• 제목/요약/키워드: 偏析

검색결과 230건 처리시간 0.03초

쌍롤 박판주조법으로 제조된 고합금계 알루미늄 합금의 미세조직 및 기계적 특성

  • 천부현;김형욱;이재철
    • 한국재료학회:학술대회논문집
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    • 한국재료학회 2009년도 추계학술발표대회
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    • pp.47.1-47.1
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    • 2009
  • 최근 환경과 에너지에 대한 관심이 증대됨에 따라 차체의 경량화를 위한 고합금계 알루미늄 합금의 연구가 활발히 진행되고 있다. 특히 5000계 알루미늄 합금은 비중이 낮을 뿐만 아니라 Mg의 첨가에 의해 높은 강도 및 성형성을 얻을 수 있기 때문에 자동차용 판재로 많은 주목을 받고 있다. 현재 사용되는 대부분의 알루미늄 합금판재는 DC주조법과 추가적인 압연공정으로 제조되기 때문에 경제성 문제와 낮은 냉각속도로 인한 금속학적인 문제를 갖는다. 그러나 DC주조법과는 달리 쌍롤 박판주조법은 용탕으로부터 직접 판재를 제조하기 때문에 경제적이며 효율적인 주조공정이다. 또한 냉각속도가 빠르기 때문에 비교적 주조편석이 적고 전반적인 미세조직이 균일하여 고합금계 알루미늄 합금 판재제조에 매우 유용하게 응용될 수 있다. 본 연구에서는 쌍롤 박판주조법으로 고합금계 알루미늄 합금 판재를제조하고, 제조된 합금의 열간압연 및 열처리 조건에 따른 기계적 특성을 비교 및 평가하였다. 또한 미세조직 및 집합조직을 분석함으로써 고합금계 알루미늄 합금 판재의 실용화 가능성을 평가하였다.

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레오로지 소재의 고상입자 거동 예측을 위한 결정립 동력학 해석 (Analysis of Grain Size Controlled Rheology Materials Dynamics for Prediction of Solid Particles Behavior)

  • 김현일;강충길
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2005년도 춘계학술대회 논문집
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    • pp.1337-1340
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    • 2005
  • A rheology casting technology has some advantages compared with conventional forming processes such as die casting, squeeze casting and hot/cold forming. The liquid segregation is important on mechanical properties of materials using rheology casting. In this study, so, molecular dynamics simulations were performed for the control of liquid segregation. Because the dynamics of fluid flow about nano-scaled materials is completely different from continuum, molecular dynamics simulations were used. The behavior of particles was far from the truth according to boundary conditions in simple flow. But various movement of particles appear at two or more molecular simulations.

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반응고 다이캐스팅공정에서 사출조건이 액상편석에 미치는 영향 (The effect of the injection condition on liquid segregation in semi-solid die casting process)

  • 신현기;서판기;강충길
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2003년도 춘계학술대회논문집
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    • pp.70-73
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    • 2003
  • Semi-solid processing is now becoming of great interest for the production of various parts by pressure die casting. Many advantages are associated with this forming process at the condition that the forming operation is performed under appropriate conditions in terms of alloy microstructure, injection velocity and pressure. In this study, to look into the relation along them, the experiment of semi-solid die casting has been peformed with various condition of injection, and investigated their microstrucure and solid fraction

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결정립제어 레오로지 소재의 입자유동 해석 (Particle Flow Analysis of Grain-Size Controlled Rheology Materials)

  • 김현일;강충길
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2004년도 추계학술대회 논문집
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    • pp.774-777
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    • 2004
  • A rheology casting technology has some advantages compared with conventional forming processes such as die casting, squeeze casting and hot/cold forming. The liquid segregation is important on mechanical properties of materials using rheology casting. In this study, so, molecular dynamics simulations were performed for the control of liquid segregation. Because the dynamics of fluid flow about nano-scaled materials is completely different from continuum, molecular dynamics simulations were used. The behavior of particles was far from the truth according to boundary conditions in simple flow. But various movement of particles appear at two or more molecular simulations.

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안정화 지르코니아 고체전해질의 입계전도 향상 (Improvement of Grain-Boundary Conduction in Stabilized Zirconia)

  • 이종흔
    • 한국재료학회:학술대회논문집
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    • 한국재료학회 2003년도 추계학술발표강연 및 논문개요집
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    • pp.25-25
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    • 2003
  • 안정화 지르코니아(Stabilized Zirconia)는 산화물 연료전지 (SOFC: Solid Oxide Fuel Cell), 전기화학식 가스센서 등에 널리 사용되고 있는 대표적인 고체전해질이다. SOFC의 효율향상 및 센서의 저온 동작을 위해서는 높은 이온전도도를 갖는 고체전해질이 요구된다. 안정화 지르코니아의 이온 전도도를 향상시키기 위해 MgO, CaO, $Y_2$O$_3$, Yb$_2$O$_3$, Sc$_2$O$_3$ 등의 안정화제가 첨가된 바 있으며, 이들 첨가제의 변화에 의한 전기전도도 향상 연구는 현재 성숙된 단계이다. 지르코니아 고체전해질의 안정화제가 정해진 상태에서 재료의 전기전도도를 향상시키는 다른 방법은 입계에서의 이온전도도를 높이는 것이다. 안정화 지르코니아는 입계가 입내에 비해 저항이 약 100-10000배 정도크기 때문에, 입계가 얇은 두께에도 불구하고 전해질의 저항에서 큰 역할을 한다고 알려져 있다. 일반적으로 입계의 Si-포함상 편석, 입계액상, 공간전하층등이 입계의 저항에 대한 원인으로 받아 들여 지고 있다.

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황동볼트 손상원인 분석사례

  • 정남근
    • 열병합발전
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    • 통권30호
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    • pp.21-25
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    • 2002
  • According to recent Korea Electric Power Company report, yearly distribution line brass cramp bolts failure summed up to 4,400 cases emerging as one of main local break-down causes. Naturally, the need for the investigation was proposed To determine the root cause of the cramp bolt failures, mechanical and metallurgical investigation were performed for 90 samples which collected from various sites. For the understanding of the geometric characteristics, stress distribution was evaluated by CAE program and proof load of each bolts was tested. The SEM&EDS was used for metallurgical investigation. Through the investigation, the root causes of failures were confirmed. All damaged bolts showed intergrannular fracture mode and the all fractured bolt showed ß phase morphology contrast to the a&ß mixture morphology of the non-damaged samples. Additionally, EDS analysis confirmed the existence of lead rich layer on grain boundaries.

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12%Cr 대형강괴(大型鋼塊)의 편석경감(偏析輕減)에 관(關)한 연구(硏究) (A Study on the Reduction of Segregation in Large 12%Cr Steel Ingot)

  • 은옥기;장윤석
    • 한국주조공학회지
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    • 제10권6호
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    • pp.520-527
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    • 1990
  • In order to reduce segregation in 12%Cr steel ingots of 60-100tons, numerical analysis by computer was applied to simulate solidification profiles and the profiles of liguid-solid coexisting zone in accordance with the ratios of H(Height) /D(diameter) of 100-ton ingot. The result is that the ratio of L(vertical length) /D(diameter) of liquid-solid coexisting zone was reduced in proportion to the decrease of H/D ratio. With the reduced H/D ratio(0.92) of ingot, the segregation in 60-ton ingot of 12% Cr steel can be much reduced and recovery was also improved by reducing ingot weight.

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7075 및 7050 알루미늄 합금의 응고 거동 및 편석에 미치는 냉각 속도의 영향 (The Effect of Cooling Rate on the Solidification Behavior and Segregation of 7075 and 7050 Aluminum Alloys)

  • 최정윤;권영동;이주원;이진형
    • 한국주조공학회지
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    • 제21권6호
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    • pp.343-349
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    • 2001
  • The effect of cooling rate on the solidification microstructure and segregation behavior of 7075 and 7050 aluminum alloy was investigated. Samples were solidified with cooling rates from 0.3 to $17^{\circ}K/sec$. Using the cooling curves of each sample, liquidus, eutectic and intermetallic reaction temperatures were estimated. The microstructures were characterized in terms of dendrite arm spacing and eutectic volume fraction. The segregation behavior of each alloying element of these alloys in various cooling rates was discussed.

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극박 3%규소강에서 Mn이 황의 편석 거동 및 자성특성에 미치는 효과 (Effects of Mn on Sulfur Segregation and Magnetic Induction in Thin-gauged 3%Si-Fe Strip)

  • 조성수
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2001년도 하계학술대회 논문집
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    • pp.917-920
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    • 2001
  • Effects of addition of manganese and final reduction on segregation behavior of sulfur and final mangetic induction during final annealing have been investigated in the 300 ppm sulfur-contained 3% silicon-iron alloy strips with or without manganese. At the same concentration of sulfur, lower final reduction is favorable for final Goss texture. This is because the probability that the initial Goss grains survive under the highly segregated sulfur atmosphere and grow selectively within the segregated sulfur-free time range becomes higher. In the case of 3% silicon-iron with manganese, much lower magnetic induction was obtained, although the weak final reduction of 30% is given to the alloy, comparative to the 40%. This is because MnS particles acted as an reducer in the primary grain size.

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