• Journal of the Korean Society for Nondestructive Testing
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• v.25 no.5
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• pp.377-383
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• 2005

Because explosive fluid is used at high temperature or under high pressure in petrochemistry and refined oil equipment, the interest about safety of equipments is intensive. Specially, the safety of high pressure reactor vessel is required among them. The material selected in this study is 2.25Cr-1Mo steel that is widely used for high pressure reactor vessel material of petrochemical plant. Eight kinds of artificially aged specimens were prepared by differing from aging periods under three different temperatures. The material was iso-thermally heat treated at higher temperatures than $391^{\circ}C$ that is the operating temperature of high pressure reactor vessel. Vickers hardness properties and electrical resistivity properties about artificially aged material as well as un-aged material were measured, and master curves were made out from the correlation with larson-Miller parameter. And electrical resistivity properties as well as Victors hardness properties measured at high pressure reactor vessel of the field were compared with master curves made out in a laboratory. Degradation evaluation possibility in the field of high pressure reactor vessel by using electrical resistivity method was examined. Electrical resistivity property measured in the field is similar with that of artificially aged material in similar aging level.

• Korean Journal of Food Science and Technology
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• v.47 no.2
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• pp.198-203
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• 2015

This study was performed to evaluate changes in the chemical composition of germinated rough rice with high hydrostatic pressure treatment (HPT). Rough rice was germinated at $37^{\circ}C$ over 6 days (control), and then subjected to HPT at 30 MPa for 24 h. The highest crude protein content was 9.54% in the control sample after 6 days of germination. Crude lipid content increased from 2.04-2.74% (control) to 2.27-3.10% (HPT). HPT samples showed higher values of total free sugar and glucose content than those of the control. The total amino acid value was not significant, but the essential amino acid content increased from 0.45-5.09 mg/g in the control to 1.57-5.30 mg/g in the HPT sample. The major fatty acids were found to be palmitic, oleic, and linoleic acid. The content of oleic acid decreases with HPT, whereas that of linoleic and linolenic acid increased slightly during the initial stages of germination. These results suggest that HPT after germination efficiently depolymerizes chemical components and enhances the content of essential nutrients.

• Journal of the Korean Chemical Society
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• v.38 no.6
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• pp.411-417
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• 1994

For the analysis of fine ceramics, which is one of the new materials difficult to be dissolved, the methods of sample pretreatments such as alkali fusion and high pressure acid digestion were studied using inductively coupled plasma-atomic emission spectrometer(ICP-AES). For the Al2O3 powder sample, the results from high pressure acid digestion method showed better reproducibility than those obtained by alkali fusion technique. In the case of the analysis of SiC powder using the former method, impurities of the powder in the range of ppm were determined without matrix interference by removing Si as Si-F volatilization. Japan Certified Reference Materials (JCRM022 and JCRM023) were analyzed by this method for ultra fine powder and the results showed high accuracy and good reproducibility.

• The monthly packaging world
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• s.274
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• pp.44-53
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• 2016

• Journal of the Korean Chemical Society
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• v.28 no.2
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• pp.143-146
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• 1984

• Journal of the Korean Chemical Society
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• v.49 no.6
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• pp.554-559
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• 2005

• Journal of the Korean Institute of Gas
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• v.22 no.5
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• pp.100-106
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• 2018

pressure buried pipes in domestic industrial estate have many long-term use pipes, Toxic, flammable, Inflammable, etc. as well as a variety of toxic chemicals are embedded in a complex be buried, A high level of safety management is required as it can damage other pipes installed nearby in the event of accidents such as various external interference. Therefore, in this study, the safety management practices of high-pressure gas distribution and urban gas distribution are utilized to derive efficient safety management methods for high-pressure gas installation piping through in-depth comparative analysis.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 1998.04a
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• pp.19-19
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• 1998

최근 화학, 연소, 동력, 제철 등의 각종 플랜트에서 조업압력이 고압화되어 가고 있으며, 이에 수반하여 배관계를 통하는 고압가스 유동에 관한 연구가 활발하게 진행되고 있다. 배관계를 통하는 고압가스의 유동에 있어서 유량의 적절한 제어, 유동에 의하여 야기되는 배관계의 소음·진동, 그리고 배기가스의 적절한 처리법 등은 공학적으로 매우 중요한 문제로 알려져 왔다. 일반적으로 정상운전을 하는 플랜트에서 고압 배기가스의 문제는 배기가스 Expander에 의하여 에너지를 회수하는 방법이 생각될 수 있으나, 실제 공업현장에서는 배기가스를 안전하고, 또 소음·진동을 발생시키지 않도록 적절하게 처리하는 것이 매우 중요한 기술적 과제로 남아 있다. 일반적으로 배기가스의 압력이 임계압력(critical pressure) 이상으로 되는 경우(실제 대부분의 플랜트에서 배기가스의 압력은 임계압력보다 매우 높다), 배관계 내부에서 충격파(shock-wave)가 발생하여 난류와동 혹은 난류경계층과 간섭하게 됨으로써 강력한 공기역학적 소음이나 진동을 발생시키게 된다. 이와 같은 소음·진동에 대한 대책으로는 현재 가스배출부에 감압밸브를 직렬로 설치하거나, 유로에 다공판(porous plates)들을 삽입하여 감압과정을 공간적으로 분산시킴으로써, 충격파가 발생하지 않도록 하는 방법을 주로 채택하고 있다. 그러나 이러한 방법을 적용하는 경우 배기가스 유동에 대한 유량의 제어기능이 저하되는 문제가 발생한다.

• The Safety technology
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• no.146
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• pp.18-19
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• 2010

전남 여수시 화치동에 위치한 금호석유화학(주) 여수정밀화학에 안전관리자로 근무하고 있는 이재섭 과장은 이곳의 총체적 안전관리를 위해 방화관리자, 고압가스안전관리책임자, 냉동안전관리책임자, 위험물안전관리자 등 사업장 전반적인 분야에서 중요한 역할을 다하고 있다. 24년 반평생 안전과 함께 걸어온 그는 이제 그 동안 쌓아온 경험과 지식을 전하고자 후학 양성이라는 새로운 목표로 제2의 도약기를 준비하고 있다.

• Korean Chemical Engineering Research
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• v.62 no.2
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• pp.163-172
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• 2024

In this study, two different scenarios for ammonia liquefaction in the green ammonia manufacturing process were proposed, and the economic-feasibility and environmental impact of each scenario were analyzed. The two liquefaction processes involved gas-liquid separation before cooling at high pressure (high pressure cooling process) or after decompression without the gas-liquid separation (low pressure cooling process). The high-pressure cooling process requires higher capital costs due to the required installation of separation units and heat exchangers, but it offers relatively lower total utility costs of 91.03 $/hr and a reduced duty of 2.81 Gcal/hr. In contrast, although the low-pressure cooling process is simpler and cost-effective, it may encounter operational instability due to rapid pressure drops in the system. Environmental impact assessment revealed that the high-pressure cooling process is more environmentally friendly than the low-pressure cooling process, with an emission factor of 0.83 tCO₂eq less than the low-pressure cooling process, calculated based on power usage. Consequently, the outcomes of this study provide relevant scenario and a database for green ammonia synthesis process adaptable to various process conditions.