• Polymer(Korea)
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• v.26 no.6
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• pp.718-727
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• 2002

In this work, an Ar+ beam was irradiated on carbon fiber surfaces to improve the interfacial shear strength (IFSS) of the resulting composites using an ion assisted reaction (IAR) method h single fiber pull-out test was executed to investigate the basic characteristics of the single Carbon fiber/matrix interface. Based on Greszczuk's geometrical model, the debonding force for pull-out of the fiber from the resins was discussed with the applied ion beam energy as a result, it was known that an ion beam treatment produced the functional groups on fiber surface and etching lines along the fiber axis direction, resulting in increasing the adhesion forces between fibers and matrix, which caused the improvement of the IFSS in a composite system. And, it was also found that the maximum IFSS was shown at 0.8 keV ion beam energy in this system.

• The korean journal of orthodontics
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• v.28 no.4 s.69
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• pp.641-657
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• 1998

This study was undertaken to compare the bond strength and the fracture site of new and recycled brackets according to the base design. 252 sound premolars extracted for orthodontic treatment were collected and Type I, Type II, Type III brackets were divided into four groups by recycling method Each bracket was then bonded to an extracted premolar. Instron Universal Testing Machine(model W) was used to measure the shear bond strength, and the surface of the recycled brackets were viewed in SEM For the analysis of the results, one way ANOVA and Scheffe's multiple range test was executed using the SPSSWIN program. 1. The shear bond strength showed statistically significant difference according to the bracket base design(p<0.001). Type III bracket(round indentation base, micro-etched) showed the highest bond strength, Type I bracket(foil-mesh base) was second, and Type II bracket(grooved integral base, micro-etched) was last. 2. The effect of recycling on the bond strength was different according to bracket type. The shear bond strength of Type I, Type II brackets showed the smallist reduction when treated for 1 minute in Big Jane(p<0.05), but the shear bond strength of Type III brackets showed no statistically significant difference according to recycling method(p>0.05). 3. In Type I, Type II brackets, frequent fracture site was bracket-resin interface, but in Type III brackets, about half of the resin was retained on the tooth surface frequently. 4. The shear bond strength was highest when about half of the resin was retained on the tooth surface(p<0.05). 5. The resin remnant on the bracket base after recycling had no effect on the shear bond strength.

• Journal of the Korea institute for structural maintenance and inspection
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• v.25 no.6
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• pp.199-208
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• 2021

The extrudability of 3D printed concrete and its member strength can be highly influenced by water cement ratio (W/C) and printing time gap (PTG). In this study, mold cast specimens and 3D printed specimens were fabricated with variables of W/C ratio and PTG, and their shear bond strength and interlayer surface moisture content were measured and analyzed. The test results showed that the shear bond strength is greatly influenced by the amount of interlayer surface moisture. It is thus recommended that proper amount of interlayer surface moisture with respect to PTG needs to be maintained to have a required interlayer shear bond strength. In addition, further research is required to estimate the effect of many environmental factors that can influence the interlayer surface moisture content.

• Journal of Dental Rehabilitation and Applied Science
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• v.24 no.3
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• pp.231-242
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• 2008

Purpose: The purpose of this study was to investigate the bond strength of the core-veneer interface in all ceramic systems. Material and Methods: The all ceramic systems tested with their respective veneer were IPS Empress 2 with IPS Eris, IPS e.max Press with IPS e.max Ceram and IPS-e.max ZirCAD with IPS e.max Ceram. Cores (N=36, N=12/group, diameter: 10mm, thickness: 3mm) were fabricated according to the manufacturer's instruction and cleaned with ultrasonic cleaner. The veneer(diameter: 3mm, thickness: 2mm) were condensed in stainless steel mold and fired on to the core materials. After firing, they were again ultrasonically cleaned and embedded in acrylic resin. The specimens were stored in distilled water at $37^{\circ}C$ for 1 week. The specimens were placed in a mounting jig and subjected to shear force in a universal testing machine(Z020, Zwick, Germany). Load was applied at close to the core-veneer interface as possible with crosshead speed of 1.00mm/min until failure. Average shear bond strengths(MPa) were analyzed with a one-way analysis of variance and the Tukey test(${\alpha}=.05$). The failed specimens were examinated by scanning electron microscopy(JSM-6360, JEOL, Japan). The pattern of failure was classified as cohesive in core, cohesive in veneer, mixed or adhesive. Results: The mean shear bond strength($MPa{\pm}SD$) were IPS e.max Press $32.85{\pm}6.75MPa$, IPS Empress 2 $29.30{\pm}6.51MPa$, IPS e.max ZirCAD $28.10{\pm}4.28MPa$. IPS Empress 2, IPS e.max Press, IPS e.max ZirCAD were not significantly different from each others. Scanning electron microscopy examination revealed that adhesive failure did not occur in any all ceramic systems. IPS Empress 2 and IPS e.max Press exhibited cohesive failure in both the core and the veneer. IPS e.max ZirCAD exhibited cohesive failure in veneer and mixed failure.

• Journal of the korean academy of Pediatric Dentistry
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• v.29 no.4
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• pp.509-518
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• 2002

The purpose of this study was to evaluate the bonding of compomer to deciduous dentin which is known to have been developed to improve the weak properties of glass ionomer cement and composite resin. 120 sound primary molars were used for the shear bond strength test and another 24 for the scanning electron microscopic evaluation. Each material was ailed into polyethylene mold attached to exposed dentinal surface($3{\times}4mm$ in diameter) of sample blocks. Shearbond strength was measured using Universal testing machine and data were analyzed statistically with Oneway-ANOVA and Scheffe test. Scanning electron microscopic observation was performed in order to evaluate the pattern of distribution and penetration of resin tags and hybrid layer. Compomer groups(II-V) showed significantly higher bond strength values than glass ionomer group(I)(p<.05). Etching-compomer groups(III, V) showed the significantly higher bond strength than non-etching compomer groups(II, IV)(p<.05), but slightly lower values than composite resin group(VI) with no statistically significant difference(p>.05). No significantly different bond strength was found between compomer groups of different bonding system(p>.05). Scanning electron micrographs showed more irregular distribution of short and thin resin tags in non-etching compomer groups(II, IV) whereas the more regular and intimate distribution of long and thick tags in etching compomer groups(III, V) and composite resin group(VI). The evaluation of hybrid layer also showed more regular formation of thicker layer in etching compomer groups(III, V). Based on the results of present study, the use of compomer as an esthetic restorative material for primary molars might be justified.

• Proceedings of the KWS Conference
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• 2010.05a
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• pp.97-97
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• 2010

최근 자동차에서 경량화의 방안으로써 높은 강성을 요구하는 고장력강 사용이 증대 되고 있다. 그러나 고장력강은 저항 점용접 시 일반 강에 비해 높은 전류를 요구하며 계면파단 및 expulsion 발생이 용이하기 때문에 가용 전류 구간이 좁은 특성을 가진다. 많은 연구자들이 hold time, tempering 등의 process를 이용하여 고장력강의 저항 점용접성을 개선하고자 하였으나 생산 공정라인에 적용하기는 어려운 실정이다. 본 연구에서는 용접 공정 변수의 변화에 따른 용접성과 전극 형상 변화을 통한 고장력강 점 용접성 향상에 대한 연구를 실시 하였다. 고장력강의 점 용접성 비교하기 위해 표준 전극(S1)과 인위적으로 가공한 전극(M1)을 사용하였으며, 실험에 사용된 판재는 두께 1.4mm의 DP590이며, 그 결과 표준전극(S1) 보다 가공 전극(M1)의 가용 전류 구간이 0.5kA 정도 넓은 것으로 확인 되었다. 두 전극을 사용한 점용접 시험편들의 인장전단강도를 비교 해보면 표준전극(S1)을 적용한 점용접 시 인장전단강도는 KS B 0850 기준에 만족하나 계면 파단이 발생 하였다. 가공 전극(M1)을 적용한 점용접 시 인장전단강도는 규격 기준에 만족하나 버튼 파단이 발생 하였다. 두 전극을 적용한 점용접부 형상 및 용접부 온도 분포에대해 저항점용접 시뮬레이션 프로그램(SORPAS)을 이용하여 실험 결과 값과 비교 분석하였고 파단모드의 변화에 대한 원인 분석을 도출 하였다.

• Journal of Adhesion and Interface
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• v.22 no.1
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• pp.8-15
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• 2021

In this study, a polyol was prepared using Jeffamine D-400 as a propylene glycol-based diamine to impart flexibility to the urethane-modified epoxy, and a urethane-modified epoxy was synthesized using the polyol. Urethane-modified epoxy synthesized with existing Bisphenol A diglycidyl ether (BADGE) epoxy, a curing agent, and a curing accelerator are mixed to prepare an epoxy adhesive, and shear strength is measured by measuring adhesion strength. As a result, shear strength and shear elongation tended to increase. These results are due to the high crosslinking density. It is believed that it can be applied to structural adhesives that are restricted in use.

• Composites Research
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• v.16 no.4
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• pp.74-79
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• 2003

Comparison of interfacial properties and microfailure mechanisms of oxygen-plasma treated poly(p-phenylene-2,6-benzobisoxazole(PBO. Zylon) and poly(p-phenylene terephthalamide)(PPTA, Kevlar) fibers/ epoxy composites were investigated using micromechanical technique and nondestructive acoustic emission(AE). Interfacial shear strength(IFSS) and work of adhesion, Wa of PBO or Kevlar fibers/epoxy composites increased by oxygen-plasma treatment. Plasma-treated Kevlar fiber shooed the maximum critical surface tension and polar term, whereas the untreated PBO fiber showed the minimum value. Microfibril fracture pattern of plasma-treated Kevlar fiber appeared obviously. Based on the propagation of microfibril failure toward core region. the number of AE events for plasma-treated PBO and Kevlar fibers increased significantly. The results oi nondestructive AE were consistent well with microfailure modes by optical observation in microdroplet and two-fiber composites tests.

• Composites Research
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• v.16 no.2
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• pp.62-67
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• 2003

Interfacial properties and damage sensing for the carbon fiber/epoxy-amine terminated (AT)-polyetherimide (PEI) composite were performed using microdroplet test and electrical resistance measurements. As AT-PEI content increased, the fracture toughness of epoxy-AT-PEI matrix increased, and interfacial shear strength (IFSS) increased due to the improved fracture toughness by energy absorption mechanisms of AT-PEI phase. The microdroplet in the carbon fiber/neat epoxy composite showed brittle microfailure mode. At 15 phr AT-PEI content ductile microfailure mode appeared because of improved fracture toughness. After curing, the change in electrical resistance $\Delta\textrm{R}$) with increasing AT-PEI content increased gradually because of thermal shrinkage. Under cyclic stress, in the neat epoxy case the reaching time until same stress was faster and their slope was higher than those of 15 phr AT-PEI. The result obtained from electrical resistance measurements under curing process and reversible stress/strain was correspondence well with matrix toughness properties.

• Journal of the Korea institute for structural maintenance and inspection
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• v.18 no.5
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• pp.9-18
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• 2014

Interface behavior and confining effects of concrete-infilled steel tube (CFT) composite beam were investigate based on the experimental observations and numerical analyses. For this purpose, laboratory four-points bending tests were performed for the two test specimens of 1,000mm long CFT composite beams. The test beams were made of ${\phi}110mm$ and 4.5mm thick steel tube and 10mm thick steel web and bottom flange. Therefore, concrete infilled in steel tube was in compression through the entire cross section due to the web and bottom flange. Two end section conditions, with end section cap and without end section cap, were considered in experiments to monitor the relative slip displacement at ends and induce confining effects at center. In numerical aspects, finite element analysis considering steel-concrete interface behavior was performed and compared to the experimental results.