• Proceedings of the Materials Research Society of Korea Conference
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• 2003.03a
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• pp.26-26
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• 2003

본 연구에서는 누적압연접합공정(ARB)을 통하여 5052 알루미늄 합금의 결정립을 약 0.2$\mu\textrm{m}$ 크기로 미세화 하였다. 누적압연에 의한 변형량 증가에 따른 미세 조직 변화와 결정립 간의 상대적인 방위각 차이를 TEM을 이용하여 관찰하였다. 누적 변형량을 함수로 상온 인장특성을 분석하였고, 초미세립 소재를 후속 열처리한 후 미세 조직 변화를 관찰하여 제조된 초미세립 소재의 열적 안정성을 평가하였다. 상온 대기 중에서 pin-on-disk 형태의 마멸시험기를 사용하여 초미세립 소재의 미끄럼 마멸시험을 변형량과 하중을 변수로 행하였다. 강소성 변형에 의해 제조된 5052 알루미늄 합금 소재의 마멸저항성은 강소성 변형 전과 비교하여 소재의 경도가 크게 증가하였음에도 불구하고 오히려 감소하였다. 마멸시험 후 마멸면의 SEM, 마멸단면의 OM 관찰과 마멸면 직하의 깊이에 따른 경도측정을 통하여 초미세립 소재의 마멸기구를 분석하였고 마멸표면의 변형 층을 관찰하였다. 또한 마멸면 직하 조직의 TEM 관찰을 통해서 마멸시험 중의 미세 조직 변화를 연구하였다.

• Proceedings of the Materials Research Society of Korea Conference
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• 2003.03a
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• pp.28-28
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• 2003

고온가압소결(Hot Pressing) 된 다이아몬드 공구용 Co-Fe, Co-Ni계 금속본드의 상온 건식 미끄럼 마멸시험을 행하고, 조성에 따른 각 본드의 마멸 특성을 비교하고 마멸 기구를 규명하였다. 미끄럼 마멸시험은 pin-on-disk 형태의 마멸시험기를 사용하여 각 조성의 성분, 적용하중 그리고 마멸상대재를 변수로 상온, 대기 중에서 실시되었다. 마멸속도는 마멸시험 전후의 시편의 무게 감량을 이론밀도와 거리로 나누어 계산되었다. 마멸기구의 규명을 위하여 시험된 시편의 마멸면과 마멸단면을 SEM과 EDS를 이용하여 분석하였다. 시험 결과 Co-Fe system의 경우 그 마멸속도는 마멸상대재의 영향보다는 Fe 첨가에 따른 시편의 미세조직과 기계적 성질의 차이에 따라 크게 변화하였다. 그러나 Co-Ni system의 마멸속도는 마멸 상대재에 따라 크게 변화하는 것이 관찰되었다. $Al_2$O$_3$를 상대재로 마멸된 경우에는 마멸속도가 시편/상대재 접촉면에서 형성되는 산화층의 영향을 크게 받았고, glass bead(83% SiO$_2$)를 상대재로 한 경우에는 시편의 경도와 마멸속도는 서로 반비례하였다.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 1993.04a
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• pp.70-79
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• 1993

세라믹은 금속에 비해서 밀도가 낮고, 내마멸성이 우수하고, 열팽창계수가 작고, 높은 온도범위에 걸쳐서 안정성과 경도를 유지함으로 기계구조용재료로서 유망시 되고 있다. 앞으로 세라믹부품에 대한 수요는 더욱 증가하리라고 예상하고 있으며, 세라믹의 응용이 시도되고 있는 부품은 더욱 다양화되어가고 있는 추세이다. 그러나, 세라믹재료에 관한 신뢰할만한 데이터베이스는 확립되지 못한 상태이고, 트라이보시스템에 관한 수명예측과 설계를 위한 기초 자료도 확립하지 못한 상태에 있다. 세라믹재료에 관한 수명예측과 설계를 위해서는 세라믹재료의 트라이보시스템(tribosystem)에서의 마멸기구의 규명과 마멸율을 평가할 수 있는 마멸식을 구하는 것이 가장 기본적인 과제라 할 수 잇다. 따라서 본 연구에서는 최신 기법에 의해서 제조된 HIP제 질화규소와 지르코니아를 실험재료로 하여 무윤활하에서의 미끄럼 마찰$\cdot$마멸실험을 수행하여 마찰$\cdot$마멸특성을 규명하고, SEM을 이용한 마멸면의 미시적 관찰을 통해서 세라믹의 마멸기구를 조사하여 세라믹마멸기구의 마멸모델을 제히하고자 한다. 제시된 마멸모델에 파괴역학을 도입하여 이론해석과 고찰을 수행하여 보다 실용적인 세라믹의 마멸율을 평가할 수 있는 새료운 무차원파라메타를 제안하고자 한다.

• Transactions of the Korean Society of Mechanical Engineers
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• v.17 no.6
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• pp.1441-1455
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• 1993

Under unlubricated condition, the friction and wear tests of silicon nitride and zirconia manufactured by HIP were carried out at room temperature. The wear resistance of silicon nitride was superior to that of zirconia under low load, whereas the wear resistance of zirconia was superior to that of silicon nitride under high load. Wear model of ceramic was suggested by the microscopic SEM observation of worn surfaces and debris. Theoretical analysis and discussions based on linear fracture mechanics were made out about this ceramic wear model. From the theoretical analysis, a new nondimensional parameter, Scf, was introduced to estimate wear rate of ceramics. This new nondimentional parameter consists of contact pressure, surface defect of contact material, frictional coefficient and fracture toughness.

• Transactions of the Korean Society of Mechanical Engineers
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• v.19 no.9
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• pp.2122-2132
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• 1995

There are some cases which require to grasp the abrasion resistance property in the fields of the high-technology to be required the high specific strength and modulus. In this study, wear test with the various test temperature and velocity were performed in the SiCw/A16061 composite and A16061 matrix using the wear test machine of the ring-on-disc type. As the results, the friction and wear properties by various test temperature and velocity were examined. The worn surface has observed by scanning electron microscope in order to examine the wear mechanism.

• Journal of the Korean Ceramic Society
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• v.39 no.1
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• pp.79-85
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• 2002

Plasma-sprayed Cr$_2$O$_3$-based coatings containing MoO$_3$were studied to gain a better understanding of the influence of MoO$_3$composition in the coatings on their tribological behaviour. A reciprocal type tribo-tester was employed to examine friction and wear behavior of the specimens at room temperature. The physical characteristics of worn surfaces were investigated by scanning electron microscopy and chemical composition of the coating surfaces was analyzed using a X-ray photoelectron spectrometer. The results showed that friction coefficient of the MoO$_3$-added coatings were lower than those without MoO$_3$addition. However pure Cr$_2$O$_3$coating showed the lowest wear loss at the self-mated test. The larger protecting layers were observed at the worn surface of plasma spray coated specimens with MoO$_3$addition. XPS analysis of the protecting layer indicated that MoO$_3$composition was dominantly formed at the surface. MoO$_3$composition in the protecting layer appears to be more favorable in reducing the friction.

• Transactions of the Korean Society of Mechanical Engineers
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• v.13 no.4
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• pp.604-610
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• 1989

This paper is concerned with the machinability of fine ceramics(Al$_{2}$O$_{3}$) by using sintered diamond tools. For this purpose, ceramics cutting experiments under various cutting conditions such as cutting speed, feed rate, and others were carried out. The main results are follows : (1) During the cutting of fine ceramics, the used tools were found to be slightly chattering at cutting speed of 70m/min, and at cutting speed of higher than this I found the fine ceramics difficult to be cut. (2) When I used a tool with large nose radius, there occured a small amount of wear on the flank of the tool. However, at the early stage of fine ceramics cutting, the tools with smaller nose radii were required mainly to prevent the chipping of the ceramics. (3) When the materials were dry-cut, the appropriate cutting speel was found to be lower than 40m/min, and when the materials were dry-cut, I could cut them without any difficulty even at the speed of 70m/min, the surface roughness of ceramics cut at the speed of 70m/min was considerly fine. (4) It is generally believed that the principal cutting force is the largest in the case of steels cutting, but I found the thrust cutting force to be larger than any other cutting forces in the case of ceramics cutting.

• Journal of the Korean Ceramic Society
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• v.39 no.9
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• pp.851-856
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• 2002

Tribological behavior of plasma-sprayed $Cr_2O_3$-based coatings containing $MoO_3$ at 450$^{\circ}C$ was investigated to understand the influence of $MoO_3$. A reciprocal disc-on-plate type tribo-tester was employed to examine fricition and wear behavior of the specimens. The microstructure and phase composition of the coating was characterized with Transmission Electron Microscopy(TEM). The TEM analysis indicated that $MoO_3$ was dispersed into the grain boundary, resulting in the increase of the hardness and density of the coating. Worn surfaces were investigated by scanning electron microscopy and chemistry of the worn surfaces was analyzed using a X-ray Photoelectron Spectrometer(XPS). The results showed that the friction coefficient of the $MoO_3$-added coatings was lower than that without $MoO_3$ addition. The larger protecting layers were observed at the worn surface of plasma spray coated specimens with $MoO_3$ composition in the protecting layer appears to be more favorable in reducing the friction.

• Journal of the Korean Society of Safety
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• v.12 no.4
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• pp.214-219
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• 1997

The mechanical seals, which are installed in rotating machines like pump and compressor, are generally used as sealing devices in the many fields of industries. The failure of mechanical seals such as leakage, crack, breakage, fast and severe wear, excessive torque, and squeaking results in big problems. To identify abnormal phenomena on mechanical seals and to propose the proper monitoring parameter for the failure of mechanical seals, sliding wear experiments were conducted. Acoustic emission, torque, and temperature were measured during experiments. Optical microstructure was observed for the wear processing after every 10 minute sliding at rotation speed of 1750 rpm and scanning electron microscopy was also observed. Except for the initial part of every experiment, the variation of acoustic emission was well coincided with torque variation during the experiments. This study concludes that acoustic emission and torque are proper monitoring parameters for the failure of mechanical seals. The intensity of acoustic emission signals is measured in root mean square voltage. Temperature of sealing face will be used as a parallel parameter for increasing the reliability of monitoring system.

• Journal of the korean academy of Pediatric Dentistry
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• v.28 no.2
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• pp.261-270
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• 2001

This study was performed to evaluate wear characteristics of light-cured composites when opposed by human enamel. Seven light-cured restorative composites were selected and enamel cusps sectioned from premolars. All samples were stored in distilled water at $37^{\circ}C$ for 10 days. 68.6 N of weight was loaded during the test. The measurements of vertical loss of enamel cusps, weight loss and volume loss of composites, and SEM observations of the polished and abraded surfaces were made after 30,000 cycles. The results obtained were summarized as follows; 1. The highest hardness value of 70.4 was observed in the Spectrum group and the lowest value of 19.8 was observed in the Heliomolar group. Results of Tukey test showed that an overall significant difference was indicated except the Spectrum, Z100 and Clearfil AP-X groups(p<0.05). 2. Enamel showed the good abrasion resistance against the Heliomolar group of microfilled composite and the Palpique Toughwell group containing the submicron hybrid type spherical fillers. 3. The abrasive wear resistance of hybrid composites was improved with the decrease of mean particle size and hybrid of submicron particle fillers. 4. SEM observation of worn surfaces revealed the protrusion, attrition and missing of fillers, cracks developing and delamination in the matrix.