• Journal of Conservation Science
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• v.28 no.2
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• pp.113-118
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• 2012

Cultural heritages emit volatile organic compounds(VOCs) during degradation as chemical, biological factors. These VOCs in the atmosphere are degradation factors for another materials. But non-destructive organic analysis methods are uncommon, and have difficulties for field application. In this study, solid phase micro-extraction(SPME) and gas chromatography( GC) are carried out for analysis of VOCs which are emitted from leather, and prove SPME field holder's efficiency. I analize leather archival objects at The National Archives of Korea by cross-checking GC and SPME methods. It could be confirmed that the compounds are (E)-2-nonenal, butyl hydroxy toluene emitted itself from leather.

• Proceedings of the KWS Conference
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• 2009.11a
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• pp.116-116
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• 2009

마그네슘 합금은 구조용으로 사용 가능한 금속 재료 중 가장 가벼운 소재이며, 동시에 비강도 및 비강성과 같은 기계적 특성이 우수하여 알루미늄 합금의 뒤를 이을 차세대 경량 재료로써 주목을 받고 있다. 더욱이 석유자원의 대부분을 소비하고 있는 운송기기 분야에서는 경량화를 통한 연비향상과 배출가스 저감이 가장 큰 과제이며, 이 문제를 해결하기 위한 노력의 일환으로 최경량 소재인 마그네슘 합금의 사용량은 더욱 증가할 것으로 기대된다. 한편 기존의 마그네슘 합금 관련 연구는 새로운 합금의 개발에 치우쳐 있었으며, 상대적으로 이들 합금을 활용하기 위한 가공기술, 특히 용접에 대한 연구는 아직까지 많이 부족한 실정이다. 이는 철강재와 비교하여 마그네슘 합금의 고유물성이 용접의 관점에서는 상당히 열악하기 때문으로, 마그네슘은 융점 및 비점은 낮은 반면, 증기압과 열전도율은 높고 표면장력 및 점성은 낮은 특성을 가지고 있다. 그러므로 타 공법에 비해 상대적으로 입열이 적고 고속용접이 가능한 레이저의 적용이 최적으로 판단된다. 따라서 본 연구에서는 Nd:YAG 레이저를 사용하여 압연판재로 상용화되어 있는 AZ31B 마그네슘 합금의 맞대기 용접성을 조사하였으며, 용접부의 미세조직과 용접조건에 따른 용접부의 기계적 특성을 비교 및 검토하였다. 용접부의 기계적 특성은 인장 및 경도시험을 통해 평가하였다. 그 결과 레이저 출력 1.2kW를 적용한 경우에 안정적인 강도를 얻을 수 있었으며 레이저 출력 1.5kW, 용접속도 80mm/sec의 조건에서 모재 인장강도 대비 103% 그리고 연신율 대비 47.1%의 최적의 결과가 얻어졌다. 또한 용접부의 경도는 모재와 동등하거나 다소 높은 수준이었다. 이는 용접시 용접부내 잔류하는 알루미늄에 의한 고용 강화 효과와 금속간화합물의 석출 빈도 증가, 그리고 레이저 용접의 특징인 급열급랭 공정에 기인한 결정립 미세화의 영향 때문으로 사료된다. 한편 용접부 미세조직을 관찰한 결과, 열영향부의 존재는 두드러지지 않았으며 용융경계부에서는 주상정이, 그리고 용접부 가운데에서는 등축정이 관찰되었다.

• Journal of Korean Society for Atmospheric Environment
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• v.22 no.5
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• pp.712-718
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• 2006

In order to investigate the analytical uncertainties associated with sampling and analysis of major greenhouse gaseous pollutants(carbon dioxide and methane), we attempted to quantify their adsorptive loss due to the contact with the container wall(such as Tedlar bag and vial). Using the GC/FID method, some basic experimental parameters(such as reproducibility and method detection limit) have been evaluated as part of the essential QA/QC The reproducibilities of carbon dioxide and methane were estimated as 2.02 and 0.2%, respectively. In addition, method detection limits were measured as 0.61 and 0.06 ng, respectively. A test of sample loss rate has also been made for Tedlar bag and vial by assessing the absolute amount of sample loss on the wall. By transferring the samples contained in Tedlar bag to various sizes of Tedlar bags, we measured differences in the absolute loss quantity due to such transfer. In addition, we also examined such loss mechanism as a function of elapsed time and light penetration rate for vial. As results, carbon dioxide and methane have shown about 2% of sample loss due to such contact. It is also noticed that the amount of loss with vial surface is lower than that of Tedlar bag. Therefore, field collection of greenhouse gases using various container types should be made more cautiously to minimize the possibility of sample loss and bias related to such loss.

• Analytical Science and Technology
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• v.18 no.3
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• pp.241-249
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• 2005

In this study, instrumental neutron activation analysis was used to measure the concentrations of about 30 trace elements in airborne particulate (PM2.5) samples at urban area of Daejeon city located in the southwestern region of Korea. An inspection of the measurement data indicates that the distribution patterns of trace elements could clearly distinguish the elements with their concentrations ranging over five orders of magnitude. The mean values for Lu and Dy were found to be the lowest at values of 0.01 and $0.04ng/m^3$, while those for K and Fe showed the highest value of 671 and $653ng/m^3$, respectively. The results of correlation analysis showed that PM2.5 concentrations can exhibit much more enhanced correlations with the elements of earth crustal components. The results of factor analysis further indicated that there are no more than six factors with statistical significance, which may exert dominant roles in regulating the elemental concentration levels in the study area. Enrichment factor analysis supports explicit interpretation of results found by this factor analysis.

• Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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• 2002.11a
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• pp.440-447
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• 2002

This paper considerated about exact flow volume calculation method from factors having an influence on measurement and introduced in anesthesia ventilator realized spirometry system. System used differential pressure sensing method with factors, that is temperature, pressure, gas density, humidity and mucus etc. System optimized for low power system for mobile system. System composed analog interface part, signal processing part, display part. Analog interface part have differential pressure flow sensor and defferential pressure sensor. Signal processing part have AVR processor for low power system display part use serial port (RS232, SPT). so it display at pc monitor or send to anesthesia ventilator. System is stable by linearizing 2th characteristics of flow-differential pressure, auto correction of sensor. Noise reduced by algorithm with analog filter and digital processing. Small, light, low power system is good at mobile system and applied to patient in emergency or mobile. and, System is useful at anesthesia ventilator by using flow sensor.

• Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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• v.21 no.2
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• pp.46-53
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• 2007

Extension of the mobile communication and the rapidly developing services connected with wireless multimedia(W-CDMA, DMB, Wibro, and so on) need great many base station transceiver systems, antennas, and many signal transmission line to embody these services. The min communication appliances system is exposed always in danger of transient overvoltage by direct stroke or induced lightning surge flowing in through antenna because the antenna of base station transceiver system or relay equipment is combined with expensive communication network equipments through signal transmission line. Now, gas discharge tube(GDT) or narrow band stub arrestor which is used by the surge protector for communication use is exposing limitations as for lightning surge protective means of the communication facility with high speed and wide frequency band. Therefore, for improving performance of surge arrestor, we applied ceramic filter which can reduce lightning surge invading from antenna effectively, and proved that ceramic filter is effective in residual voltage reduction through the experimental research.

• The Transactions of the Korean Institute of Electrical Engineers B
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• v.51 no.9
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• pp.522-529
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• 2002

In this paper, computer simulations of the physical Phenomena occurring in the arc region before and after current zero were carried out to evaluate the thermal recovery characteristics of a Laval nozzle. A commercial CFD program "PHOENICS" is used for the simulation and the user-coded subroutines to consider the arcing phenomena were added to this program by the authors. The computed results were verified by the comparison with the test results presented by the research group of GE Co.(General Electric Company). In order to investigate the state of the arc region after current zero, the simulation was carried out with three steps. They are steady state arc simulation, transient arc simulation before current zero, and transient hot-gas flow simulation after current zero. The semi-experimental arc radiation model is adapted to consider the radiation energy transport and Prandtl's mixing length model is employed as the turbulence model. The electric field and the magnetic field were calculated with the same grid structure used for the simulation of the flow field. The post-arc current was calculated to evaluate the thermal recovery characteristics after current zero. Compared with the results obtained by GE Co., it has been found that the critical RRRV(ratio of rise of recovery voltage) will be determined previously by this study.his study.

• Proceedings of the KIEE Conference
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• 2003.07c
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• pp.1770-1772
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• 2003

본 연구는 국내에서 최초로 제안되고 적용가능성이 입증되어 설계, 제작된 Probe-type Pockets sensor(HY-Pockets Sensor)를 GIS등의 고전압 장비들에 응용한 레이저 부분방전 진단 시스템 개발을 목표로 하고 있다. 이러한 목적으로, 170kV 급 실 규모 GIS내부의 전류 도체에 다양한 곡률 반경의 침 전극을 부착시켜 부분 방전에 기인된 불평등 전계를 형성시켜 개발된 센서의 실규모 적용 가능성을 고찰하였다. 본 레이저 계측 시스템은 He-Ne laser, single multi-mode optical fiber, $2{\times}2$ 50/50 laser to single mode fiber coupler, probe-type Pockets sensor, photo detector 등으로 구성하여 레이저의 진행을 유도하고, 신호의 특성을 분석하였다. probe-type Pockets sensor로부터 의 출력 신호는 photo detector를 통해 전기적 신호로 변환되어 digital oscilloscope에 의해 측정되고, 또한 PC를 통해 데이터의 저장과 통계적, 분석적 처리 과정을 수행하게 된다. 본 연구의 결과로서 부분방전원에서 생성된 방전 신호에 대한 거리에 따른 센서 감도 결정, 그에 대한 센서 감도의 보정 향상, 전계의 세기의 변화에 따른 센서의 선형성 등이 도출되었고, 이러한 실험결과를 통해 실 GIS(170kv급) 내부에서 발생하는 부분방전의 검출에 본 레이저 부분방전 진단 시스템의 적용 가능성이 제시 되었다.

• Land and Housing Review
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• v.4 no.3
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• pp.287-294
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• 2013

Energy saving strategy for public housing is given a sizable portion in Land and Housing corporation. From this reason, the consumer's characteristics and energy consciousness of public housing dweller was derived from field survey for compare with sale housing residents characteristics. Utilities fees (e.g. gas and electric) for public housing residents was about 50 percent of sales housing dweller, but real energy consumption was accounting for 70% of sales housing residents in electric consumption. Among the respondents for public housing dweller up to 80 percentile of end-user comment that they have less demanding utilities fees. Given the major energy saving strategies, such as install EMS, make a teaching tool for children, sale housing residents is more proactive approach to participant energy saving strategies than public housing residents.

• Journal of the Korean Applied Science and Technology
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• v.31 no.3
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• pp.345-351
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• 2014

Dinitramide ($N(NO_2)_2$) salts are one of plausible oxidizing agents for a high efficient propellant. Guanidine dinitramide (GDN) is an organic salt improving its stability against moisture, so that enables massive production and long term storage. Several types of GDN (GDN-1,2,3,4,5) were synthesized using some types of starting materials such as guanidine acetate, chloride, carbonate, nitrate and sulfate. As a result of the experimental work, synthesized GDN from the carbonate salt appeared fairly pure relatively higher yield (99%) than the other samples. The absorption wave length of all prepared GDNs by FTIR were found at 3452, 3402, 3354, 3278, 3208, 1642, 1570, 1492, 1416, 1337, 1179 and $1000cm^{-1}$. DSC analysis found a thermal phase change at $130^{\circ}C$, and indicated exothermic reaction at about $150^{\circ}C$ to $160^{\circ}C$.