• Journal of the Korean Applied Science and Technology
• /
• v.10 no.2
• /
• pp.41-47
• /
• 1993

Chitin was isolated from crab shells by modified Hackman's method, which was treated again with aqueous sodium hydroxide solution to give alkali chitin(sodium alkoxide of chitin). And after, the alkali chitin is allowed to react with monochloroacetic acid to synthesize 6-O-(carboxymethyl) chitin [CM-Chitin] under diminished pressure. In order to synthesize high performance CM-Chitin as hygroscopic agent, it was measured that the yield and degree of subsititution of each CM-Chitin according to molar ratio(monochloroacetic acid equivalent mol/N-acetyl-D-glucosamine residue) and their moisture-absorption and moisture-release properties were measured and compared with those of hyaluronic acid. The moisture-absorption and moisture-release properties of CM-Chitin, especially 0.8 in degree of substitution, were found quite similar to those of hyaluronic acid. The preliminary results show that CM-Chitin might be used as hygroscopic agent instead of hyaluronic acid in field of cosmetics.

• Journal of the Korea Institute of Military Science and Technology
• /
• v.6 no.3
• /
• pp.44-53
• /
• 2003

Cu/C films were prepared at room temperature under $Cu(hfac)_2-Ar-H_2$ atmosphere in order to obtain metallized polymer by using ECR-MOCVD(Electron Cyclotron Resonance Metal Organic Chemical Vapor Deposition) coupled with a DC bias system. The room temperature MOCVD on polymer substrate could be possible by collaboration of ECR and a DC bias. Structural analysis of the films by ECR was found that fine copper grains embedded in an amorphous polymer matrix with indistinctive interfacial layer. The increase in $H_2$ contents brought on copper-rich film formation with low electric resistance. On the other hand carbon-rich films with low sheet electric resistance were prepared in argon atmosphere. The electric sheet resistance of Cu/C films with good interfacial property were controlled at $10^8$~$10^0$ Ohm/sq. ranges by the $H_2$/Ar mole ratio and the shielding effectiveness of the film showed maximum up to 45dB in the our experimental range.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 2008.04b
• /
• pp.8-9
• /
• 2008

In the procedure of the estimation, the short time breakdown characteristics for the epoxy composite specimens, which were made with the variation of hardener and/or filler, were tested firstly. Then the long time voltage-to-time test was implemented. Finally, the long time breakdown voltage of each specimen was estimated with the parameters obtained from the statistical treatment with Weibull distribution. Base on the results, it has been found that the optimal weight ratio of epoxy resin/hardener/filler that has the excellent long time breakdown characteristic was 100/100/65. It was due to the silane treatment which relieves the electric field at the interface between filler and epoxy.

• The Transactions of the Korean Institute of Electrical Engineers C
• /
• v.54 no.3
• /
• pp.120-126
• /
• 2005

The Korean Superconducting Tokamak Advanced Research (KSTAR) tokamak device is being constructed to perform long-pulse, high-beta, advanced tokamak fusion physics experiments. The long-pulse operation requires the non-inductive current drive system such as the Lower-Hybrid Current Drive (LHCD) system. The LHCD system drives the non-inductive plasma current by means of C-band RF with 2-MW CW power and 5-GHz frequency. For the LHCD test experiments, an RF test system is developed. It is composed of a 5-GHz, 1.5-MW pulsed magnetron and a compact pulse modulator with $4\;{\mu}s$ of pulse width. The pulse modulator provides the maximum output voltage of 45 kV and the maximum current of 90 A. It is composed of 7 stages of Pulse Forming Network (PFN), a thyratron tube (E2V, CX1191D), and a pulse transformer with 1:4 step-up ratio. In this paper, the detailed design and the performance test of the pulse modulator are presented.

• Transactions on Electrical and Electronic Materials
• /
• v.4 no.5
• /
• pp.28-32
• /
• 2003

Europium-doped gadolinium oxide ($Gd_2O_3;Eu^{3+}$) phosphors have been prepared by combustion method using urea[H$_2$NCONH$_2$] or carbohydrazide[H$_2$NNHCONHNH$_2$] as fuel materials in a preheated furnace at 500$^{\circ}C$. The phosphors obtained were fired at 1200$^{\circ}C$ for 3 hours to get better luminescent properties. The combustion method used was found to be a simple and fast method for the preparation of fine-sized particles. The influence of the fuel/oxidant (urea or carbohydrazide/nitrate) mole ratio on the phosphor has been investigated and the optimum values for various parameters have been determined. By this method, phosphor that has better brightness and smaller size particles than that obtained by conventional method has been prepared.d has been prepared.

• Proceedings of the KIEE Conference
• /
• 2005.07c
• /
• pp.1881-1883
• /
• 2005

In this study, PZT thin films were fabricated using sol-gel Processing onto $Si/SiO_2/Ti/Pt$ substrates. PZT sol with different Zr/Ti ratio(20/80, 30/70, 40/60, 52/48) were prepared, respectively. The films were fabricated by using the spin-coating method on substrates. The films were heat treated at $450^{\circ}C$, $650^{\circ}C$ by rapid thermal annealing(RTA). The preferred orientation of the PZT thin films were observed by X-ray diffraction(XRD), and Scanning electron microscopy(SEM). All of the resulting PZT thin films were crystallized with perovskite phase. The fine crystallinity of the films were fabricated. Also, we found that the ferroelectric properties from the dielectric constant of the PZT thin films were over 600 degrees, P-E hysteresis constant. And the leakage current densities of films were lower than $10^{-8}\;A/cm^2$. It is concluded that the PZT thin films by sol-gel process to be convinced of application for ferroelectric memory device.

• Proceedings of the KIEE Conference
• /
• 2003.07c
• /
• pp.1562-1564
• /
• 2003

In this study, PZT thin films were fabricated using sol-gel processing onto Si/$SiO_2$/Ti/Pt substrates. PZT sol with different Zr/Ti ratio(20/80, 30/70, 40/60, 52/48) were prepared, respectively. The films were fabricated by using the spin-coating method on substrates. The films were heat treated at $450^{\circ}C,\;650^{\circ}C$ by rapid thermal annealing(RTA). The preferred orientation of the PZT thin films were observed by X-ray diffraction(XRD), and Scanning electron microscopy(SEM). All of the resulting PZT thin films were crystallized with perovskite phase. The fine crystallinity of the films were fabricated. Also, we found that the ferroelectric properties from the dielectric constant of the PZT thin films were over 600 degrees, P-E hysteresis constant. And the leakage current densities of films were lower than $10^{-8}A/cm^2$. It is concluded that the PZT thin films by sol-gel process to be convinced of application for ferroelectric memory device.

• Journal of Korea Foundry Society
• /
• v.17 no.5
• /
• pp.494-501
• /
• 1997

In order to manufacture large rod preforms of 2014 Al alloy with a good mechanical property by spray forming method, it was spray-formed at a droplet temperature of $715^{\circ}C$, a droplet flight distance of 400mm, and a spraying angle of $35^{\circ}$. The rod preforms were extruded at $397^{\circ}C$ with the die temperature of $420^{\circ}C$ under the hot extrusion ratio 21:1 and T6 heat treatment was performed. The 2014 Al alloys cast by hot top process were also extruded and heat-treated at the same condition as a reference material. Microstructural observation and tensile test were carried out to investigate the effects of extrusion on microstructure and mechanical property of spray-formed Al alloy. Spray-formed Al alloys had many porosities due to inappropriate process conditions such as long droplet flight distance and low droplet temperature but have fine equiaxed grain. These porosities were reduced with decreasing in grain size by hot extrusion. Ultimate tensile strength and yield strength of spray formed-extruded 2014 Al alloy were inferior to those of the normal cast-extruded 2014 Al alloy, but elongations were superior. The control of porosity was important to get spray formed preform with a good mechanical property.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 2004.07a
• /
• pp.461-464
• /
• 2004

In this paper, the elastic epoxy added elastomer having viscoelasticity to existing epoxy was measured thermal, structural properties through TGA(Thermogravimetric Analysis) and FESEM(Field Emission Scanning Electron Microscope). Specimens were made of dumbbell forms by the ratio of 5[phr], 10[phr], 15[phr], and 20[phr] by regulation with elastomer contents. The measurement temperature dimensions of TGA were $0[^{\circ}C]\;to\;800[^{\circ}C]$, and rising temperature was $5[^{\circ}C/min]$. And we observed structure through FESEM at the magnification of 1000times with the voltage of 15[kV] after breaking by quenching specimens. As thermal analysis results, we could know that thermal and structural properties was improved quantity according to decrease of elastomer contents. In general, thermal, structural properties of 15[phr] was excellent among the specimens.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2005.05a
• /
• pp.407-410
• /
• 2005

The drawability of AZ31B magnesium sheet is estimated according to the variable temperatures (200, 250, 300, 350 and $400^{\circ}C$), forming speed (20, 50, 100 mm/min), thickness (0.8, 1.4 t), blank holding force (1.0, 1.4, 1.7kN). The deep drawing process (DDP) of circular cup is used in forming experiments. The results of deep drawing experiences show that the drawability is well at the range from 250 to $300^{\circ}C$, 50mm/min forming speed and 1.4kN blank holding force. The 0.8t magnesium sheets were deformed better than 1.4t. BHF was controlled in order to improve drawability and protect the change of cup thickness. When BHF was controlled, tearing and thickness change were decreased and LDR. was improved from 2.1 to 3.0.