• Proceedings of the Optical Society of Korea Conference
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• 2002.07a
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• pp.60-61
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• 2002

Laser-induced incandescence (LII) 측정법은 조사된 레이저에 의하여 입자가 가열됨에 따라서, 그 온도에 상응하는 흑체복사의 시간적 감소추이가 입자의 크기에 따라서 달리 나타나는 것을 이용하여 입자의 크기를 측정하는 방법이다. LII 감쇄법은 레이저에 의하여 가열된 입자의 에너지 균형 상관식에서 입자의 크기가 클수록 신호의 감쇄속도가 느리고, LII 신호의 감쇄비가 실험적으로 입자의 크기에 비례한다는 사실을 이용하여 연소진단에 응용되어 왔다. (중략)

• Journal of the Korean Society for Nondestructive Testing
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• v.19 no.1
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• pp.16-24
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• 1999

Residual stress is one of the causes which make defects in engineering components and materials. And interest in the measurement of residual stress exists in many industries. There are commonly used methods by which residual stresses are currently measured. But these methods have a little demerits. time consumption and other problems. Therefore we devised a new experimental technique to measure residual stress in materials with a combination of laser speckle pattern interferometry, finite element method and spot heating. The speckle pattern interferometer measures in-plane deformations while the heating provides for very localized stress relief. FEM is used for determining heat temperature and other parameters. The residual stresses are determined by the amount of strain that is measured subsequent to the heating and cool-down of the region being interrogated. A simple model is presented to provide a description of the method. In this paper, the ambiguity problem for the fringe patterns has solved by a phase shifting method.

• Journal of the Korean Society of Combustion
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• v.1 no.1
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• pp.75-82
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• 1996

Laser induced incandescence, LII, recently developed technique for measuring soot concentration in flames, can overcome most of limitations of conventional laser extinction measurement. In this study, experiments were performed to investigate the effect of laser intensity, detection wavelength, and also laser beam quality on both LII signal at a particular position and peak-to-centerline LII signal ratio. The results of LII signal with increasing laser intensity shows its near-independence of laser intensity once threshold level of laser intensity has been reached. However, this near-independence depends on laser beam quality and the incident optical setup. The peak-to-centerline LII signal ratio slowly but continuously increases with laser power. This fact is due to the dependence of LII signal on particle mean diameter. LII signal is attenuated during it passes through the flame containing soot particles. The attenuation rate is inversely proportional to detection wavelength. In this study, LII signal at 680 nm band is 10% greater than the signal at 400 nm band.

• Electrical & Electronic Materials
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• v.3 no.3
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• pp.187-194
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• 1990

광자기 메모리용 재료인 비정질 TbFe 박막을 대상으로 열자기 기록시 박막에 분포하는 온도와 이때 만들어지는 bit의 크기간에 상호관련성을 조사하였다. 레이저 조사에 의해 가열된 박막의 온도분포는 유한요소법을 이용한 열전달 해석에 의해 계산하였다. 레이저 가열종료 직전 박막 면에 분포하는 온도 contour로 부터 bit 크기를 예측하였다. 여기서 bit 크기는 온도 상승에 따라 보자력이 약화되어 외부자계와 박막반자장의 합력이 역자구를 만들어 준다고 가정하여 이 경계가 되는 온도(Tcrit)로 이루어지는 등온선의 크기로부터 정하였다. 열자기 기록 실험으로부터 기록 bit의 크기(Dmeas.)을 측정하여 레이저조사조건별로 예측한 bit크기(Dpred.)와 비교하였다. 특히, 레이저 pulse시간 변화에 따른 여러온도의 등온선 contour 직경변화를 조사하여 실측한 bit크기와 비교 검토함으로써 bit형성에 미치는 온도분포의 영향을 조사하였다. 이 결과 레이저 pulse시간이 길어지거나 레이저 power가 상대적으로 작을때 실측한 bit크기가 예측된 bit크기보다 커지는 것으로 나타났으며 이는 Tcrit 온도구배가 완만해질수록 bit경계가 되는 온도가 낮아지는 것으로 해석된다.

• 한국연소학회:학술대회논문집
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• 1997.06a
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• pp.45-50
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• 1997

An experimental study on LII signal images from soot particles in a flame has been carried out in order to investigate the effect of the incident laser characteristics. By changing the wavelength of the incident laser beam, the LII signal was saturated at smaller laser power with 532 nm than 1,064 nm. This implies that the larger absorption coefficient of soot particles at 532 nm would influence the LII signal characteristic. Using the deconvolution technique, the projected LII line images were coverted to reconstruct the local LII signals inside the beam. The results show that the LII images at ICCD camera result from the integration of LII signal across the laser beam.

• Journal of the Korean Society for Precision Engineering
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• v.25 no.3
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• pp.101-108
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• 2008

Residual stress is one of the causes which make defects in engineering components and materials. Many methods have been developing to measure the residual stress. Though these methods provide the information of the residual stress, they also have disadvantage like a little damage, time consumption, etc. In this paper, we devised a new experimental technique to measure residual stress in materials with a combination of laser speckle pattern interferometry and spot heating. The speckle pattern interferometer measures in-plane deformation during the heat provides for much localized stress relief. 3-D shape is used for determining heat temperature and other parameters. The residual stresses are determined by the amount of strain that is measured subsequent to the heat and cool-down of the region being interrogated. A simple model is presented to provide a description of the method. In this paper, we could experimentally confirm that residual stress can be measured by using laser interferometry and spot heating method.

• Proceedings of the Korean Vacuum Society Conference
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• 2011.08a
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• pp.295-295
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• 2011

CIGS박막을 동시 증발법(co-evaporation)으로 몰리브덴이 증착된 소다라임 유리 위에 성장시켰다. CdS 박막은 화학적 용액 성장법 (chemical bath deposition: CBD)을 이용하여 약 60 nm를 증착하였다. 열처리는 가열판 (hot-plate)을 사용하여 공기중에서 하였다. 열처리 온도는 0~350$^{\circ}C$까지 변화하였으며, 열처리 시간은 각각 5분이었다. 시료의 표면 및 계면의 변화를 SEM측정을 통하여 관측하였다. CdS/CIGS 박막의 열처리 온도 변화에 따른 photoluminescence 특성을 조사하였다. 여기 레이저는 488 nm ($Ar^+$ laser)와 632.8 nm (He-Ne laser)를 사용하여 결함의 근원을 조사하였다. 온도 의존성 실험을 통하여 CIGS 박막의 띠 간격 에너지를 확인할 수 있었으며, 결함 준위의 활성화 에너지 및 특성을 알 수 있었다. $Ar^+$ laser에서만 관측되는 신호의 근원은 CdS에 기인한 것이었다.

• Transactions of the Korean Society of Automotive Engineers
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• v.5 no.3
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• pp.54-65
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• 1997

To quantify the LII signals from soot particle of flames in diesel engine cylinder, a new method has been proposed for correcting LII signal attenuated by soot particles between the measuring point and the detector. It has been verified by an experiment on a laminar jet ethylene-air diffusion flame. Being proportional to the attenuation, the ratio of LII signal at two different detection wavelengths can be used to correct the measured LIIsignal and obtain the unattenuated LII signal, from which the soot volume fraction in the flame can be estimated. Both the 1064-nm and frequency-doubled 532-nm beams from the Nd : YAG laser are used. Single-shot, one-dimensional(1-D) line images are recorded on the intensified CCD camera, with the rectangular-profile laser beam using 1-mm-diameter pinhole. Two broadband optical interference filters having the center wavelengths of 647 nm and 400 nm respectively and a bandwidth of 10 nm are used. This two-wavelength correction has been applied to the ethylene-air coannular laminar diffusion flame, previously studied on soot formation by the laser extinction method in this laboratory. The results by the LII measurement technique and the conventional laser extinction method at the height of 40 nm above the jet exit agreed well with each other except around outside of the peaks of soot concentration, where the soot concentration was relatively high and resulting attenuation of the LII signal was large. The radial profile shape of soot concentration was not changed a lot, but the absolute value of the soot volume fraction around outside edge changed from 4ppm to 6.5 ppm at r=2.8mm after correction. This means that the attenuation of LII signal was approximately 40% at this point, which is higher than the average attenuation rate of this flame, 10~15%.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.22 no.8
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• pp.1073-1082
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• 1998

When thermal diffusivity is measured by laser flash method, the thermal diffusivity call be calculated front the assumption of the uniformly heated whole surface of the specimen. It has been known that the approximate 5% error is made by the non-uniform energy distribution on the specimen surface of laser pulse heat source. In this study, to obtain the highly-uniformed laser beam, which has both the low non-uniform heating error from non-uniform laser beam and the energy loss, research was carried out on no transmitting loss by optical fiber and high repetitions. In addition, heating error and thermal diffusivity were measured as the measuring positions were varied and compared with the results using the uniform and the non-uniform laser beams. In addition, dole to using the uniformalized laser beam, the whole surface of the specimen was heated uniformly and as a result, it was the thought that this was very effective to reduce the variations of the errors of the thermal diffusivity as the measuring positions were varied. It can be obtained that when the thermal diffusivity of POCO-AXM-5Q1 of SRM in NBS was measured with both the uniform and the non-uniform laser beams, the dispersion error of the former was from 2 to 2.5%, which was more improved than that of the latter.

• Korean Journal of Crystallography
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• v.9 no.1
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• pp.21-29
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• 1998

The rare-earth orthoborate family, RM3(BO3)4 is known to be the most promising material for the microlaser host. To grow LaSc3(BO3)4 single crystal, the phase relation of the system LaBO3-ScBO3 was investigated by DTA method. LaSc(BO3)4 was the unique intermediate compound in the binary system the peritectic reaction point of which was 1495 ±2℃. Owing to the peritectic behavior of the compound, the crystal growth of the rare-earth Sc-borate was carried out by pulling from the melt-soultion of La1+xSc3-x(BO3)4. The optimal conditions for the growth of LaSc3(BO3)4 were determined by traditional CZ method : pulling speed 0.7mm/hr, rotation speed 7-10 rpm under reduction condition. Pt and Ir crucibles could be used for about 8-10 times of growth. The effect of thermal configurations on the temperature distribution was investigated. A special two-coordinate manipulator was made for the precise movement of thermocouples from the melt to the top of the furnace for several thermal configurations. The radial gradient on the melt surface depends strongly on the construction of the afterheater. On the other hand, the axial gradient was mainly propotional to both the opening degree of baffle plate and the mutual positions of crucible and heater.