• Title/Summary/Keyword: $WS_2$

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Cutting Efficiency and Mechanical Characteristics of Diamond Micro-blades Containing WS2 Lubricant (WS2 윤활제를 첨가한 마이크로 다이아몬드 블레이드의 절삭성능과 기계적 특성)

  • Kim, Song-Hee;Jang, Jae-Cheol
    • Journal of the Korean institute of surface engineering
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    • v.45 no.1
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    • pp.37-42
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    • 2012
  • $WS_2$ powder was added to the Cu/Sn bond metal of diamond micro-blades for machining of semi-conductor and IC chips to improve cutting efficiency. The effect of $WS_2$ additive on cutting efficiency was investigated and compared with the micro-blades with $MoS_2$ developed in previous research. Flexural strength, frictional coefficient, and wear resistance of blades decreased with $WS_2$ but wear depth increased. It was found that the blades including $WS_2$ consumed less momentary energy than the blades containing $MoS_2$ during dicing test. Micro-blades containing $WS_2$ exhibited lower flexural strength than the blades with $MoS_2$ resulting from higher amount of sintering defects relevant to the less effectiveness of $WS_2$ on fluidity. The effect of $WS_2$ and $MoS_2$ on fluidity during sintering was analyzed in terms of mismatching degree between the longitudinal direction of lubricant particles and the perpendicular direction to the compact loading. The blade with 8.1 vol.% of $WS_2$ showed the best cutting efficiency.

Synthesis of WS$_2$ Solid Lubricant and Its Application to the Ball Bearing (WS$_2$ 고체윤활제의 합성 및 구름베어링 적용)

  • 신동우;윤대현;최인혁;김경도
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 1998.04a
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    • pp.173-179
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    • 1998
  • The processing conditions for the synthesis of platelet WS$_2$ lubricant powder through the solid-gas reaction were optimized. The tungsten and sulfur powders were sealed in a vacuum of 10$^{-6}$ torr, prior to heat-treating at 850$\circ$C for 8 days. The react~on product showed the well-developed platelet WS$_2$ powder with an average size of 3.8 $\mu$m. The synthesized WS$_2$ powder was coated on the commercial deep grooved ball bearing (No. 6203) to examine the effects of WS$_2$ coating layer on the noise and endurance of the ball bearing. The level of noise obtained from WS$_2$ coated-ball bearing was higher (56 dB) than the value occurred in the case of greece (37 dB). The life-time of the ball-bearing assembled after coating WS$_2$ powder increased 50 times compared to the non-coated bali-bearing.

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Generation and Extension of Models for Repeated Measurement Design by Generalizability Design (일반화가능도 디자인에 의한 반복측정 실험설계의 모형 생성 및 확장)

  • Choi, Sung-Woon
    • Journal of the Korea Safety Management & Science
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    • v.13 no.2
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    • pp.195-202
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    • 2011
  • The study focuses on the Repeated Measurements Design (RMD) which observations are periodically made for identical subjects within definite time periods. One of the purposes of this design is to monitor and keep track of replicated records within regular period over years. This paper also presents the classification models of RMD that is developed according to the number of factors in Between-Subject (BS) variates and Within-Subject (WS) variates. The types of models belong to each number of factors: One factor is 0BS 1WS. Two factors are 1BS 1WS and 0BS 2WS. Three factors are 1BS 2WS and 2BS 1WS. Lastly, the four factors include model of 2BS 2WS In addition, the study explains the generation mechanism of models for RMD using Generalizability Design (GD). GD is a useful method for practitioners to identify linear model of experimental design, since it generates a Venn diagram. Lastly, the research develops three types of 1BS 2WS RMDs with crossed factors and nested factors. Those are random models, mixed models and fixed models and they are presented by using Generalizability Design, $(S:A{\times}B){\times}C$. Moreover, the example of applications and its implementation steps of models developed in the study are presented for better comprehension.

A Study on the DYC 4WS Control Method for Improving the Dynamic Characteristics of Vehicle (자동차의 주행성능 향상을 위한 DYC 4WS 제어방법에 관한 연구)

  • 김형내;김석일;김동룡;김건상
    • Transactions of the Korean Society of Automotive Engineers
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    • v.6 no.2
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    • pp.1-11
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    • 1998
  • The 4WS system is usually developed to improve the maneuverability at low speed and the straight line stability at high speed, but it is found to have the severe understeer characteristics at high speed. Therefore a 4WS vehicle requires to turn the steering wheel much more than a 2WS vehicle at high speeds even a driver goes through the same curved road. In this study, to enhance the cornering performance of the 4WS vehicle at high speed, a DYC 4WS system is proposed based on the nonlinear 4WS system and direct yaw moment control system. Especially the proposed DYC 4WS system is able to realize a zero side slip angle for vehicles and a cornering performance similar to the 2WS vehicle at high speed.

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Inhibition Effect of Environment-Friendly Agricultural Materials on Yellowish Kiwifruit Soft Rot Pathogen (Botryosphaeria dothidea) (친환경농자재의 황색참다래 과실무름병 병원균 억제 효과)

  • Moon, Doo-Gyung;Chung, Bong-Nam;Koh, Sang-Wook;Kim, Seong-Cheol;Joa, Jae-Ho
    • Korean Journal of Organic Agriculture
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    • v.24 no.2
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    • pp.253-262
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    • 2016
  • The SS (Bacillus subtilis 10%), WS (Microbial extract 70%), and DS (Sulfur 78%) agents were selected by mycelial growth inhibitory effect test against kiwifruit soft rot pathogen (B. dothidea) with 11 kinds of environment-friendly agricultural materials on PDA medium for 10 days. They showed at 94.2%, 65.2%, 58.9%, respectively. The control value of WS and SS agents were better than DS in storage experiment. It was effective SS and WS single application, DS-WS and WS-SS alternate application in the field trial.

Effects of Alternate-Week Feeding Strategies on Growth and Feed Efficiency Ratio of Juvenile Nile Tilapia Oreochromis niloticus in a Recirculating System

  • Cho, Sung-Hwoan
    • Fisheries and Aquatic Sciences
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    • v.8 no.3
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    • pp.128-131
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    • 2005
  • The effects of alternate-week feeding strategies on growth and feed efficiency ratio of juvenile Nile tilapia were investigated in a recirculating aquaculture system. Twenty fish initially weighing 25.5 g were randomly distributed into each of 18 tanks to conduct three replicates for each of six different feeding strategies. Weight gain of fish in the control that were fed daily for 6-week feeding trial was significantly higher than those of fish subjected to various alternate-week feeding regimes. Weight gain of fish that were starved for 3 weeks and then fed daily for 3 weeks (3WS+3WF) was not significantly different from that of fish, starved and fed daily for alternate 1-week period during the trial (1WS+1WF), but was significantly higher than those of fish starved for 2 weeks, and fed for 2 weeks (2WS+2WF); fish starved for 4 weeks and fed for 2 weeks (4WS+2WF); and fish fed for 5 weeks and fed for 1 week (5WS+1WF.) The amount of feed supplied to fish in the groups of 1WS+1WF and 3WS+3WF was significantly lower than that fed to fish in the control group, but significantly higher than the amount feed supplied to fish in the other three groups. Feed efficiency ratio for fish in the control group did not differ from that for fish in the groups of 1WS+1WF, 2WS+2WF and 3WS+3WF, but was significantly higher than that for fish in the groups of 4WS+2WF and 5WS+1WF. In conclusion, juvenile Nile tilapia that were subject to starvation for 1 to 5 weeks did not exhibit compensatory growth sufficient to attain the same weight as fish fed daily for 6 weeks. In addition, fish subjected to starvation exhibited low feed efficiency ratio compared to fish fed daily, which were probably attributable to poor weight gain.

Evaluation of Dicing Characteristics of Diamond Micro-blades with Cu/Sn Binder Including Etched WS2 Particles (표면 부식 처리한 WS2 입자를 첨가한 Cu/Sn계 다이아몬드 마이크로 블레이드의 절삭특성)

  • Kim, Song-Hee;Jang, Jaecheol
    • Journal of the Korean institute of surface engineering
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    • v.46 no.1
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    • pp.22-28
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    • 2013
  • $WS_2$ particles were added to micro-diamond blades with Cu/Sn binding metal as lubricants to improve cutting efficiency. It was found in previous works that the added $WS_2$ lubricant could reduce remarkably the momentary energy consumption during dicing tests but increased wear rate slightly owing to weak bonding between lubricant particles and bond metals. In the present work, the surface of $WS_2$ lubricant particles were etched for activating the surface of $WS_2$ particles that provide even distribution of particles during powder mixing process and improvement of wetting at the interfaces between $WS_2$ particles and molten Cu/Sn bond metals during pressurized sintering so that could provide the improved strength of micro-blades and result in extended life. Chipping behavior of workpiece with the types of micro-blades including $WS_2$ were compared because it is important in semiconductor and micro-packaging industries to control average roughness and straightness of sliced surface which is closely related with quality.

Mass-production of WS$_2$ Solid Lubricant and Its applications (WS$_2$ 고체윤활제의 양산 및 적용)

  • 신동우;최인혁;윤대현;김경도
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 1998.10a
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    • pp.221-226
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    • 1998
  • The processing conditions for the mass production of platelet WS$_2$ lubricant powder were optimized. The mixture of tungsten and sulfur powders was sealed in a vacuum of 10$^{-3}$ torr and heat-treated at 850$\circ$C for 2 h. The internal pressure of reaction chamber was maintained at certain level by controlling the release valve automatically. The reaction product was the platelet WS$_2$ powder with an average size of 15 $\mu$m. The synthesized WS$_2$ powder was then coated on the wiper-blade of automobiles and the commercial deep-grooved ball bearing using wet and dry coating methods, respectively. High lubricity and wear resistance of wet coated wiper-blade were confirmed by the life test of 70,000 cycles. The life-time of the ball bearing assembled after WS$_2$ coating onto each part increased 50 times compared to the non-coated ball bearing.

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Synthesis of $WS_2$ Solid Lubricant ($WS_2$ 고체 윤활제의 합성)

  • 신동우;윤대현;황영주;김성진;김인섭
    • Tribology and Lubricants
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    • v.13 no.4
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    • pp.60-65
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    • 1997
  • The tungsten disulfide $(WS_2)$ solid lubricant was synthesized by two different reaction processes, i.e., the reaction between $CS_2$ gas phase and solid $WO_3$powder, and the vapour phase transport method of tungsten and sulfur in a high vacuum. The chemical and physical characteristics of synthesized $WS_2$powder were analyzed in terms of the average particle size, morphology, crystalline phase etc. in comparison with those of commercial $WS_2$powder. The solid $WO_3$ powder with the average size of 0.2 ${\mu}{\textrm}{m}$ was reacted with $CS_2$gas flowed with$N_2$or 96%$N_2{\times}4%H_2$forming gas for 36 h and 24 h at 90$0^{\circ}C$ respectively. $WS_2$ crystalline phase was then formed through the intermediate phase of .$W_{20}O_{58}$ In the case of vapour phase transport method, the 3.5 wt% iodine was added as a vapour transport reagent into the composition of tungsten and sulfur powders maintaining a constant molar ratio of W:S=1:2.2. The mixture was then heat treated at 85$0^{\circ}C$ for 2 weeks in vacuum. The reaction product obtained showed the average size of 12 ${\mu}{\textrm}{m}$ and the hexagonal plate shape of typical solid lubricant with 2H-$WS_2$crystalline phase.

Factors Controlling Friction Coefficient of WS$_2$ Solid Lubricant (각종 응용환경에서 WS$_2$ 고체윤활제의 마찰 계수)

  • 신동우;윤대현;최인혁;김인섭
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 1997.10a
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    • pp.110-116
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    • 1997
  • The tribological behaviour of WS$_2$ solid lubricant was investigated using a ball-on-disk type tester. The WS$_2$ powder was spray-coated at room temperature and the effects of specimen configuration, atmosphere, applied load and rotating spccd on the friction coefficient was examined. WS$_2$ coated ball and disk showed the lowest friction coefficient of 0.05 in the nitrogen atmosphere under 0.3 kgf and 100 rpm, whereas relatively high coefficient of 0.1 - 0.15 was observed in air atmosphere. This confirmed that the spray-coated WS$_2$ solid lubricant was effective in reducing the friction coefficient and improving wear life in nitrogen atmosphere.

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