• Proceedings of the Korean Institute of Communication Sciences Conference
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• 1995.06a
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• pp.269-272
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• 1995

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2008.11a
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• pp.168-168
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• 2008

고체산화물 연료전지의 전해질로 사용되는 상용의 YSZ powder는 나노 크기의 입자로서 습식 후막 성형을 위한 분산공정에 많은 문제를 가지고 있다. 기존 tape casting을 이용한 후막 공정의 경우 수 micron 대역의 powder가 주로 사용되었고 MLCC 공정에서 sub micron 크기의 입자가 상용으로 적용되는 수준에 있다. 그러므로 아직 후막 공정이 확립되지 않은 YSZ의 경우 수십 nano 크기 powder의 분산과 casting에 관한 연구 결과 보고는 아직 미흡하다. 본 연구에서는 이러한 연구 필요성에 따라 수십 nano의 입자크기를 나타내는 YSZ 입자의 고농도 분산 조건을 위한 분산제와 용매 량에 대한 기본적인 실험 결과를 제시하고자 하였다. 그리고 이 결과에 기초하여 기존 tape casting 공정에서 사용되는 유기 binder system을 이용하여 후막의 casting 조건 및 sheet의 균일성 확보 조건을 확인 하고자 하였다.

• Proceedings of the KIPE Conference
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• 2017.07a
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• pp.485-486
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• 2017

본 논문에서는 10m 반경의 공간에 위치한 웨어러블 기기를 충전하기 위한 무선 전력전송을 제안한다. 장거리 무선전력전송의 송신코일 양단의 높은 전압문제를 해결하기 위해 공진 커패시터를 분산하여 각 코일의 유기전압을 줄이는 분산권선형 다이폴 코일을 제안하였다. FEM 시뮬레이션 결과, 분산권선형 다이폴 코일이 형성한 자속밀도의 균일도는 최소 71%로 집중권선형 다이폴 코일의 최소 51%보다 높았다. 또한 거리별 최고 자속밀도는 분산권선형 다이폴 코일이 낮았지만 거리가 멀어질수록 차이는 줄어들어 5m 거리 이후에서의 차이는 30 % 이내임을 확인하였다. 시뮬레이션 설계를 바탕으로 분산권선형 다이폴 송신코일과 4가지의 다른 형태를 갖는 수신 코일을 제작하여 10m 거리 이내에서 10 mW 이상의 전력을 전송하였다.

• Korean Journal of Food Science and Technology
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• v.38 no.6
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• pp.767-772
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• 2006

In this study, we sought to produce a double layer microcapsule containing Lactobacillus sp. as the core material. The conditions for this microencapsulation process were optimized for the formation of a microcapsule with high storage stability. The effects of the ratio of[core material] to [wall material], the type and concentration of emulsifier used, the stirring rate(dispersibility) and the temperature of the dispersion fluid on the microencapsulation yield were studied. The optimal concentration and type of emulsifier required in order to allow for the stable formation of a W/O type emulsion (a primary process in double layer microencapsulation) were 1.00% (w/w) and polyglycerol polyricinileate (PGPR, HLB 0.6). However, the optimal concentration and type of emulsifier required to construct a W/O/W type emulsion (a secondary process in double layer microencapsulation), were 0.65% (w/w) and polyoxyethylene sorbitan monolaurate (PSML, HLB 16.7). Finally, we obtained a maximum yield of microencapsulation with a dispersion fluid stirring rate of 270rpm and a dispersion fluid temperature of 10$^{\circ}C$ after spraying a W/O/W type emulsion into the dispersion fluid.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.30 no.3
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• pp.91-95
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• 2020

In this study, we report a hydrothermal synthesis in which BaTiO₃ nanoparticles (NPs) with enhanced size uniformity and dispersibility are synthesized by increased time and temperature, increasing nucleation and diffusion rates. The formation process of an uniform size of 20 nm BaTiO₃ NPs, which has not been extensively researched, was optimized through hydrothermal synthesis at 180℃. Simultaneous increase in the nucleation rate of TiO₂ and diffusion length of Ba²⁺ ions, resulting from a higher temperature, allowed for the synthesis of BaTiO₃ NPs (20 nm) with significantly enhanced size-uniformity. The size and crystallinity of BaTiO₃ NPs which exhibit excellent dispersibility in hexane solvent were investigated using transmission electron microscopy and X-ray diffraction. The results presented herein provide insights into improving the size uniformity and dispersibility of BaTiO₃ NPs by hydrothermal synthesis for applications to variety of electronic devices.

• Journal of the Korea Society for Simulation
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• v.28 no.3
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• pp.83-89
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• 2019

This research describes quantitative effects of initial dispersion conditions upon the dispersion randomness of Magnus rotor bomblets. Ratios of the missile spin rate to the missile velocity, a, flight path angles, ${\gamma}$ and altitudes, h, were changed to investigate their effects on dispersion randomness. Dispersion was analyzed through calculation of 6 degree of freedom motion equation with aerodynamic coefficients from wind tunnel experiments. In order to analyze the randomness, regression analysis is adopted to calculate the coefficient of determination. The optimized ratio of the missile spin rate to the missile velocity and flight path angle were obtained and the dispersion altitudes had more effect on the dispersion diameter and had less effect on dispersion than other parameters.

• Applied Chemistry for Engineering
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• v.9 no.6
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• pp.846-851
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• 1998

An experimental research on the preparation of zinc oxide fine particles in w/o emulsions was conducted. Precipitation solutions were zinc nitrate aqueous solutions with hexamethylenetetramine(HMTA) as precipitant. The precipitation solutions formed stable w/o emulsions with kerosine in the presence of Span 80. Homogeneous precipitation reaction occurred in the w/o emulsion after the resultant w/o emulsion was heated above the decomposition temperature of HMTA and zinc oxide particles were precipitated. In some case, zinc oxide particles of bi-modal distribution were obtained. However, zinc oxide fine particles of narrow particle size distribution could be obtained, even when the initial zinc concentration of precipitation solution and the conversion to zinc oxide are both higher that those in bulk homogeneous precipitation.

• Journal of the Korean Data and Information Science Society
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• v.17 no.3
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• pp.707-716
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• 2006

When the regression function is discontinuous at a point, the variance function is usually discontinuous at the point. In this case, we had better propose a test for the existence of a discontinuity point with the regression function rather than the variance function. In this paper we consider that the variance function only has a discontinuity point. We propose a nonparametric test for the existence of a discontinuity point with the second moment function since the variance function and the second moment function have the same location and jump size of the discontinuity point. The proposed method is based on the asymptotic distribution of the estimated jump size.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.18 no.2
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• pp.711-718
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• 2017

Silver nanoparticles were attached by chemical reduction after synthesizing a porous PVK-CTA complex. The PVK-CTA complex was synthesized by polymerizing N-vinylcarbazole in a CTA-chloroform solution using iron(III) chloride as an oxidizing agent and a honeycomb-pattern with uniformly formed macropores was formed by applying steam to the complex surface soaked with a volatile solvent under humid conditions. Using TTF as a reducing agent and PVP as a dispersant, silver nanoparticles were attached on the Honeycomb-pattern complex surface through chemical reduction. The formation of the complex was confirmed by FT-IR and UV-Vis spectrometry, and the degree of thermal decomposition of the complexes was analyzed after N-vinylcarbazole was polymerized by varying its concentration. The uniformity of the pores on the composite surface and the dispersibility of the attached silver nanoparticles were investigated by SEM. The dispersibility of the silver nanoparticles was also analyzed by varying the concentrations of reducing agent and dispersant and precursor.

• Proceedings of the Korean Vacuum Society Conference
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• 2006.02a
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• pp.129-129
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• 2006