• 제목/요약/키워드: (5/3) transform

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Fourier Transform Infrared Spectrophotometric Direct on Filter 방법을 이용한 석영 분석의 기초 연구 - 필터재질, 비균일 침착 및 습도의 영향 - (The Preliminary Study on the Quantitative Analysis of Quarts by Fourier Transform Infrared Spectrophotometric Direct on Filter(FTIR-DOF) Method -Effects of filter materials, inhomogeneity of deposition, and humidity-)

  • 피영규;김현욱
    • 한국산업보건학회지
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    • 제15권1호
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    • pp.1-7
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    • 2005
  • Although the Fourier Transform Infra-Red spectrophotometric Direct on Filter(FTIR-DOF) method is a useful analytical technique for quantifying quartz content in respirable dust samples, a number of analytical problems must be taken into consideration such as, to name only a few, inhomogeneous deposition of particles, level of environmental humidity, uneven surface of the filter, and interfering minerals in the sample. This study was designed to select the most suitable wavelength and proper filter material for the method, and to investigate effects of humidity and inhomogeneous deposition of particles on the filter. Samples of respirable dust, created in a dust chamber containing standard material of quartz, were collected using a cyclone equipped with a 25mm filter as a collection medium. The results were as follows; 1. Among seven (7) commercially available filters tested for the FTIR-DOF method, the DM 800 filter showed the best analytical performance having the lowest background absorbance bands and no overlapping peaks at 799, 779, and $695cm^{-1}$. 2. The variations of absorbance due to humidity ranged from 1.0% to 3.3% for $799cm^{-1}$, 1.0% to 3.3% for $779cm^{-1}$, and 8.9%~20.9% for $695cm^{-1}$ peaks, respectively. The $699cm^{-1}$ peak was proved to be most vulnerble to environmental humidity for quantitative analysis of quartz. 3. As for effects of inhomogeneous deposition of samples, the highest variation of absorbance of 10.9% ($13.5{\mu}g$) was observed when using the 695cm-1. The variations of absorbance from the other two peaks, 799 and $779cm^{-1}$, ranged from 1.2 to 3.2%, and 1.4 to 4.1%, respectively. Therefore, the $799cm^{-1}$ peak was considered to be most reliable for quantitative analysis of quartz. The results of this study suggest that, for quantitative analysis of quartz in the respirable dust samples, use of the $799cm^{-1}$ peak can minimize the influence of environmental humidity and inhomogeneous deposition of particles on the filter. The FTIR-DOF method, if adopted for routine analysis of quartz in the respirable dust samples, could save sample preparation time and efforts substantially and also could increase analytical throughputs. Since use of the $799cm^{-1}$ peak is prone to be affected by interferences in the sample, further research on minimizing the effects is needed.

시간 적응 3차원 subband 부호화 기법 (Temporal adaptive 3D subband image sequence coding technique)

  • 김용관;김인철;이상욱
    • 한국통신학회논문지
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    • 제21권5호
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    • pp.1096-1108
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    • 1996
  • In this paper, we propose a temporal adaptive tranform 3D SBC coder with motion compensation, exploiting redundancy in the temporal domain. We propose a temporal adaptivity measure, by which the R-D optimal temporal transform can be chaosen. The base temporal subband frame is coded using H.261-like MC-DCT coder, while the higher temporal subband frames are coded using the 2D adaptive wavelet packet bases, considering the various energy distribution which results from the temporal variation. In encoding the subbands, we employ adaptive scanning methods, uniform step-size quantization with VLC, and coded/not-coded flag reduction technique using the quadtree structure. From the simulation results, the proposed adaptive 3D subband coder shows about 0.29~3.14 dB gain over the H.261 and the fixed 3D subband coder techniques.

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In-situ 도핑된 M/NEMS용 다결정 3C-SiC 박막의 특성 (Characteristics of in-situ doped polycrystalline 3C-SiCthin films for M/NEMS applications)

  • 김강산;정귀상
    • 센서학회지
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    • 제17권5호
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    • pp.325-328
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    • 2008
  • This paper describes the electrical properties of poly (polycrystalline) 3C-SiC thin films with different nitrogen doping concentrations. In-situ doped poly 3C-SiC thin films were deposited by APCVD at $1200^{\circ}C$ using HMDS (hexamethyildisilane: $Si_2(CH_3)_6)$) as Si and C precursor, and $0{\sim}100$ sccm $N_2$ as the dopant source gas. The peak of SiC is appeared in poly 3C-SiC thin films grown on $SiO_2/Si$ substrates in XRD(X-ray diffraction) and FT-IR(Fourier transform infrared spectroscopy) analyses. The resistivity of poly 3C-SiC thin films decreased from $8.35{\Omega}{\cdot}cm$ with $N_2$ of 0 sccm to $0.014{\Omega}{\cdot}cm$ with 100 sccm. The carrier concentration of poly 3C-SiC films increased with doping from $3.0819{\times}10^{17}$ to $2.2994{\times}10^{19}cm^{-3}$ and their electronic mobilities increased from 2.433 to $29.299cm^2/V{\cdot}S$, respectively.

Analysis of Antenna Impact on Wide-band Indoor Radio Channel and Measurement Results at 1 GHz, 5.5 GHz, 10 GHz and 18 GHz

  • Santella, Giovanni
    • Journal of Communications and Networks
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    • 제1권3호
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    • pp.166-181
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    • 1999
  • The object of this paper is to investigate the influence of antenna pattern on indoor radio channel characteristics. Different from previous works where this analysis was carried out at a fixed frequency using different antennas, in the present paper (where measurements were taken in a wide frequency range) the variation of the radiation pattern was caused by two factors: the change of the radiation pattern when the same antenna was used at different frequenicies and the use of different type of antennas. To carry out this analysis, frequency domain measurements of the indoor radio channel at 1 GHz, 5.5 GHz, 10 GHz and 18 GHz were collected. Measurements were taken using a network analyzer. Serveral re-alizations of the channel transfer function were obtained varying, for each measurement, the positon of the transmitter and keep-ing the receiver fixed. Estimate of the channel impulse response was obtained from the Inverse Fourier Transform (IFT) of the fre-quency response. The measurements were performed in an office enviroment with mostly metallic walls and inner separations. The obtained data were elaborated to obtain the power versus distance relationship, the Cummulative Distribution Functions(CDFs) of rms Delay Spread(DS) and of the 3 dB frequency correlation band-width. Finally, the 3 dB width of the frequency correlation func-tion has been empirically related to the inverse of the rms DS of the impulse response.

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Comparative Biodegradation of HDPE and LDPE Using an Indigenously Developed Microbial Consortium

  • Satlewal, Alok;Soni, Ravindra;Zaidi, Mgh;Shouche, Yogesh;Goel, Reeta
    • Journal of Microbiology and Biotechnology
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    • 제18권3호
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    • pp.477-482
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    • 2008
  • A variety of bacterial strains were isolated from waste disposal sites of Uttaranchal, India, and some from artificially developed soil beds containing maleic anhydride, glucose, and small pieces of polyethylene. Primary screening of isolates was done based on their ability to utilize high- and low-density polyethylenes (HDPE/LDPE) as a primary carbon source. Thereafter, a consortium was developed using potential strains. Furthermore, a biodegradation assay was carried out in 500-ml flasks containing minimal broth (250ml) and HDPE/LDPE at 5mg/ml concentration. After incubation for two weeks, degraded samples were recovered through filtration and subsequent evaporation. Fourier transform infrared spectroscopy (FTIR) and simultaneous thermogravimetric-differential thermogravimetry-differential thermal analysis (TG-DTG-DTA) were used to analyze these samples. Results showed that consortium-treated HDPE (considered to be more inert relative to LDPE) was degraded to a greater extent (22.41% weight loss) in comparison with LDPE (21.70% weight loss), whereas, in the case of untreated samples, weight loss was more for LDPE than HDPE (4.5% and 2.5%, respectively) at $400^{\circ}C$. Therefore, this study suggests that polyethylene could be degraded by utilizing microbial consortia in an eco-friendly manner.

Novel Synthesis Method and Electrochemical Characteristics of Lithium Titanium Oxide as Anode Material for Lithium Secondary Battery

  • Kim Han-Joo;Park Soo-Gil
    • KIEE International Transactions on Electrophysics and Applications
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    • 제5C권3호
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    • pp.119-123
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    • 2005
  • Lithium titanium oxide as anode material for energy storage prepared by novel synthesis method. Li$_{4}$Ti$_{5}$O$_{12}$ based spinel-framework structures are of great interest material for lithium-ion batteries. We describe here Li$_{4}$Ti$_{5}$O$_{12}$ a zero-strain insertion material was prepared by novel sol-gel method and by high energy ball milling (HEBM) of precursor to from nanocrystalline phases. According to the X-ray diffraction and scanning electron microscopy analysis, uniformly distributed Li$_{4}$ Ti$_{5}$O$_{12}$ particles with grain sizes of 100nm were synthesized. Lithium cells, consisting of Li$_{4}$ Ti$_{5}$O$_{12}$ anode and lithium cathode showed the 173 mAh/g in the range of 1.0 $\~$ 3.0 V. Furthermore, the crystalline structure of Li$_{4}$ Ti$_{5}$O$_{12}$ didn't transform during the lithium intercalation and deintercalation process.

DFT 확산 방식의 OFDM 통신 시스템에서 위상잡음과 직교 불균형 보상 (Compensation of Phase Noise and IQ Imbalance in the OFDM Communication System of DFT Spreading Method)

  • 유상범;유흥균
    • 한국전자파학회논문지
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    • 제20권1호
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    • pp.21-28
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    • 2009
  • DFT(Discrete Fourier Transform) 확산 방식의 OFDM(Orthogonal Frequency Division Multiplexing) 통신 시스템은 PAPR(Peak-to-Average Power Ratio) 저감에 매우 효과적인 시스템이며, 3GPP LTE($3^{rd}$ Generation Partnership Project Long Term Evolution)의 상향 링크에 SC-FDMA(Single Carrier-Frequency Division Multiple Access)에 사용된다. SC-FDMA는 일반적으로 OFDM 시스템보다 위상잡음과 직교 불균형으로 인한 ICI(Inter-Carrier Interference)에서 더 성능 열화가 발생하며, 등화기에 심각한 영향을 미친다. 그러므로 본 논문에서는 상향 링크에서 신호 전송 시 발생하는 위상잡음과 직교 불균형(IQ Imbalance: In-phase/Quadrature Imbalance), 그리고 전력 증폭기(HPA: High Power Amplifier)의 백-오프 특성에 따른 영향을 분석하고, ICI 성분을 제거할 수 있는 효과적인 등화 알고리듬을 제시한다. 제안된 등화기는 FDE(Frequency Domain Equalizer) 방식을 기반으로 설계하였으며, 기존의 PNS(Phase Noise Suppression) 알고리듬을 FDE에 사용될 수 있도록 수정하고 개선하여 위상 잡음과 직교 불균형으로 인한 ICI를 보상한다. 시뮬레이션 결과를 통하여 back-off 5.5 dB 상태에서 위상 잡음 $0.06\;rad^2$, 위상 에러 5도, 진폭 에러 0.005인 경우, 위상 잡음과 직교 불균형을 보상하여 SNR=14 dB 정도에서 $BER=10^{-4}$의 성능을 만족할 수 있다.

WT 평면에서의 두 신호 시지연 추정 (Time Delay Estimation of Two Signals in Wavelet Transform Domain)

  • 김재국;이영석;김성환
    • 한국음향학회지
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    • 제16권4호
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    • pp.5-10
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    • 1997
  • 본 논문에서는 웨이브렛 변환을 이용한 새로운 시지연 추정방법인 WTD-LMSTDE을 제안하였다. 이 방법은 시평면에서 입력 신호 자기상관 행렬의 고유치 분포를 줄임으로서 수렴속도를 향상시켰다. 이 알고리즘의 성능을 시불변과 시변인 경우에 대해서 평가하였다. 결과로서 시불변 시지연의 경우에, WTD-LMSTDE의 추정 정확도가 LMSTDE보다 SNR에 따라서 3.3%에서 12.5%까지 개선되었다. 시변 시지연의 경우에는, 선형적으로 증가하는 자연 환경에서 WTD-LMSTDE의 평균 오차 전력이 잡음이 없는 상태에서 LMSTDE와 비교하여 2.4dB정도 감소하였다. 결론적으로 WTD-LMSTDE의 성능이 LMSTDE보다 우수함을 확인할 수 있었다.

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2D 및 3D DCT를 활용한 포인트 클라우드 압축 비교 실험 (Comparative Experiment of 2D and 3D DCT Point Cloud Compression)

  • 남귀중;김준식;한무현;김규헌;황민규
    • 방송공학회논문지
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    • 제26권5호
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    • pp.553-565
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    • 2021
  • 포인트 클라우드는 3D 오브젝트를 표현하기 위한 점들의 집합으로 3D 좌표 정보인 기하 정보와 색상, 반사율 등을 나타내는 속성 정보로 이루어져 있으며, 이러한 표현 방식으로 인해 2D 영상에 비해 방대한 양의 데이터를 가진다. 따라서, 포인트 클라우드 데이터를 전송하거나 다양한 분야에서 활용하기 위해서 포인트 클라우드 데이터를 압축하는 과정이 필수적으로 요구된다. 포인트 클라우드는 2D 영상과 같이 해당 영상을 구성하는 2D 기하 정보에 대응하는 색상 정보가 모두 존재하는 것과 달리, 3D 공간 중 일부만이 색상과 같은 속성 정보를 포함하여 포인트 클라우드를 표현하고 있기에, 기하 정보에 대한 별도의 처리도 요구된다. 이와 같은 포인트 클라우드의 특징을 기반으로 고밀도 포인트 클라우드 데이터의 압축 방안으로 국제 표준화 기구 ISO/IEC 산하 MPEG에서는 포인트 클라우드 영상을 사영한 뒤 2D DCT 기반의 2D 영상 압축 코덱으로 압축하는 V-PCC 를 표준화 중에 있다. 해당 표준은 3D 포인트 클라우드를 2D로 변환하여 압축을 진행하기에 3D 공간 정보를 정확하게 표현하기에는 한계가 존재한다. 이에, 본 논문에서는 포인트 클라우드 정지영상을 3D 상에서 3D DCT로 변환하여 포인트 클라우드 데이터를 압축하는 방안인 3D Discrete Cosine Transform based Point Cloud Compression을 제시하고, 2D DCT 기반의 V-PCC와 비교하여 3D DCT의 효율성을 확인하고자 한다.

SPUTTER-DEPOSITION OF CARBON NITRIDE FILMS WITH HIGH NITROGEN CONCENTRATION

  • Taki, Yusuke;Takai, Osamu
    • 한국표면공학회지
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    • 제29권5호
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    • pp.498-504
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    • 1996
  • The synthesis of carbon nitride thin films with high nitrgen concentration was accomplished by reactive supttering at relatively high working pressure. In conventional reactive sputter-deposition of carbon nitride films, working pressure was 0.3-5Pa and the ratio of nitrogen to carbon(N/C ratio) in the films was less than 0.5. In this study, amorphous carbon nitride films with the N/C ratio $\tickapprox$ 1.0 were prepared on Si(100). substrates at higher pressure, 20-60 Pa. Structural analyses with Fourier transform infrared spectroscopy and X-ray photoelectron spectroscopy revealed that the films prepared consisted of triazine-like plain network.

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