• Title/Summary/Keyword: 금속 실

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Studies on the Protease procuced by Streptomyces sp. (Streptomyces 속균이 생산하는 Pretense에 관한 연구)

  • 김광현;서정훈
    • Microbiology and Biotechnology Letters
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    • v.2 no.1
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    • pp.13-17
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    • 1974
  • A strain of Streptomyces sp. which producing a metal containing proteolytic enzyme was isolated from soil and some properties of this enzyme were investigated. The following results were obtained. 1. Optimal pH and temperature of this enzyme were pH7.0 and 37$^{\circ}C$ 2. This enzyme was easily inactivated with heat treatment: for example, by the treatmentat 37$^{\circ}C$ for 100 minutes the activity of the enzyme was decreased to about 50 per cent of intial actively but this enzyme was stable at neutral pH. 3. The activity of this enzyme was not inhibited by $Mg^{++}$, $_Mn^{++}$, $Ca^{++}$, Pb$^{++}$, or $Ba^{++}$ ect. but strongly inhibited by Hg$^{++}$, Co$^{++}$, Ag$^{+}$, Cu$^{++}$, or Cd$^{++}$. 4. This enzyme was strongly inhibited by EDTA but was not inhibited by oxalic acid, citric acid, 2, 4-dinitrophenol, $\varepsilon$-aminocaproic acid, cysteine, or thiourea.

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Protection Effects According to the Conditions of Installations of SPDs for Information-Oriented Equipments (정보화 기기용 SPD의 설치조건에 따른 보호효과)

  • Lee, Bok-Hee;Lee, Dong-Moon;Cheong, Dong-Chul;Lee, Su-Bong;Lee, Seung-Chil
    • Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.21 no.1
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    • pp.35-41
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    • 2007
  • Recently, there are increasing social needs for stable supply of electric power and securing high quality of information and communication services. In this work, to propose the effective protection countermeasures of information-oriented equipments against lightning surges, the protection effects of surge protective devices(SPDs) were experimentally investigated using actual-sized test circuits in various installation conditions. As a result, it was found that the protection effect of SPDs is quite different depending on the factors, such as the grounding system of power source, numbers of branch circuits, wiring method of grounding leads, and etc. In case of installing SPDs for information-oriented equipments, including all electric power lines and communication lines, the common grounding should be the most effective. Wiring method containing grounding leads with power lines in metal conduit is suitable to improve the surge cutoff performance of SPDs.

A Study of Ultrasonic concentrator with Rotating parablic surace (회전 기물면을 이용한 초음파 집속기에 관한 연구)

  • 김주홍;전병실
    • Journal of the Korean Institute of Telematics and Electronics
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    • v.11 no.1
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    • pp.1-7
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    • 1974
  • This paper discribes the reflector type ultrasonic concentrator which makes hghintencity of ultrasonic field. This was made by rotating parabolic surface which only using total reflection aria, that makes boundary by the critical angle of reflection of sound. I made two binds of concentrator acording to the type of ultrasonic transduser: one is internal surface reflector type concentrator, which is available for disc type transducer, and the other is external surface reflector type concentrator which is available cylinderical transduser. In the mony aspects the reflector tripe concentrator is supel'ier to the reflection type concentrator as plastics lens; It is more durable in high temperature and high intencity ultrasonicfield then refrector type concentrator because of it is made by glass or metal, and it has higher. efficiency because of it wasts made by only total reflection aria that is without absoption lose. I think this is useful ultrasonic concentrator in mony industrial field, in which high intencitr of ultrasonic energy was used.

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수십 MeV 양성자빔을 이용한 금속나노입자 제조 기술 및 장치

  • Kim, Gye-Ryeong;Jeong, Myeong-Hwan;Na, Se-Jin
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.02a
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    • pp.493-494
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    • 2011
  • 수 MeV~수십 MeV 양성자빔을 이용해 백금, 은 등의 나노입자 제조실험을 수행하였다. 나노 입자는 의료분야와 산업 분야에서 그 응용성이 다양해 여러 지 방법을 이용한 제조기술이 개발되고 있다. 전자빔, 감마선, 양성자빔 등의 방사선을 이용한 나노입자 제조방법은 가장 널리 이용되고 있는 화학적 제조방법에 비해 비교적 공정이 단순하다는 장점을 가지고 있지만 공정 변수의 제어방법이 확립되어 있지 않아 이에 대한 연구가 필요한 실정이다. 특히, 양성자빔의 경우 에너지에 따른 투과깊이의 조절과 플럭스나 총 선량, LET (Linear Energy Transfer) 등의 변수와 제조된 나노입자의 상관관계 등에 대한 연구가 선행되어야 한다. 본 논문에서는 백금산 용액을 이용한 나노입자 제조 결과와 대면적 양성자빔을 이용하기 위한 초음파 이용 나노입자제조장치의 제작 및 실험결과에 대해 논하고 향후 건설될 100MeV 선형 양성자가속장치의 나노입자 제조실험에의 응용을 위한 이용시설을 소개하고자 한다. 나노입자 제조실험은 한국원자력의학원의 MC-50 싸이클로트론을 이용하여 수행하였으며, 가속기로부터 인출되는 에너지는 35, 45MeV, 빔전류는 수십 nA~수${\mu}A$의 범위 내에서 조절하였다. 제조된 나노입자는 TEM을 이용하여 그 크기와 분포를 관찰하였다. 대면적의 양성자빔을 이용하는 경우, 수mm의 두께와 수십 cm의 직경을 가지는 원반 모양의 시료용기를 사용하여 양성자빔의 에너지와 선량을 정확히 조절할 수 있게 되는데 이 때 용기 내 시료와 양성자빔간의 균일한 반응을 위해 용액을 적절하게 섞어 주어야만 한다. 이러한 목적으로 초음파를 이용하여 나노입자 제조장치를 제작하여 실험을 수행하였다. 나노입자 제조는 현재 교과부의 지원으로 경주 건천지역에 건설되고 있는 100MeV 선형양성자가속기의 주요 이용 분야 중의 하나로 20MeV 빔라인 중 한 개의 빔라인과 표적실을 나노입자 제조 등의 실험을 위한 시설로 구축 중이다. 최대 평균전류 1.6mA 까지 가능하고 펄스폭은 0.05~1.33 msec까지 조절가능하도록 개발되고 있다.

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Modeling the Heterogeneous Microstructures of Ti-MMCs in Consolidation Process (강화공정에 따른 비균질 티타늄 금속기 복합재료 모델링)

  • Lee Soo-Yeun;Kim Tae-Won
    • Composites Research
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    • v.18 no.3
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    • pp.21-30
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    • 2005
  • Vacuum hot pressing has been used for the development of titanium metal matrix composites using foil-fiber-foil method. Heterogeneous microstructures prior to and following consolidation have been quantified, and the relations to densification behavior investigated. As shown by the results, dramatic variations of the microstructures including equiaxed $\alpha$, transformed $\beta$ and $ Widmanst\ddot{a}tten$ $\alpha$ are obtained during the process according to the fiber distributions. The dependence of microstructures on the consolidation then has been explained in terms of the change in mechanisms such as grain growth and recrystallization that occur with changing levels of inhomogeneity of deformation. Further, micro-mechanics based constitutive model enabling the evolution of density over time together with the evolutions of microstructure to be predicted has been developed. The mode developed is then implemented into finite element scheme so that practical process simulation has been carried out.

Metal-Dinitrosyl Complexes(Ⅳ) : Synthesis and Characterization of Symmetric and Asymmetric Dinuclear Molybdenum and Tungsten Complexes (금속-디니트로실 착물 (제 4 보) : 몰리브덴과 텅스텐의 대칭 및 비대칭 이핵 착물의 합성과 특성)

  • O, Sang O;Mo, Seong Jong
    • Journal of the Korean Chemical Society
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    • v.38 no.7
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    • pp.485-495
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    • 1994
  • Several new symmetric and asymmetric homo and hetero dinuclear complexes of the type $[Cl(dppp)(NO)_2M({\mu}-pyz)M'(NO)_2(dppp)Cl][ClO_4]_2$ and $[Cl(phen)(NO)_2M({\mu}-pyz)M'(NO)_2(dppp)Cl][ClO_4]_2$(M,M'= Mo or W; phen = 1,10-phenanthroline; dppp = 1,3-bis(diphenylphosphino)propane; pyz = 1,4-pyrazine) were synthesized in three-steps starting from $[M(NO)_2Cl_2]_n(M = Mo, W)$. The final products were purified by eluting it through silica gel column ($2{\times}20$ cm) with acetone as the eluent. Characterization of these complexes and some related complexes was accomplished through UV-vis., $^1H$-NMR, $^{13}C$-NMR and IR spectroscopies as well as elemental analysis. The infrared spectra indicate that the NO groups occupy cis-positions of the octahedral. The $^1H$ and $^{13}C-NMR$ data for the new compounds revealed a dimeric structures with bridged pyz.

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Phosphoprotein Partitioning in Metal-Affinity Aqueous Two-Phase Systems and Prediction of Partitioning Behavior (금속 친화성 액 이상분계 시스템에서 Phsphoprotein분배 및 분배예측)

  • 정봉현
    • KSBB Journal
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    • v.9 no.3
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    • pp.279-286
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    • 1994
  • A mathematical model has been derived and used to describe phosphoprotein partitioning in Fe(III) IDA-PEG/dextran two-phase systems. This model includes the inhibitory effects of hydrogen and hydroxyl ion concentrations on protein partitioning. For aqueous two-phase partitioning experiments, the Al and A2 subcomponents of ovalbumin carrying two and one surface phosphoryl group(s) were purified using an immobilized metal ion affinity chromatography (IMAC). The ratio of partition coefficients in the presence and absence of Fe(III)IDA-PEG, K/Ko, increased in the pH range of 3.0 to 5.0 due to deprotonation of the second oxygen of the phosphoryl group, and above pH 5.0 declined steeply by the inhibitory binding of hydroxyl ions to the metal ion. This partitioning behavior was well described by the mathematical model. The binding constants for formation of the complex between the phosphoryl group and the Fe(III)IDA-PEG were found to be $6.1{\times}10^3M^{-1} and 2.3{\times}10^4M^{-1}$ in the top and bottom phases, respectively. These values are 3-5 times those for interaction of Cu(II)IDA-PEG with a single surface-accessible histidine.

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Optical Diagnostic Study for Flame Characteristic Analysis in Aluminum Dust Clouds (알루미늄 군입자 화염특성 분석을 위한 광학기법 연구)

  • Lee, Sanghyup;Ko, Taeho;Lim, Jihwan;Lee, Dohyung;Yoon, Woongsup
    • Journal of the Korean Society of Propulsion Engineers
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    • v.17 no.5
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    • pp.47-53
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    • 2013
  • In this study, In order to develop the measurement method of high energy density metal aluminum dust cloud combustion, flame temperature and emission spectrum was measured using spectrometer. Because of the ultra high ${\mu}m$-sized aluminum flame temperature more than 2400 K, it was measured by non-contact optical technique which is the modified two wavelength pyrometry with 520, 640 nm and spectrum comparison method. These methods were applied to experiment after accurate verification. As a result, we could identify that flame temperature is more than 2400 K in bottom of combustor in both methods. And on the emission spectrum analysis, we could measure AlO radical which is occurred dominantly in aluminum combustion.

Effects of Crud on reflood heat transfer in Nuclear Power Plant (핵연료 크러드가 원전 재관수 열전달에 미치는 영향)

  • Yoo, Jin;Kim, Byoung Jae
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.22 no.5
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    • pp.554-560
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    • 2021
  • CRUD (chalk river unidentified deposits) is a porous material deposited on the surface of nuclear fuel during nuclear power plant operation. The CRUD is composed of metal oxides, such as iron, nickel, and chromium. It is essential to investigate the effects of the CRUD layer on the wall heat transfer between the nuclear fuel surface and the coolant in the event of a nuclear accident. CRUD only negatively affects the temperature of the nuclear fuel due to heat resistance because the effects of the CRUD layer on two-phase boiling heat transfer are not considered. In this study, the physical property models for the porous CRUD layer were developed and implemented into the SPACE code. The effects of boiling heat transfer models on the peak cladding temperature and quenching were investigated by simulating a reflood experiment. The calculation results showed some positive effects of the CRUD layer.

Characteristics of Excimer Laser-Annealed Polycrystalline Silicon on Polymer layers (폴리머 위에 엑시머 레이저 방법으로 결정화된 다결정 실리콘의 특성)

  • Kim, Kyoung-Bo;Lee, Jongpil;Kim, Moojin;Min, Youngsil
    • Journal of Convergence for Information Technology
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    • v.9 no.3
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    • pp.75-81
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    • 2019
  • In this work, we investigated a low temperature polycrystalline silicon (LTPS) thin film transistors fabrication process on polymer layers. Dehydrogenation and activation processes were performed by a furnace annealing at a temperature of $430^{\circ}C$ for 2 hr. The crystallization of amorphous silicon films was formed by excimer laser annealing (ELA) method. The p-type device performance, fabricated by polycrystalline silicon (poly-Si) films, shows a very good performance with field effect mobility of $77cm^2/V{\cdot}s$ and on/off ratio current ratio > $10^7$. We believe that the poly-Si formed by a LTPS process may be well suited for fabrication of poly-Si TFTs for bendable panel displays such as AMOLED that require circuit integration.