• Title/Summary/Keyword: 나노결정

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A Study on Inductive Power Line Communication with Metal Block Channel (금속블록 채널이 있는 유도형 전력선통신에 관한 연구)

  • Sohn, Kyung-Rak;Kim, Hyun-Sik
    • Journal of IKEEE
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    • v.25 no.1
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    • pp.95-100
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    • 2021
  • If we know the location of the hull block and the welding feeder in the shipyard, we can easily obtain the location information of the worker. That data is very useful for implementing a workplace safety monitoring system. However, it is difficult to apply a fixed communication network to the workplace due to the specificity of the hull structure and welding process. In this study, inductive power line communication, which can replace dedicated communication line, was reviewed. A ferrite core was used as an inductive coupler to be installed on the power cable of the welding machine, and a nano-crystalline core was applied as a coupler to be fastened to the support rod of the metal block. In order to visualize the operating principle of the proposed couplers, 3D modeling and finite element analysis were performed with the COMSOL AC/DC module. In the communication performance test using an aluminum profile, when the communication channel was formed by the contact of the welding electrode, the bandwidth was kept above 6 Mbps.

Effect of CaF2 Addition on the Crystallinity of Hexagonal Boron Nitride Nanoparticles (육방정 질화붕소 나노입자의 결정성에 미치는 불화칼슘 첨가의 영향)

  • Jung, Jae-Yong;Kim, Yang-Do;Kim, Young-Kuk
    • Korean Journal of Metals and Materials
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    • v.56 no.12
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    • pp.915-920
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    • 2018
  • With the development of modern microelectronics technologies, the power density of electronic devices is rapidly increasing, due to the miniaturization or integration of device elements which operate at high frequency, high power conditions. Resulting thermal problems are known to cause power leakage, device failure and deteriorated performance. To relieve heat accumulation at the interface between chips and heat sinks, thermal interface materials (TIMs) must provide efficient heat transport in the through-plane direction. We report on the enhanced thermal conduction of $Al_2O_3-based$ polymer composites, fabricated by the surface wetting and texturing of thermally conductive hexagonal boron nitride(h-BN) nanoplatelets with large anisotropy in morphology and physical properties. The thermally conductive polymer composites were prepared with hybrid fillers of $Al_2O_3$ macro beads and surface modified h-BN nanoplatelets. Hexagonal boron nitride (h-BN) has high thermal conductivity and is one of the most suitable materials for thermally conductive polymer composites, which protect electronic devices by efficient heat dissipation. In this study, we synthesized hexagonal boron nitride nanoparticles by the pyrolysis of cost effective precursors, boric acid and melamine. Through pyrolysis at $900^{\circ}C$ and subsequent annealing at $1500^{\circ}C$, hexagonal boron nitride nanoparticles with diameters of ca. 50nm were synthesized. We demonstrate that the addition of a small amount of calcium fluoride ($CaF_2$) during the preparation of the melamine borate adduct significantly enhanced the crystallinity of the h-BN and assisted the growth of nanoplatelets up to 100nm in diameters. The addition of a small amount of h-BN enhanced the thermal conductivity of the $Al_2O_3-based$ polymer composites, from 1.45W/mK to 2.33 W/mK.

Formation of Mesoporous Membrane by Reverse Thermally induced Phase Separation (RTIPS) Process Using Flash Freezing (Mesoporous 막 제조를 위한 급냉법에 의한 역 열유도상전이공정)

  • Yeom, Choongkyun;Kim, Jiwon;Park, Heeyoung;Park, Seong Eun;Lee, Kee Yoon;Lee, Kew-Ho
    • Membrane Journal
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    • v.31 no.1
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    • pp.67-79
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    • 2021
  • Mesoporous polystyrene (PS) and polyethersulfone (PES) membranes have been fabricated by reverse-thermally induced phase separation (RTIPS) process, using flash freezing. The mesoporous pores can be created by the nano-scaled phase separation induced by the formation and growth of solvent crystals in the dope solution in RTIPS process. RTIPS process has been characterized through analysis on the enthalpy change in the solvent of the dope solution, the morphology of the membrane fabricated with different polymer content, and the pore size distribution and its standard deviation of pore size of the membrane with polymer content via DSC, SEM, and BET, respectively. It is found that the kinetic aspect of the dope solution, i.e., the crystallization of solvent is a crucial factor to determine the structure of membrane fabricated in RTIPS rather than the thermodynamic aspect of the dope solution.

Chipped Titanium Scraps as Raw Materials for Cutting Tools (타이타늄 밀링/터닝 스크랩의 절삭공구 소재화)

  • Kwon, Hanjung;Lim, Jae-Won
    • Resources Recycling
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    • v.30 no.2
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    • pp.61-67
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    • 2021
  • Scraps are a byproduct of the machining process used for transforming titanium ingots into useful mechanical parts. Scraps take two forms, namely, bulky scraps, which are produced by cutting, and chipped scraps, which are produced by milling. Bulky scraps are comparatively easier to recycle because of their small surface area and less oxygen content; as a result, they pose only a small risk of explosion. In contrast, chipped scraps pose a higher risk of explosion, because of which, their recycling is complicated, resulting in most such scraps being discarded. With the aim of avoiding this waste, we proposed a novel process for converting chipped scraps into stable carbide materials. Methods typically applied to reduce particle size and impair the formation of solid solution type phase in the carbide materials were used to improve the mechanical properties of carbides prepared from chipped scraps. Our novel recycling process reduced carbide production costs and improved carbide quality.

Quantification Analysis of Element Surface by Fractal Dimension (프랙탈 차원에 의한 소자 표면의 정량화 분석)

  • Kyung-Jin, Hong
    • The Journal of the Institute of Internet, Broadcasting and Communication
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    • v.23 no.1
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    • pp.145-149
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    • 2023
  • High-resolution images of surfaces provide detailed information on pores or shapes with specific sizes ranging from nano sizes to micrometers. However, it is not yet clear to determine an efficient association for pores or shapes from high-resolution images of surfaces. For the efficient association of pores and shapes, the surface characteristics of the device were considered as fractal dimensions by taking SEM photographs and binarizing the images. The fractal program was directly coded for surface analysis of the device. The device surface characteristics and electrical characteristics are thought to be related to the fractal dimension. The fractal dimension decreased with an increase in internal pores. The density and grain boundary of particles, which are structural characteristics of the device surface, were related to the fractal dimension. The particle size decreased with an increase in the fractal dimension and was uniformly formed. When the particles were uniformly formed, fewer pores were present and the fractal dimension increased.

Study on the size-based separation of nano to micron particles in natural water and soil using flow and sedimentaion Field-flow fractionation (흐름 및 침강 장-흐름 분획법에 의한 자연수 및 토양 중 나노 크기로부터 마이크론 입자들의 크기별 분리에 관한 연구)

  • Eum, Chul Hun;Kang, Dong Young;Lee, Tae Woo;Lee, Seungho
    • Analytical Science and Technology
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    • v.22 no.1
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    • pp.75-81
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    • 2009
  • A flow and sedimentation field-flow fractionation method has been used to characterize colloidal particles in environmental samples. The opposed flow sample concentration (OFSC) method was employed. The OFSC procedure was optimized for the analysis of particles in ground water with respect to various experimental parameters including sample introduction time, flow rates, etc. The effectiveness in low concentration and characterization of the OFSC-FlFFF was demonstrated with GW-1 and GW-2 ground water samples. Ground water of upto 100 mL has been successfully loaded, concentrated, and characterized by OFSC-FlFFF. The OFSC technique allow the application of FlFFF possible for the separation and characterization of colloidal particles in very low concentrations. The results show FFF provides a simplified alternative to existing off-line concentration procedures, and shows a high potential for the applications to the analysis of dilute colloidal particles in the environmental samples.

Electrochemistry of bis(1,10-phenanthroline)copper(II)-sodium dodecyl sulfate solution in the presence of MgCl2 (염화마그네슘 존재 하의 비스(1,10-페난트롤린) 구리(II)-도데실황산나트륨 용액의 전기화학)

  • Ko, Young Chun
    • Analytical Science and Technology
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    • v.20 no.6
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    • pp.483-487
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    • 2007
  • Electrochemistry of 1.0 mM bis(1,10-phenanthroline)copper(II) $(Cu(ph){_2}^{2+})$ in 100 mM NaCl solution including 27 mM $MgCl_2$ with and without sodium dodecyl sulfate (SDS) is studied. In the presence of SDS, $E_{pa}$ and $E_{1/2}$ of $Cu(ph){_2}^{2+}$ by adding $Mg^{2+}$ shifts to a positive direction compared to the SDS free. The intersection of two lines on ${\Delta}E_p$ vs -log[SDS] plot is determined as a critical micelle concentration (CMC). When $Mg^{2+}$ is added, it seems that the double layer became more compact. And the formation of micelles is retarded.

A Study on Crystalline Structural Variations of the Rigid Spherical-Tip scratch on the Surface of α-Titanium substrates via Molecular Dynamics Simulations (α-티타늄 평판표면에서 강체 구형팁의 스크래치로 인한 내부 결정구조 특성 변화에 대한 연구)

  • Yeri Jung;Jin Ho Kim;Taeil Yi
    • Tribology and Lubricants
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    • v.39 no.5
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    • pp.167-172
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    • 2023
  • Titanium alloys are widely recognized among engineering materials owing to their impressive mechanical properties, including high strength-to-weight ratios, fracture toughness, resistance to fatigue, and corrosion resistance. Consequently, applications involving titanium alloys are more susceptible to damage from unforeseen events, such as scratches. Nevertheless, the impact of microscopic damage remains an area that requires further investigation. This study delves into the microscopic wear behavior of α-titanium crystal structures when subjected to linear scratch-induced damage conditions, utilizing molecular dynamics simulations as the primary methodology. The configuration of crystal lattice structures plays a crucial role in influencing material properties such as slip, which pertains to the movement of dislocations within the crystal structure. The molecular dynamics technique surpasses the constraints of observing microscopic phenomena over brief intervals, such as sub-nano- or pico-second intervals. First, we demonstrate the localized transformation of lattice structures at the end of initialization, indentation, and wear processes. In addition, we obtain the exerted force on a rigid sphere during scratching under linear movement. Furthermore, we investigate the effect of the relaxation period between indentation and scratch deformation. Finally, we conduct a comparison study of nanoindentation between crystal and amorphous Ti substrates. Thus, this study reveals the underlying physics of the microscopic transformation of the α-titanium crystal structure under wear-like accidental events.

GRINDING OPTIMIZATION MODEL FOR NANOMETRIC SURFACE ROUGHNESS FOR ASPHERIC ASTRONOMICAL OPTICAL SURFACES (천체망원경용 비구면 반사경 표면조도 향상을 위한 최적연삭변수 수치결정모델)

  • Han, Jeong-Yeol;Kim, Sug-Whan;Kim, Geon-Hee;Han, In-Woo;Yang, Sun-Choel
    • Journal of Astronomy and Space Sciences
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    • v.22 no.1
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    • pp.13-20
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    • 2005
  • Bound abrasive grinding is used for the initial fabrication phase of the precision aspheric mirrors for both space and ground based astronomical telescopes. We developed a new grinding optimization process that determines the input grinding variables for the target surface roughness, checks the grinding error magnitude in resulting surface roughnesses, and minimizes the required machining time. Using the machining data collected from the previous grinding runs and subsequently fed into the multivariable regression engine, the process has the evolving controllability that suggests the optimum set of grinding variables for each target surface roughness. The process model was then used for ten grinding experiments that resulted in the grinding accuracy of $=-0.906{\pm}3.38(\sigma)\;nm(Ra)$ for the target surface roughnesses of Zerodur substrate ranging from 96.1 nm (Ra) to 65.0 nm (Ra) The results imply that the quantitative process optimization technique developed in this study minimizes the machining time and offers the nanometric surface roughness controllability superior to the traditional, qualitative, craftsman based grinding process for the astronomical optical surfaces.

Fabrication of ATO thin film for IR-cut off by sol-gel method (솔-젤 법에 의한 적외선 차단 ATO 박막 제조)

  • Kim, Jin-Ho;Lee, Kwang-Hee;Lee, Mi-Jai;Hwang, Jonghee;Lim, Tae-Young
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.23 no.5
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    • pp.230-234
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    • 2013
  • IR cut-off thin films consisted of ATO nanoparticles were successfully fabricated by sol-gel method. The coating solution was synthesized with organic/inorganic hybrid binder and ATO colloidal solution and ATO thin films were coated on a slide glass with the withdrawal speed of 5~40 mm/s. As the withdrawal speed increased from 5 mm/s to 40 mm/s, the thickness of coating thin films also increased from $1.05{\mu}m$ to $4.25{\mu}m$ and the IR cut-off in wavelength of 780~2500 nm increased from 49.5 % to 66.7 %. In addition, the pencil hardness of ATO thin films dried at $80^{\circ}C$ was ca. 5H and the coating films were not removed after a cross cutter tape test because of the hybrid binder synthesized with tetraethylorthosilicate and methyltrimethoxysilane. The surface morphologies, optical properties and film thickness of prepared thin films with a different withdrawal speed were measured by field emission scanning electron microscope (FE-SEM), UV-Vis spectrophotometer, and Dektak.