• 한국세라믹학회지
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• 제29권11호
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• pp.843-850
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• 1992

The purpose of this study was to describe the heterogeneity effects on Intermediate/Final microstructure in isothermal liquid phase sintering. Several kinds of pore shapes were made by the different in the heterogeneity stress level during Intermediate/Final stage. Specimen with 48% green density especially showed that the local regions of a sintered compact were subject to more rapid shrinkage than the surroundings. This densification limiting factors generally inhibited sintering and made the large isolated crack-like pore in heterogeneous microstructures.

• 산업기술연구
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• 제5권
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• pp.15-20
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• 1985

The microstructure of sintered body of two component(kaolin-pottery stone) system after firing was examined with scanning electron microscope. At first the pottery stone was melted into glassy phase and the kaoline was decomposed to mullite and silica at higher temperature. The interlocked mullite crystals and silica surrounded by glassy phase are belived to increase strength.

• 암석학회지
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• 제23권2호
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• pp.61-73
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• 2014

소백산육괴의 중앙부에 위치하는 경상북도 북후면-평은면 지역에서 주 구성암류인 선캠브리아기 변성퇴적암류와 중생대 화강암에 대한 변형된 암석 및 미구조 연구를 통하여 (동)북동-(서)남서 방향으로 발달하는 우수 주향 이동성 예천전단대의 상대적인 형성시기, 변형온도, 초압쇄암대의 분포 등을 파악하였다. 연성 변형된 주요 암석구조는 전단변형에 의해 형성된 압쇄구조면과 신장선구조 그리고 편마구조면 내지 압쇄구조면이 습곡되어 형성된 (동)남동-버전스의 완침강-중경사 밀착습곡 등이 있다. 연성전단변형 동안에 형성된 장석들의 특징적인 미구조는 플레임 퍼어사이트, 밀메카이트, 미세단열, 미세킹크, 킹크대, 파동소광 등이 인지된다. 재결정된 석영집합체의 c-축 배열은 rhomb와 basal가 탁월한 미끄럼계로 작용하여 형성된 single girdle과 Type I crossed girdle 형태를 보여준다. 전단운동감각 결정면상에서 인지되는 전단운동감각은 우세한 방향성인 북서-경사와 부수적인 방향성인 남동-경사 압쇄구조면상에서 상부-북동-이동과 상부-남서-이동을 각각 보여준다. 이러한 특징적인 암석 및 미구조로부터 예천전단운동은 밀착습곡이 형성된 이후 발생하였으며, 예천전단운동이 발생할 당시의 변형온도는 $350{\sim}450^{\circ}C$이었음을 알 수 있다. 선캠브리아기 변성퇴적암류의 대상 분포와 변형된 선캠브리아기 변성퇴적암류의 장석과 중생대 화강암의 석영의 입도 분포로부터 불노봉과 박달산 북부를 통과하는 (동)북동 방향의 예천전단대의 초압쇄암대가 설정된다.

• 한국세라믹학회지
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• 제29권7호
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• pp.517-524
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• 1992

For the present study two alumina bodies were prepared. The sinter-aid alumina body(SAA) was made by conventional sinter-process using sintering additives of TiO2 & MgO/CaO and the reaction-bonded alumina (RBA) made from Al-Al2O3 mixed powder. A comparison was made between those two bodies and this investigation seeks to evaluate their microstructure, physical properties and material's reliability as well as their fracture behaviour. In spite of its considerable microstructural densification accompanied by sintering shrinkage, SAA is largely inferior to RBA in fracture strength. However, SAA shows a somewhat higher m-value than RBA in respect to the material's reliability, the Weibull modulus(m). RBA, which has high fracture strength, shows much longer lifetime under static loading than SAA. Though, as with m of fracture strength, the reliability(mt) of lifetime prediction in RBA is less high than of SAA.

• 한국세라믹학회지
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• 제16권4호
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• pp.206-212
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• 1979

The phase relations and microstructure appeared at 1700℃ in a system of Si3N4-Al2O3-SiO2 were studied. The samples were pressurelessly sintered at 1700℃ for 1hr and reheated at 1600℃ for 1hr under nitrogen atmosphere. The compounds formed were identified by X-ray diffraction method and the microstrues were observed by SEM. The stable phases appeared in this system were X-phase, Si2ON2, β'-Si3N4 and Mullite. From the results of those experiments, it was concluded that the X-phase has very close composition to that proposed by G, K. Layden, Si3Al6O12N2. SEM photographs showed that Si2ON2 was a plate phase and X-phase was a rectagular plate phase.

• 한국세라믹학회지
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• 제19권2호
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• pp.121-126
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• 1982

This paper deals with the $Si_3N_4$-bonded SiC refractory in terms of its microstructure development during nitridation. When mixture of SiC grains and fine Si power is fired under nitrogen atmosphere, an interlocking network of $Si_3N_4$ whiskers is formed by nitridation of Si. It is found that the strength of $Si_3N_4$-bonded SiC refractory is soley due to the physical nature of this interlocking whiskers. At the initial stage of nitridation, $Si_3N_4$ whisker forms in very thin and long shape and, with further nitridation, it becomes thicker with diameters up to 0.35$\mu\textrm{m}$. It is found that the mechanical strength of $Si_3N_4$-bonded SiC refractory depends on the degree of nitridation and the development of microstructure.

• 한국세라믹학회지
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• 제28권10호
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• pp.751-756
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• 1991

Continuous microstructural changes on heating of hardened paste prepared from primary clinker of CA2 composition was studied. On heating period, several characteristic shrinkages and microstructural changes took place in the specimen due to the dehydration and recrystallization of calcium aluminates without regard to the accelerative shrinkage resulted from sintering. Though micropores formed by dehydration decreased with recrystallization of calcium aluminates, micropores formed by plate-type gibbsite in the hydrates were maintained up to the temperature at which CA2 becomes main phase and had influence to the microstructure of the final clinker.

• 한국세라믹학회지
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• 제20권3호
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• pp.217-226
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• 1983

Adquate amount of calcia was added to the regent-grade Zirconia body. Here the amount and the form of calcia were 7-21 mol% and regent-grade calcium cabonate respectively. The specimens were fired at 175$0^{\circ}C$ for 0, 3, 5 and 7 hours respectively. The phase Strength X-ray diffraction analysis and Scaning electron microscopy. The results were as follows (1) As the additive amount of calcia was increased the firing linear shrinkage apparent density compressive strength and modulus of rupture decreased but the apparent porosity increased. (2) The specimens soaked and containing calcia displayed the grain growth. (3) Monoclinic and cubic zirconia were seen in the sepcimens containing 7 mol% calcia. When without soaking the specimens containing 7-10 mol% calcia had the volume change by monoclinic$\rightleftharpoons$tetragonal transformation. (4) The lattice parameter increased according as the calcia additive was increased. The specimens containing above 19mol% calcia had the costant lattice parameter. The value of that was from 5.1264 to 5.1396 $\AA$ in the case of 7 hours soaking.

• 한국세라믹학회지
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• 제36권12호
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• pp.1342-1349
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• 1999

In order to improve the density and the mechanical strength without change in chemical composition the hardened pastes of hydroxyapatite cement were reinforced with powders and/or whiskers of hydroxyapatite. The powders behaved as a seed of hydroxyapatite formation rather than a filler while the whiskers were mrerly dispersed in matrix and capillary pores of the hardened bodies leading to increase in mechanical strength. But the increase in strength But the increase in strength was nnt enough owing to the lack of homogeneous dispersion of the fibers. The highest diametral tensile strength of 18.5 MPa was measured at the hardened hydroxyapatite body in which well-dispersed whisker phase formed uniformly during hydro-thermal curing of power-added and dry-formed hydroxyapatite cement.

• 암석학회지
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• 제7권3호
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• pp.190-206
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• 1998

북부 소백산육괴의 중남부에 위치한 장군봉지역의 고생대 변성퇴적암류(조선누층군과 평안층군)에 대한 미구조와 변형작용과 변성광물들 성장(변성작용) 사이의 상대적인 시간관계를 연구하였다. 첫 번째 변성작용은 스태크상 클로리토이드 및 조립 흑운모와 안구상 홍주석 광물들의 결정화작용과 관련된 저압형 변성작용으로 인지된다. 이러한 변성작용은 동-서향의 등사 향사습곡(장군봉 습곡)과 그 축면엽리에 해당하는 S1 엽리면 형성과 관련된 D1 변형 이전의 비변형조건하에서 발생하는 고생대 변성퇴적암류에 광역적인 동-서향의 광물분대를 형성시켰다. 두 번째 변성작용은 직선 내지 곡선 형태의 내부엽리 Si를 갖는 십자석과 석류석 반상변정들의 성장과 관련된 중압형 변성작용이다. 이러한 변성작용은 장군봉 습곡 구성지층들의 부분적인 결손을 초래하는 동-서향 드러스트들의 발달과 관련된 D1 변형 이후의 비변형조건하에서 발생하였고, 동-서향의 예천전단대 형성과 관련된 D2 변형 동안에 계속 발생하여 고생대 변성퇴적암류에 역시 광역적인 동-서향의 광물분대를 형성시켰다. 세 번째 변성 작용은 팻치상 홍주석과 주상 내지 섬유상 규선석 그리고 조립 석류석 광물들의 성장과 관련된 쥬라기 춘양화강암에 의한 접촉변성작용이다. 이러한 접촉변성작용은 S3 파랑엽리면 형성과 관련된 D3 변형 이전의 비변형조건하에서 발생하였고, D3 변형의 전기단계 동안에 계속 발생하여 춘양화강암체의 근접부에 제한된 남-북향의 광물분대를 형성시켰다.