴리프로필렌/탈크 복합재료의 기계적 물성)

  • Lee, Jaechoon;Ha, Chang-Sik
    • Journal of Adhesion and Interface
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    • v.17 no.4
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    • pp.131-135
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    • 2016
  • We investigated the specific gravity and mechanical property changes of solid-state extruded polypropylene (PP)/talc composites before and after orientation. The specific gravity of the composites increases with increasing the filler contents. The specific gravity of the oriented specimen containing filler in PP matrix is found to be much smaller than that of pre-specimen due to the formation of more micro-voids. It was found that the tensile properties of the composites are increased up to the talc content of 10 wt%, but after the contents exceeding 10 wt%, the tensile properties are decreased. For oriented specimens, the tensile strength of the composites showed monotonously decrease with increasing talc contents. When the contents of talc is 10 wt%, the theoretical values according to Halpin-Tsai equation are close to the experimental values but over 20 wt% of talc contents, the deviation of the experimental values from the theoretical prediction becomes higher. The maximum flexural strength and modulus were observed for PP/talc composites when the talc contents was 10 wt% for both pre-specimen and oriented specimen.

Physicochemical Characteristics of Rice Flour Gelatinized by Extrusion-Cooking (압출성형에 의한 알파미분의 물리화학적 특성)

  • Han, Ouk;Lee, Sang-Hyo;Lee, Hyun-Yu;Kim, Young-Myoung;Min, Byong-Lyoung
    • Korean Journal of Food Science and Technology
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    • v.20 no.4
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    • pp.470-475
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    • 1988
  • The extrusion-cooking method was used to make gelatinized rice extrudate from rice grits of the Chuchung and the Samgang varieties. The water contents of raw rice grits varied from 15% to 25%, and the physicochemical properties of extrudates were evaluated. Low moisture content showed high expansion ratio in rice extrudate and resulted in some decrease in gelatinization, bulk density and break strength. Increasing the water content to 25% resulted in increase in water absoption index but decrease in water solubility index. With regards to Brabender Amylograph values and rheological patterns, higher moisture content in raw materials revealed stronger pseudoplastic flow behavior with lower viscogram property. Hunter's color values of rice flours extruded at low water content were low in b values. Scanning electron microscopy demonstrated the break-down of starch granules during extrusion.

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Effects of Extrusion Ratio and Extrusion Temperature on Microstructure and Tensile Properties of SEN6 Magnesium Alloy (SEN6 마그네슘합금의 미세조직과 인장 특성에 미치는 압출비와 압출 온도의 영향)

  • H. J. Kim;J. Y. Lee;S. C. Jin;S. H. Park
    • Transactions of Materials Processing
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    • v.33 no.3
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    • pp.178-184
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    • 2024
  • In this study, we investigated the effects of extrusion ratio and extrusion temperature on the microstructure and tensile properties of extruded Mg-6Al-0.3Mn-0.3Ca-0.2Y (SEN6) alloy. As the extrusion ratio and temperature increase, dynamic recrystallization during extrusion is promoted, leading to the formation of a fully recrystallized microstructure with increased grain size. Additionally, the increases in extrusion ratio and temperature lead to texture strengthening, exhibiting a higher maximum texture intensity. The extruded materials contain three types of secondary phases, i.e., Al8Mn4Y, Al2Y, and Al2Ca, with irregular or polygonal shapes. The quantity, size, distribution, and area fraction of the second-phase particles are nearly identical between the two materials. Despite its larger grain size, the tensile yield strength of the material extruded at 450 ℃ and an extrusion ratio of 25 (450-25) is higher than that of the material extruded at 325 ℃ and an extrusion ratio of 10 (325-10), which is mainly attributed to the stronger texture hardening effect of the former. The ultimate tensile strength is similar in the two materials, owing to the higher work hardening rate in the 325-10 extrudate. Despite differences in grain size and recrystallization fraction, numerous twins are formed throughout the specimen during tensile deformation in both materials; consequently, the two materials exhibit nearly the same tensile elongation.

Evaluation of the Effect of Rotating Tool for Friction Stir Welding Al6005-T6 (회전공구 회전속도에 따른 알루미늄 합금 (Al6005-T6)의 마찰교반접합 특성 연구)

  • Choi, Dooho
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.18 no.11
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    • pp.124-129
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    • 2017
  • In this study, we report characteristics of friction stir welding (FSW) technique applied to Al-6005-T6 extruded sheets, which is a common material for railway car bodies. With the welding speed fixed at 300 mm/min, the revolution per minute (RPM) of the rotating tool was varied from 600 to 1800 RPM, with the aim at evaluating the resultant microstructure and mechanical behaviors. Comparison is also made with the conventional Metal Inert Gas (MIG) welding technique. Unlike MIG, no micro-voids were observed for FSW specimens. Hardness measurement revealed that the increased heat input by increasing RPM results in widened heat affected zone (HAZ) and decreased hardness for HAZ due to grain coarsening. Hardness results for the nugget do no show difference. During tensile tests, specimens fractured at HAZ, and increasing rpm led to decrease of the yield stress and tensile stress for the selected RPM range, which is considered to be due to the grain coarsening for HAZ.

Relationship Between Tool Rotating Speed and Properties of Friction Stir Welded Al 6005-T6 (알루미늄 합금 (Al6005-T6)의 마찰교반접합 시 공구의 회전속도와 접합 특성의 상관관계 연구)

  • Choi, Dooho
    • Journal of Convergence for Information Technology
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    • v.9 no.7
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    • pp.94-99
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    • 2019
  • Friction stir welding was first reported by TWI(The Welding Institute) in 1991, and this welding method has been rapidly used in various industrial areas such railway, automobile, aerospace and shipbuilding industry. Here, we study core characteristics of friction stir welding (FSW) applied to Al 6005-T6 extruded sheets, which is the typical alloy used for railway car bodies. With the fixed welding speed of 500 mm/min, the rotating tool speed was varied from 600 to 1800 RPM. The results of hardness measurement revealed that the hardness of nugget area is ~70% with respect to the parent material, and for the selected range of rotation speed, no clear dependence was observed and the hardness values close to the parent materials were achieved for the area located 5 mm away from the welding interface. The tension test shows that yield strength and tensile strength were slightly decreased with increasing RPM, with no observed difference for the elongation.

Characterization and Microstructure of an Extruded Flat-Tubular-Type Alumina Filter (압출공정에 의한 수 처리용 평관형알루미나 필터의 미세구조와 특성평가)

  • Bae, Byung-Seo;Ha, Jang-Hoon;Song, In-Hyuck
    • Journal of the Korean Ceramic Society
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    • v.51 no.5
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    • pp.406-412
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    • 2014
  • In this study, flat-tubular-type alumina filters were manufactured using alumina powder of two sizes ($2.4{\mu}m$ ALM-44 and $0.4{\mu}m$ AP 400) by an extrusion process. The manufactured alumina filter was sintered at $1200-1600^{\circ}C$ for 1 h. As particle size increased, the largest pore size, average pore size and porosity increased; but density and linear shrinkage decreased. The alumina filter fabricated using ALM-44 powder sintered at $1500^{\circ}C$ was confirmed as the best water treatment filter after investigation of the bending strength, water permeability and impurity-removal efficiency of the experimental filters. This flat-tubular-type alumina filter is expected to be useful not only for direct water treatment, but also for use as a support filter during coating processes, to control pore size.

Segmented 평관형 SOFC에서 다공성 $MgAl_2O_4$ 지지체 제조 및 특성

  • Park, Seong-Tae;Choe, Byeong-Hyeon;Lee, Dae-Jin;Kim, Bit-Nam;Ji, Mi-Jeong
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.11a
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    • pp.273-273
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    • 2009
  • 고체산화물 연료전지 (Solid Oxide Fuel Cell, 이하 SOFC)는 제조형태에 따라 크게 평판형과 원통형으로 구분할 수 있다. 단위면적당 출력 효율이 높은 평판형의 장점과 원통형의 밀봉이 용이한 장점을 동시에 가지는 평관형 형태로 지지체를 제작하였으며, 셀의 배치를 평면상 직렬로 연결하는 다전지식으로 구성함으로 전극의 길이나, 셀 간격을 기존 평판형이나 원통형에 비해 대폭 감소시켜 단위면적당 전압 및 출력효율을 높이고자 하였다. Segmented 평관형 지지체의 소재로는 연료전지의 성능 특성에 관여하지 않으며 열사이클 저항성과 기계적 강도가 우수한 spinel구조를 가지는 $MgAl_2O_4$를 선정하였다. 연료가스의 원활한 공급이 가능하도록 carbon을 기공 전구체로 사용하여 압출성형하였으며 건조과정에서 crack이 생기지 않는 공정을 확립한 후 $1400^{\circ}C$ 에서 소결하였다. 제조된 지지체는 수은침투법과 3점 굽힘 강도법으로 기공율과 기계적 강도를 각각 측정하였다. Anode를 스크린 프린팅법으로 지지체 위에 적층한 후 미세구조를 확인하였고 이를 바탕으로 다공성이며 기계적 강도를 가지고 음극과의 반응이 없는 우수한 지지체를 제조할 수 있었다.

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Charactetristical Analysis of the Microstructure and the Stress-Strain Curves for the Evaluation of 7xxx Series Aluminum Extrudates (7xxx계급 알루미늄 열간 압출재의 평가를 위한 미세조직과 응력-변형률 곡선의 분석)

  • Lee, S.Y.;Woo, Y.H.
    • Journal of the Korean Society for Heat Treatment
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    • v.31 no.6
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    • pp.307-314
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    • 2018
  • Simple tensile tests and microstructural investigations have been performed on extrudates of high strength aluminum alloys such as 7075, 7021 and 7xxx(Sc) to understand correlation between extruding conditions and extruded properties. Tensile specimens which were taken from different locations at the same cross section of an extrudate were tested at room temperature and with a strain rate of $8.9{\times}10^{-5}/s$. The microstructures according to the locations at the cross section have been observed using optical microscopy and electron back-scattered diffraction (EBSD) mapping to characterize the effect on stress-strain curve. The results could be classified in three types independent of alloying contents and extusion methods. The fine differences in the stress-strain curves were resulted from inhomogenity in the microstructures according to locations of an extrudate which were performed through instantaneous extruding conditions such as temperature, strain rate and strain.

Microstructure of Rapidly Solidified Al 6061 Flake Powder and It's Extrudate (Al 6061 Flake 파쇄분말 및 압출재의 미세조직)

  • Cho S.S.;Jin D.Z.;Lee J.G.;Yim K.H.;Lee B.S.;Eum S.H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1999.05a
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    • pp.47-55
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    • 1999
  • The microstructure of Al 6061 powder milled from rapidly solidified flake and it's extrudate were investigated. The grain size of flake was about $0.8-1.5{\mu}m$ and the powder shape was spherical due to the milling condition. In the microstructure of extrudate, the unbinded powder boundary was found the front part of extrudate and all the macroscopic defects such as boundary defect, holes or cracks was not observed except the front part. It was found that the extrudate except 60cm of front part was useful part.

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