• Journal of the Korean Ceramic Society
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• v.41 no.9
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• pp.663-669
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• 2004

Mullite and cordierite, which were stable oxides having excellent thermal and chemical characteristics, were widely used as an engineering and electronic materials. However, thermal shock resistance of the mullite was detriorated, and strength of the cordierite was also reduced at high temperatures. The mullite-cordierite composite powders were synthesized for solving these problems in this study. The mullite-cordierite composite powders were manufactured by the solution-polymerization method using mixtures of fused silica, aluminium nitrate, magnesium nitrate, and PVA. Crystallinity, phase formation, density, and surface area of the synthesis powders were characteristics. Fine mullite-cordlerite composite powders were successfully synthesized at 1300$^{\circ}C$ and their surface areas were about 20㎡/g after planetary milling for 1h. With increasing the milling time, surface area increased to 23 ㎡/g for 4h ana 24㎡/g for 8h.

• Korean Journal of Materials Research
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• v.5 no.7
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• pp.786-793
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• 1995

Ag-doped $Y_1$Ba$_2$Cu$_3$O$_{7-y}$ samples have been prepared by solid state reaction. High-Tc super conductivity, microstructure and mechanical property of the Ag-doped $Y_1$Ba$_2$Cu$_3$O$_{7-y}$ samples have been studied. As the Ag content increased, the grain size of $Y_1$Ba$_2$Cu$_3$O$_{7-y}$, increased and connectivity between the grains was improved, and the sample becomed denser and harder than the undoped. From the result, it is concluded that Ag addition reduced weak link and weak coupling between grains and led to the strong coupling. Furthermore, the anisotropy of crytstal structure was decreased and thermal stability, mechanical property of $Y_1$Ba$_2$Cu$_3$O$_{7-y}$-Ag were improved.mproved.

• Fire Science and Engineering
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• v.21 no.2 s.66
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• pp.54-63
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• 2007

Concrete is generally accepted to have good inherent fire resistance. It mainly relies on the assumption that concrete has low heat-transfer characteristic and spatting does not occur during the course of a fire. However, the significant numbers of fire accidents have shown in recent years that incidence of spatting has caused sever damages to many structures. This review has systematically investigated the behaviour of concrete in fire, including phenomenon of spatting, with respect to the theorical consideration and experimental results. Explosive spatting is caused by the build-up of water vapor pressure in concrete subjected to increasing temperatures. When this pressure exceeds the tensile strength of the concrete over a fire-exposed area, explosive spatting can result in a typical temperature range between $200^{\circ}C\;and\;400^{\circ}C$. The major functions are known to be moisture content, pore pressure, load ratio, and heating regime.

• Proceedings of the Materials Research Society of Korea Conference
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• 2009.05a
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• pp.42.1-42.1
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• 2009

오스테나이트 스테인리스강은 우수한 내식성 및 기계적 특성으로 인해 구조용 재료로 널리 사용되고 있다. 표준원전 경수로의 경우 가압기 밀림관소재로 Nb 안정화 오스테나이트 스테인리스강인 type 347 스테인리스강이 사용되고 있다. 그러나 원전배관에서는 운전중 배관내 온도편차에 의한 열응역과 하중변화에 의한 기계적하중에 의해 피로손상을 받는다. 일반적으로 범용 오스테나이트 스테인리스강(AISI 304, 316)의 피로균열 성장거동에 대한 연구결과는 국내외적으로 다수 축적되어 있으나 type 347 탄소, 질소 함량에 따른 기계적 특성 및 피로균열성장 연구는 매우 미비하다. 따라서 본 연구에서는 탄소와 질소의 함량에 따른 기계적거동을 평가하고, 이에 따른 피로균열전파속도를 관찰하여 스테인리스강의 정확한 피로균열전파속도 곡선을 제시하고자 한다. 실험에 사용된 시편은 두께 5mm, 폭 25.4mm CT시편을 사용하였으며, 1mm의 예비균열을 주었다. 그리고 실험온도는 상온과 원전가동온도인 $316^{\circ}C$에서 실시하였으며, 주파수는 10Hz를 주었다. 실험결과 각 함량에 따른 type 347의 미세조직 관찰결과 기지내에 압연방향을 따라 조대한 석출물의 흐름이 관찰되었으며, 크기나 분포가 큰 차이를 보였다. C+N 함량이 낮은 시편은 주로 $0.1\;{\mu}m$ 이하의 미세한 입자들이 오스테나이트 기지조직의 입내와 입계에 고르게 분포되어 있었다. 그러나 C+N 함량이 높은 시편의 경우에는 $0.1\;{\mu}m$ 이하의 미세한 입자들과 함께 국부적으로 $1\sim10\;{\mu}m$의 조대한 입자들이 분포하고 있는 것이 관찰되었다. 그리고 질소의 함량이 높아짐에 따라 인장강도는 증가하였으며, 피로시험결과 고온에서 실험한 피로균열성장률 곡선이 상온보다 높게 나타남을 확인할 수 있었다. 그리고 질소가 적게 첨가되고 탄소의 함량이 많을수록 피로균열성장률은 ASME 곡선보다 낮게 나타났다.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.33 no.3
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• pp.107-113
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• 2005

A calorimeter of 2-ton thrust level rocket engine chamber has been developed to measure the wall heat flux. The liner of the chamber is made of copper-chromium alloy to maximize the heat transfer performance and structural strength. 1-D design code based on empirical correlations has been used for the prediction of the global thermal characteristics while 3-D CFD has been applied for the verification of local cooling performance. The predicted average wall heat flux at the throat is 43 $MW/m^{2}$ for the combustion chamber pressure of 53 bar. The chamber structure is confirmed to be safe at the pressure of 150 bar through 2-D stress analysis and measurement of the strain of the test species. Finally, the test of pressurizing the calorimeter chamber has been performed with water at the pressure of 150 bar in room temperature environment. No thermal damage has been detected after the hot-fire test in the test nozzle of same cooling performance with the developed calorimeter though the measured throat heat flux is higher than the design value by 10%.

• Composites Research
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• v.36 no.3
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• pp.193-198
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• 2023

Currently, there are many discussions about composite materials and 3D printed composite material to weight reduction of ships. A test was conducted to confirm the applicability of the 3D printed composite material to ships and offshore structures by linking the 3D printing technology with excellent productivity and the composite material with corrosion resistance and lightweight characteristics in salt water environments. In order to apply the 3D printed composite material used in this paper to ships and offshore structures, the temperature environmental effects that can be exposed in the marine environment should be considered. Therefore, the tensile test was conducted with specimen of Carbon + Onyx, Carbon + Nylon, HSHT glass + Onyx, HSHT glass + Nylon material in low temperature (-50℃), room temperature (20℃), and high temperature (50℃) environments that can be exposed to the marine environment. As a result of the tensile test, the carbon + onyx specimen showed the highest tensile strength and the HSHT glass + onyx specimen showed the highest tensile strain. In addition, by analyzing the tested specimens, the failure mode of the 3D printed composite material specimens exposed to various temperature environments was analyzed.

• Journal of the Korean Recycled Construction Resources Institute
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• v.4 no.4
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• pp.418-424
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• 2016

This study is an experimental study on the recycling of bottom ash in coal ash discharged from a thermal power plant. Bottom ash has limited research on recycling because it has more porous and higher water absorption ratio than fly ash. In this paper, the bottom ash was pulverized to a specific surface area of $4,000cm^2/g$ in order to use as a binder, and the flow, compressive strength test and microstructure analysis of the bottom ash based geopolymer mortar were performed. The flow measurement results of the geopolymer mortar showed that the flow rate was improved by increasing mixing water as the molar concentration of activator was increased. Compressive strength increased with increasing curing temperature and molar concentration. Through the microstructure analysis, we could confirm the geopolymer gel produced by the reaction of the condensation polymerization. It is considered that it is possible to make the bottom ash based geopolymer concrete through proper molar concentration of activator and high temperature curing.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.18 no.4
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• pp.111-117
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• 2017

This study examined the material properties of Korean rice husk ash (RHA) according to the manufacturing process, and evaluated the feasibility of its use as a new admixture for high strength concrete. For this purpose, its particle size distribution, chemical composition, and microstructure were analyzed under various parameters, such as calcination temperature ($400^{\circ}C$, $650^{\circ}C$, and $900^{\circ}C$) and the inclusion of a milling process. X-ray fluorescence analysis confirmed that the silicon oxide ($SiO_2$) content of RHA was improved to more than 92% with a calcination process at $650^{\circ}C$ or higher. In addition, microstructural analysis showed that the RHA calcined at $650^{\circ}C$ has a porous structure. Because of this, the absorption capacity of the RHA was improved. On the other hand, when the milling process was applied, the porous structure was destroyed; thus, the absorption capacity tended to decrease further. Based on the analysis results, it was concluded that RHA calcined at $650^{\circ}C$ can be used as an admixture for high strength concrete, which possesses functions of both a shrinkage reducing agent and a pozzolanic activator.

• Journal of the Microelectronics and Packaging Society
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• v.28 no.2
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• pp.71-79
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• 2021

In this study, we have successfully fabricated the Sn-Ni paste and evaluated the bonding properties for high-temperature endurable EV (Electric Vehicle) power module applications. From evaluating of the micro-structural changes in the TLPS (Transient Liquid Phase Sintering) joints with Sn and Ni contents in the Sn-Ni pastes, a lack of Ni powders and Ni particle agglomerations by Ni surplus were observed in the Sn-20Ni and Sn-50Ni joints (in wt.%), respectively. In contrast, relatively dense microstructures are observed in the Sn-30Ni and Sn-40Ni TLPS joints. From differential scanning calorimetry (DSC) thermal analysis results of the fabricated Sn-Ni paste and TLPS bonded joints, we confirmed that the complete reactions of Sn with Ni to form Ni-Sn intermetallic compounds (IMCs) at bonding temperatures occurred, and there is no remaining Sn in the joints after TLPS bonding. In addition, the interfacial reactions and IMC phase changes of the Sn-30Ni joints under various bonding temperatures were reported, and their mechanical shear strength were investigated. The TLPS bonded joints were mainly composed of residual Ni particles and Ni₃Sn₄ intermetallic phase. The average shear strength tended to increase with increasing bonding temperature. Our results indicated a high shear strength value of approximately 30 MPa at a bonding temperature of 270 ℃ and a bonding time of 30 min.

• The Journal of Korea Institute of Information, Electronics, and Communication Technology
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• v.10 no.6
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• pp.487-495
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• 2017

The thermal characteristics of the electrodeless lamp are one of the main factors that determine the design and performance of the lamp. The coupler changes the impedance characteristic by heat and its use temperature is usually within about $150^{\circ}C$. In this study, we observed the phenomenon when the coupler was exposed at a temperature of $150^{\circ}C$ or higher, which has not been discussed so far. Two types of coupler A and coupler B with different spacing between the inner tube and the coupler were analyzed for electrical, thermal and optical properties and deterioration characteristics with different heat and heat shielding conditions. First, the impedance of the system is obtained and used as a criterion for analyzing the electrical characteristics through it. The diameters of the two types of couplers are 1 mm, and the experimental result shows that the coupler diameter is 1 mm, which can cancel out the loss of the magnetic field strength. Therefore, based on these results, when the coupler is exposed to high temperature of about $200^{\circ}C$, the efficient design method corresponding thereto is proposed.