• Title/Summary/Keyword: 마이크로핀

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Synthesis of Reduced Graphene-metal Hybrid Materials via Ion-exchange Method and its Characterization (이온교환법에 의한 환원 그래핀-금속 하이브리드 소재의 합성 및 특성)

  • Park, Aeri;Kim, Sumin;Kim, Hyun;Han, Jong Hun
    • Journal of the Microelectronics and Packaging Society
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    • v.27 no.4
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    • pp.25-37
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    • 2020
  • In this study, hybridization of graphene oxide and metal was carried out by the functional groups containing oxygen and thermal treatment for reduction in order to enhance the electrical conductivity and magnetic properties of graphene materials. Graphene-metal hybrid materials were synthesized using the oxygen-containing functional groups (-OH, -COOH and so on) on the surface of graphene oxide by replacing them with metal ions via ion exchange method as well as thermal reduction. The metals used in this study were Fe, Ag, Ni, Zn, and Fe/Ag, and it was confirmed that metal particles of uniform size were well dispersed on the graphene surface through SEM, TEM, and EDS. All of the metal particles on the graphene surface had an oxide-crystalline structure. To check the electrical properties, sheet resistance of the rGO-metal hybrid sample was measured on the PET film made by the dip-coating, and the specific resistance was calculated by measuring the thickness of the specimen through SEM. As a result, the specific resistance was in the range of 2.14×10-5 and 3.5×10-3 ohm/cm.

An Analysis of Arbitrarily Shaped Microstrip Antennas Using Transmission - Line Matrix Representation and Moment Methods (전송선로의 매트릭스 표현법과 모멘트법을 이용한 임의 형태를 갖는 마이크로스트립 안테나의 해석)

  • 조원서;김정기
    • The Proceeding of the Korean Institute of Electromagnetic Engineering and Science
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    • v.2 no.2
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    • pp.11-18
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    • 1991
  • In this paper, the analysis of arbitrarily shaped microstrip antennas is described. The analysis method is based on the transmission - line matrix representation for the interior problem and the moment method for the problem along the peripheries of the patch. Using this method, the input impedance and other antenna parameters are calculated and compared with experimental results for a circular and an equilateral triangular microstrip antenna. For all of the results, theoretical and expreimental results are in good agreement and the validity of the method is confirmed. This analysis can also be used to analyze microstrip antennas with shorting pins.

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그래핀 표면 접착력을 이용한 전주도금 공정

  • No, Ho-Gyun;Park, Mi-Na;Lee, Seung-Min;Bae, Su-Gang;Kim, Tae-Uk;Ha, Jun-Seok;Lee, Sang-Hyeon
    • Proceedings of the Korean Vacuum Society Conference
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    • 2016.02a
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    • pp.131-131
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    • 2016
  • 기원전 5000년 이집트에서부터 시작된 도금은 시간이 지남에 따라 점점 발전하여, 1900년대에 들어 전기를 이용한 도금공정이 개발되었고, 현재 뿌리산업으로써 각종 제조업에 널리 이용되고 있다. 도금 공정은 금속을 부식으로부터 보호하고, 제품의 심미성과 기능성, 생산성 등을 높이기 위해 주로 이용된다. 전주도금 공정은 완벽하게 동일한 형태의 생산품을 다량으로 제작 할 수 있기 때문에, 그 높은 생산성으로 주목 받고 있다. 특히, 나노/마이크로 크기의 정밀 소자 등을 가공하는 차세대 기술인 LIGA공정과 접목이 가능하다는 장점이 있다. 몰드를 이용하여 복제하는 방식인 전주 도금은 도금공정이 끝난 후 몰드와 완성된 제품을 분리해내는 추가공정이 필연적으로 발생하게 되는데, 둘 사이의 접착력을 낮추기 위하여 몰드의 표면에 이형박리제를 도포하게 된다. 이형박리제로는 전기가 잘 흐르면서 접착력이 낮은 이산화 셀렌이나 중크롬산이 주로 이용되지만, 원활한 박리를 위해서는 그 두께가 30 um 이상 확보되어야 하기 때문에 정밀한 미세구조 전주도금이 어렵다는 문제점이 있다. 또한 이와 같은 화학 약품들은 매우 유독하기 때문에 추가적인 폐수 처리 공정이 필요하며, 작업자의 안전을 위협하고 심각한 환경 오염을 초래한다는 추가적인 문제가 발생한다. 따라서, 매우 얇고 친 환경적이며 안전한 전주도금 이형박리제에 대한 연구가 요구되고 있다. 본 연구에서는 전주도금 몰드로 사용한 구리의 표면에 TCVD를 이용하여 단일 층 그래핀을 성장시킨 후, 그래핀이 코팅된 몰드에 구리를 전주도금하여 박리하였다. 박리 후 그래핀은 몰드에 손상 없이 남아있는 것을 Raman microscopy를 통해서 확인하였고, 몰드와 그래핀 사이의 접착력 (약 $0.71J/m^2$)에 비해 그래핀과 전주도금 샘플간에 낮은 접착력 (약 $0.52J/m^2$)을 갖는 것을 확인하였다. 이와 같이 낮은 접착력을 통해 박리 시 표면구조의 손상 없이 정밀한 구조의 미세 패턴구조를 형성할 수 있었다. 전주도금을 이용한 전극 형성과 고분자와의 융합을 통해 유연기판을 제작하여 bending 실험을 진행하였다. $90^{\circ}$의 bending 각도로 10000회 이하에서는 저항의 변화가 없었고, LED chip을 mounting한 후 곡률반경 4.5 mm까지 bending을 진행하여도 이상 없이 LED가 발광하는 것을 확인하였다. 위와 같은 전주도금 공정을 이용하여 고집적 전자기기, 광학기기, 센서기기 등의 다양한 어플리케이션의 부품제조에 활용될 수 있을 것으로 기대한다.

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Preparation of PVA/Graphene Oxide/Fe3O4 Magnetic Microgels as an Effective Adsorbent for Dye Removal (폴리바이닐알코올/그래핀 옥사이드/산화철 자성 마이크로겔을 이용한 염료 제거)

  • Go, Seongmoon;Kim, Keunseong;Wi, Eunsol;Park, Rae-Su;Jung, Hong-Ryun;Yun, Changhun;Chang, Mincheol
    • Composites Research
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    • v.35 no.2
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    • pp.98-105
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    • 2022
  • In this study, polyvinyl alcohol (PVA)/graphene oxide (GO)/iron oxide (Fe3O4) magnetic microgels were prepared using a microfluidic approach and the dye adsorption capacity of the microgels was confirmed. The adsorption capacity (qe) of the gels was evaluated by varying the dye concentration, pH, and contact time with the microgels. The dyes used in this work were methylene blue (MB), crystal violet (CV), and malachite green (MG), and microgels showed the highest adsorption capacity (191.1 mg/g) in methylene blue. The microgels exhibited the highest adsorption capacity in the dye aqueous solution at pH 10 due to the presence of atomic nitrogen ions (N+) on the dye molecules. The adsorption isotherm studies revealed that the Langmuir isotherm is the best fit isotherm model for the dye adsorption on the microgels, indicative of monolayer adsorption. The kinetic analysis exhibited that the pseudo-second order model fits better than the pseudo-first order model, confirming that the adsorption process is chemisorption. In addition, the magnetic microgels showed good reusability and recovery efficiency. It was confirmed that the adsorption capacity of the gels maintains more than 70% of the initial capacity after 5 times of cycle experiments.

Experiments on Condensation Heat Transfer Characteristics and Flow Regime Inside Microfin Tubes (마이크로핀관내 유동 양식과 응축 열전달 특성 연구)

  • 한동혁;이규정
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.13 no.7
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    • pp.602-611
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    • 2001
  • Experiments on the condensation heat transfer characteristics inside a smooth and a microfin tube with R410A/R22 are performed in this study. The test tubes 7/9.52 mm in outside diameters and 3m in length are used. Varying the mass flux of the refrigerant and the condensation temperatures, the average heat transfer coefficients and pressure drop are investigated. Most flows in this study are in the annular and/or wavy flow regime. It is shown that the heat transfer is enhanced and the pressure drops are larger in the microfin tube than the smooth tube. From the heat transfer enhancement coefficients and the pressure drops, it is found that the high heat transfer enhancement factors are obtained in the range of small mass flux while the penalty factors are almost equal. Experiments results show that average heat transfer coefficients of R410A is larger than that of R22 and pressure drop of R410A is less than R22.

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Slit Folded Type Microstrip Antenna for Omnidirectional E-plane and H-plane (전방향성 E & H면 슬릿 Folded형 마이크로스트립 패치 안테나)

  • 김종래;우종명;오승엽
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.13 no.9
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    • pp.956-963
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    • 2002
  • A linearly polarized folded type and H-shape slit folded type microstrip patch antenna at GPS(center frequency:1.575 GHz) were designed and fabricated by folding a conventional single $\lambda_{g}/2(\lambda_{g}:wavelength)$ rectangular patch a half along the length direction at the center of patch and inserting ground plane in the middle. As a result, two types of omnidirectional radiation patterns for E-plane (for zx-plane) in the direction of the length of patch and H-plane (for xy-plane) have been acquired. The experimental results show that the average gains of folded type and slit folded type for omnidirectional E-plane and H-plane are -1.5 dBd (-2.4 dBd) and -3.27 dBd(-2.5 dBd). Slit folded type microstrip patch antenna was more miniaturized than folded type microstrip patch antenna by 27.5 %. In case of slit folded type antenna, average gains of omnidirectional radiation pattern for E & H-plane are almost same.

Condensation and evaporation heat transfer characteristics of HFC-134a in a horizontal smooth and a micro-finned tube (수평 평활관과 마이크로핀 관내에서 HFC-134a의 응축 및 증발열전달 특성)

  • Lee, Sang-Cheon;Park, Byeong-Deok;Han, Un-Hyeok;Lee, Jae-Hui
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.20 no.5
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    • pp.1725-1734
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    • 1996
  • Experimental condensation and evaporation heat transfer coefficients were measured in a horizontal smooth tube and a horizontal micro-finned tube with HFC-134a. The test sections are straight, horizontal tubes with have a 9.52mm outside diameter and about 5000mm long. The micro-finned tube had 60 fins with a height of 0.12mm and a spiral angle of 25.deg.. The condensation test section was a double-pipe type with counter flow configuration. The evaporation test section employed an electic heating method. Enhancement factors which is defined as a ratio of the heat transfer coefficient for micro-finned tube to that for smooth tube, varied from 1.3 to 1.6(mass flux:110~190kg/m$^{2}$s) for condensation and 1.2 to 1.5 (mass flux:70~160kg/m$^{2}$s) for evaporation. The experimental data of condensation and evaporation heat transfer coefficients were compared to several empirical correlations. Based on these comparisons, modified correlations of the condensation and evaporation heat transfer coefficient for both smooth and micro-finned tubes were proposed.

Evaporation Heat Transfer Characteristics of Propane and Iso-butane in Micro-fin Tubes (마이크로핀관에서 프로판과 이소부탄의 증발 열전달 특성에 관한 연구)

  • Son, Chang-Hyo;Roh, Geon-Sang
    • Journal of the Korean Institute of Gas
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    • v.11 no.4
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    • pp.35-40
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    • 2007
  • In this paper, evaporation heat transfer characteristics of propane and iso-butane in micro-fin tubes were investigated experimentally. Test section has a micro-fin tube with outside diameter of 12.70 mm, and 75 fins with a fin heights of 0.25 mm. The experimental results summarize as the followings: The average evaporation heat transfer coefficients of He's refrigerants is higher than those of HCFC22, and appeared in the order of iso-butane, propane with respect to the approaching of the high mass flux. The evaporation heat transfer coefficient of micro fin tube is about $10{\sim}80%$ higher than those of smooth tube. This results from the study can be used in the case of designing heat transfer exchanger using hydrocarbons as the refrigerant for the air-conditioning systems.

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Effect of the lubrication oil on heat transfer and pressure drop characteristics of supercritical carbon dioxide in a microfin tube (마이크로핀관내 냉동기유가 초임계 이산화탄소의 열전달과 압력강하에 미치는 영향)

  • Ku, Hak-Keun
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.13 no.4
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    • pp.1440-1446
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    • 2012
  • This paper presents an experimental study of heat transfer and pressure drop characteristics of supercritical carbon dioxide with PAG inside a horizontal microfin tube. Heat transfer coefficient and pressure drop gradients were measured at 10 MPa in pressure and 520 kg/$m^2s$ in mass flux with variation of PAG mass concentration from 0.06% to 2.26%. The tendencies of both heat transfer and frictional pressure drop characteristics show the same as those of pure $CO_2$ up to 0.3% in PAG mass concentration. In case of 2.26% in PAG mass concentration, measured heat transfer coefficients showed 50% lower than those of pure $CO_2$ near the pseudocritical temperature and measured frictional pressure drop gradients show 1.6 times higher in comparison with those of pure $CO_2$ at $60^{\circ}C$ in $CO_2$ bulk temperature.

Development of Wideband Spatial Combined High Power Amplifier (광대역 공간 결합 고출력 전력증폭기 개발)

  • Lee, Ho-Seon;Park, Kwan-Young;Kong, Tong-Ook;Chun, Jong-Hoon
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.28 no.4
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    • pp.286-297
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    • 2017
  • This paper is a study of 6~18 GHz wideband high power amplifier which is composed of 10 single amplifier and coaxial type spatial power combiner. The property of this spatial power combiner is on a similar principle to antipodal antenna radiation mechanism. Therefore, the key structure of proposed spatial power combiner is the antipodal finline PCB board and the finline curve shape is numerically synthesized by using Klopfensein's optimum impedance taper. The measured CW output power of spatial combined high power amplifier is nearly 50 W. In conclusion we prove the good combining performance between the spatial power combiner and 10 single amplifier over 6~18 GHz frequency ranges. Also, we developed the key component PA and MFC MMIC which controls the phase and gain of the each amplifier, The main characteristic of MFC MMIC is to maximize combining efficiency of power amplifier.