• 한국결정학회지
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• 제6권1호
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• pp.27-35
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• 1995

1-tert-butoxycarbonyl-4-[N-(tert-butoxycarbonyl)-N-(ethoxycarbonylmethyl)amino]-3-phenylsulfonylpyrrolidind [C24H36O8N2S;이하 BEP]의 분자 및 결정구조를 X-선 회절법으로 연구하였다. 이 결정의 분자는 C24H36O8N2S, 삼사정계이고 공간군은 P1이다. 단위세포 길이는 a=11.363(8)Å, b=11.589(6)Å, c=11.013(10)Å,α=95.32(6)°,β=98.64(7)°,γ=79.57(5)°,V=1406.8(18)Å3, t=293K, Z=2이다. 구조해석에 사용한 X-선은 CuKα선(λ=1.5418Å)을 사용하였다. 분자구조는 직접법으로 풀었으며 최소자승법으로 정밀화하였다. 최종 신뢰도 R값은 F≥4 σ(F)인 3621개의 회절반점에 대하여 R=9.78% 이었다.

• 한국임상수의학회지
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• 제12권1호
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• pp.799-818
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• 1995

This study was performed to examine the general anesthetic efficacy of tiletamine-zolazepam, a mixture of phencyclidine-derived tiletamine and benzodiazepine-related zolazepam. The antagonistic activities of doxapram and yohimbine to the anesthetic effects of tiletamine-zolazepam were also studied. Thirty healthy mongrel dogs were divided into three groups (each of 10) twenty minutes after being anesthetized with tiletamine-zolazepam : T-Z-S group(tiletamine-zolazepam-saline), T-Z-D group (tiletamine -zolazepam-doxapram), T-Z-Y group (tiletamine-zolaz.pam-yohim bine). Various parameters wert evaluated in terms of the onset and recovery time of analgesia, respiration rates, hear rates, body temperature, electrocardiogram, blood chemistry, and lymphocyte blastogenesis. The results obtained through these experiment could be summarized as follows: 1. he anesthetic efficacy of tiletamine-zolazepam was considered desirable, with the onset time of anesthesia being as short as 0.23-0.24 minutes. 2. Both of the antagonistic effects of yohimbine and doxapram on the anesthesia induced by liletamine-zolazepan were evaluated statistically significant(p<0.05) as the recovery time was shortened from 39.3$\pm$4.9 min(T-Z-S group) to 25.3$\pm$2.9 nin(T-Z-Y group) and 29.9$\pm$8.8min(T-Z-D group), respectively. 3. Respiration rates were not changed by the treatments of both doxapram and yohimbine, with the only transient increase in the T-Z-D group. The changes in the respiration rate were not observed during the whole time course of the experiment. 4. Yohimbine(T-Z-Y group) increased the heart rate significantly from 30 minutes after the adminstration compared to the T-Z-S group and T-Z-D group (p<0.05). 5. The decreases in th, body temporature were observed from 30 minutes in the T-Z-S group(p<0.05) and 40 minutes in th, T-Z-D group(p<0.05), after the adminstration. On the other hand, there was no hypothermia in the T-Z-Y group. 6. In the all experimental groups of the T-Z-S, T-Z-D and T-Z-Y, there were no specific findings on the electrocardiograph incept slight shift to the tachycardia in all cases. 1. We could not find any differences in the blood chemistry between all experimental groups (T-Z-S, T-Z-D and T-Z-Y). 8. the inhibition of the lymphocyte blastogenesis shown in the T-Z-S with 3 hours decreasing and thereafter restoring to the normal values up to the point 5 hours were not occurred in the T-Z-D and T-Z-Y groups. With the above results, we could conclude that both doxapram and yohimbine can be clinically used as recovery agents towards anesthesia by tiletamine- zolazepam fi:on the efficacy point of view, but yohimbine is more recommendable in this case if considering the recovery time and lymphocyte blastogenesis.

• Journal of Forest and Environmental Science
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• 제9권1호
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• pp.67-80
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• 1993

무공해 대체 펄프화법 개발의 일환으로 비교척 최근에 많은 연구가 이루어지고 있는 아세트산-물 용매 증해법을 이용하여 현사시나무와 소나무률 펄프화 하였다. 펄프 특성의 변화에서 현사시나무는 거의 모든 아세트산 충해초건에서 우수한 펄프화 경향을 보였지만 소나무는 저온에서 충해가 거의 일어나지 않았다. 현사시나무의 최적 중해조건은 중해농도 95%, 중해온도 $185^{\circ}C$, 증해시간 0.5hr이었다. 구성당 성분의 거동은 현사시나무와 소나무에서 glucose만이 소량 감소하는 반면 그외의 당성분들은 다량 용출되었다. 폐액중의 용출 아세트산 리그닌에 대한 기초척인 성질을 살펴본 결과 현사시나무의 아세트산 리그닌의 원소조성은 C가 63.88%, H가 5.45%, O가 30.67%이며 $C_9$의 formular는 $C_9H_{9.15}O_{3.24}$였고 소나무의 아세트산 리그닌의 조성온 C가 61.85%, H가 6.14%, O가 32.01% 이며 $C_9$의 formular는 $C_9H_{9.15}O_{3.50}$이었으며 두 수종의 아세트산 리그닌 중합 명균분자량은 현사시나무가 731이며 소나무는 725였다.

• Journal of Korean Neurosurgical Society
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• 제41권2호
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• pp.77-81
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• 2007

Objective : In a variety of thoracolumbar diseases, corpectomy followed by interbody bone graft and anterior instrumentation has allowed direct neural decompression and reconstruction of the weight-bearing column by short segments fusion. In this study, we compared spinal stability of the two different anterior thoracolumbar instruments : Z-plate and Kaneda device representing plate and two-rods type, respectively. Methods : A retrospective review was performed for all the patients with thoracolumbar diseases or traumas treated with anterior corpectomy, autologous iliac bone graft, and fixation with instruments from 1996 to 2000. For the anterior instrumentation, Z-plate or Kaneda device was used for 24 [M:F=5:9, average age=37] and 12 [M:F=9:3, average age=41] patients, respectively. The plain AP and lateral flexion-extension films were taken immediately after surgery and at each follow-up. The sagittal and coronal Cobb's angles at the operation segments were used to observe the change of initial fixation status. The surgical time length and bleeding amount of the two groups were compared. Intra-operative and post-operative instrument associated complications were evaluated. Student t-test was used for statistical analysis and p-value less than 0.05 was considered to be significant. Results : Mean follow-up durations for Z-plate and Kaneda device were 24 and 21 months, respectively. The fusion rate was 91% for Z-plate and 100% for Kaneda device. Two cases of Z-plate group showed instrumentation failure during the follow up period, in which additional surgery was necessary. The mean differences of sagittal Cobb's angles among the AP images immediate after surgery and at follow-up were 7 and 2 degrees for Z-plate and Kaneda device, respectively [p<0.05]. The mean differences of coronal Cobb's angles were 5 and 2 degrees for Z-plate and Kaneda device, respectively [p<0.05]. No Intra-operative complication has occurred in both groups. There was no difference in surgery time and bleeding amount between two groups. Conclusion : We think that Kaneda device [rod type] is stronger than Z-plate [plate type] to keep the spinal stability after anterior thoracolumbar surgery.

• 한국결정학회지
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• 제3권1호
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• pp.31-36
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• 1992

플루오로시노론 아세토나이드, C24H30F2O6, 삼사 정계, 공간군 R3(육방정계 단위세포), a=b=17. 896 A., c: 18365 ,3,, V=5094.3 A',2:9 A(MoK a) =0.7107 k, D-: 1.31 g/cm", D.: 1.328 g/cm", T=298 K,1101 개의 독립된 회절반점에 대한 최종신뢰도값 R=0.050. 분자구조는 관련된 코티코 스테로이드 화합물의 구조와 일치한다. 3회 회전 대칭 관계에 있는 세개의 분자가 수소결합에 의해 서로 연결되어, c-축에수직한 층을 형성한다.

• 한국초전도ㆍ저온공학회논문지
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• 제15권2호
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• pp.16-19
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• 2013

The magneto-resistivity and electric field-current density (E-J) curves were investigated up to a magnetic field 9 T in the optimally doped $BaFe_{1.8}Co_{0.2}As_2$ single crystal with a superconducting temperature ($T_c$) of 24.6 K. The E-J Scaling behaviors below and above vortex glass transition temperature ($T_g$) were found, confirming the existence of the vortex glass phase transition. The critical exponents for the diverging spatial and time correlations at $T_g$, were obtained as v = $1.1{\pm}0.1$ and z = $4.5{\pm}0.3$, respectively. The obtained critical exponents are in good agreement with the predicted values of v ~ 1 - 2 and z > 4 within the 3D vortex glass theory.

• Journal of Magnetics
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• 제21권1호
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• pp.20-24
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• 2016

Magnetic properties of bio-magnetic molecule ferritin have been investigated. Two ferritin samples were synthesized under different magnetic fields, 0 and 9.4 T, respectively. This work is focused on the influence of magnetic field on biomineralization process. While magnetization vs. temperature (M-T) data of both samples measured at 1000 Oe are almost identical except for low temperature region (T < 6 K), magnetization vs. field (M-H) data show noticeable difference. From an analysis of M-H data by using a modified Langevin function, we could extract the saturation magnetization $m_0$(T), the effective magnetic moment ${\mu}_{eff}$(T) and the linear susceptibility x(T). The difference between the samples is most prominent in the x(T), whereby the x(T) of the sample prepared at 9.4 T is 1.7 times bigger than that of the other. In addition, from hysteresis and relaxation measurements, we found the sample prepared at 9.4 T showed strikingly smaller coercivity and slower relaxation.

• Bulletin of the Korean Chemical Society
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• 제8권1호
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• pp.1-3
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• 1987

The crystal structure of $K_5Na_2[SbW_6O_{24}]{\cdot}12H_2O$ has been determined. Final R = 0.081 for 890 observed independent reflections collected by diffractometry. Crystal data as follows; trigonal, space group R3m, a = 9.794(1) ${\AA},\;{\alpha}$ = 84.72$(1)^{\circ}$, Z = 1. The heteropolyanion has a structure with point symmetry $D_{3d}$ (3m), of the ideal Anderson-type heteropolyanion. The Sb-W and W-W distances are 3.259(2) and 3.259(3) ${\AA}$. Three types of W-O ($W-O_t,\;W-O_b\;and\;W-O_c$) distances are 1.73(2), 1.95(4) and 2.20(3) ${\AA}$. The Sb-O distance is 1.97(3) ${\AA}$.

• 천문학논총
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• 제32권1호
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• pp.213-217
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• 2017

The recent updates of the North Ecliptic Pole deep ($0.5deg^2$, NEP-Deep) multi-wavelength survey covering from X-ray to radio-wave is presented. The NEP-Deep provides us with several thousands of $15{\mu}m$ or $18{\mu}m$ selected galaxies, which is the largest sample ever made at these wavelengths. A continuous filter coverage in the mid-infrared wavelength (7, 9, 11, 15, 18, and 24 µm) is unique and vital to diagnose the contributions from starbursts and AGNs in the galaxies out to z=2. The new goal of the project is to resolve the nature of the cosmic star formation history at the violent epoch (e.g. z=1-2), and to find a clue to understand its decline from z=1 to present universe by utilizing the unique power of the multiwavelength survey. The progress in this context is briefly mentioned.

• Pediatric Gastroenterology, Hepatology & Nutrition
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• 제16권4호
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• pp.254-260
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• 2013

Purpose: Recently, vitamin D insufficiency has increased and has been correlated to growth and puberty in children. This study was conducted to find the prevalence of subclinical vitamin D insufficiency and its influence on school-aged children in Korea. Methods: The subjects of this study were 397 children aged 7 to 15 years who had been tested for 25-OH vitamin D3 among the outpatients of the Department of Pediatrics in Eulji General Hospital from March 2007 to February 2011. Data for age, sex, comorbidities, serum 25-OH vitamin D3, height, weight, body mass index (BMI), and sunlight exposure time were collected before and after 3 months of vitamin D administration, retrospectively. Results: Vitamin D insufficiency was present in 343 (86%) of the subjects. In the vitamin D insufficient group, chronological age was $8.96{\pm}1.72$ years, mean height (z-score [z]) was $0.51{\pm}1.26$, mean BMI (z) was $0.81{\pm}2.20$, and bone age was $10.26{\pm}1.75$ years. In the vitamin D sufficient group, chronological age was $9.61{\pm}1.77$ years, mean height (z) was -$0.66{\pm}0.98$, mean BMI (z) was -$0.01{\pm}1.16$, and bone age was $9.44{\pm}2.12$ years. A paired t-test showed that three months after vitamin D administration, the mean 25-OH vitamin D3 level in the insufficient group increased to $24.38{\pm}10.03$ ng/mL and mean BMI (z) decreased to $0.67{\pm}1.06$. Conclusion: In Korean school-aged children, vitamin D insufficiency were relatively higher and may be closely related with higher BMI. Insufficient rise of the level of vitamin D after supplementation suggest the new supplementation guidelines, especially for Korean children.