• Corrosion Science and Technology
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• 제11권2호
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• pp.48-55
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• 2012

Clamping force of a high strength bolt is reduced by a certain period of time after the initial set-up. In case of special treatments on faying surfaces such as protective coating, clamping force is relaxed more severely. Tests for slip critical joints subject to various faying surface parameters were conducted. Five different surface treatments were tested including mill scale surface, blast surface, rust surface and coated surfaces. Each specimen was composed of F10T M20 of high strength bolts and steel plates. Based on the result of slip coefficient test, blast treatment surface showed 0.59, rust treatment surface showed 0.54 and inorganic zinc treatment surface exhibited 0.44. Clean mill treatment surface and red lead paint treatment surface were 0.23, 0.21 respectively. It is identified that the slip coefficient in Korean structural design guide should be determined for various surface conditions. Subsequently from long term relaxation test of ASTM A 490 high strength bolts, relaxation of no-coated surfaces such as blast, clean mill, rust treatment, the loss of initial clamping load was 10.5%, 13.6% and 7.9% for 1,000 hours, while the loss of initial clamping force was reached as 15.0%, 18.7% more than the required redundancy 10% in case of inorganic zinc and red lead painted treatment. It is required that the limit of relaxation on coated faying surface should be established separately for various surfaces.

• 한국자기학회지
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• 제6권5호
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• pp.294-297
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• 1996

Electrooptic 물질 $KTiOPO_{4}(KTP)$에 대하여 $^{31}P$ 핵자기공명을 수행하였다. 17.9 MHz의 공명 주파수에서 77-390 K 온도 범위내에서의 스핀-격자 완화 시간($T_{1}$) 측정으로부터 전도 기구의 변화에 따른 두 개의 상전이를 관측하였으며, 이에 따른 각 상에서의 활성화 에너지를 구할 수 있었다.

• 한국자기공명학회논문지
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• 제23권1호
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• pp.6-11
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• 2019

Parahydrogen induced hyperpolarization (PHIP) technique is extensively studied to increase the sensitivity of the conventional NMR spectroscopy and recently try to apply this advanced technique into the revolutionary future of the MRI. The other hyperpolarization technique, which is widely utilized, is DNP (Dynamic Nuclear Polarization)-based hyperpolarization one. Despite its great advances in these fields, it contains several drawbacks to overcome: fast relaxation time, expensive equipment is needed, long build-up time is required (several hours), and batch scale material is hyperpolarized. To overcome all those limitations, one can effectively harness the hyperpolarized spin state of parahydrogen. One important step for utilizing the spin state of parahydrogen is doing well-developed experiments of ALTADENA and PASADENA. Based on those concepts, we successfully obtain the hydrogenation signals of ALTADENA and PASADENA from styrene by using benchtop NMR spectrometer. Also those signals were conceptually analyzed and confirmed with different mechanisms. To our best knowledge, those experiments using 1.4T (benchtop NMR) is the first reported one. Considering these experiments, we hope that parahydrogen-based hyperpolarization transfer studies in NMR/MRI will be broadened in Korea in the future.

• Investigative Magnetic Resonance Imaging
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• 제21권1호
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• pp.1-8
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• 2017

Purpose: To investigate the exchange and redistribution of hyperpolarized $^{13}C$ metabolites between different pools by temporally analyzing the relative fraction of dual $T_2{^*}$ components of hyperpolarized $^{13}C$ metabolites. Materials and Methods: A dual exponential decay analysis of $T_2{^*}$ is performed for [1-$^{13}C$] pyruvate and [1-$^{13}C$] lactate using nonspatially resolved dynamic $^{13}C$ MR spectroscopy from mice brains with tumors (n = 3) and without (n = 4) tumors. The values of shorter and longer $T_2{^*}$ components are explored when fitted from averaged spectrum and temporal variations of their fractions. Results: The $T_2{^*}$ values were not significantly different between the tumor and control groups, but the fraction of longer $T_2{^*}$ [1-$^{13}C$] lactate components was more than 10% in the tumor group over that of the controls (P < 0.1). The fraction of shorter $T_2{^*}$ components of [1-$^{13}C$] pyruvate showed an increasing tendency while that of the [1-$^{13}C$] lactate was decreasing over time. The slopes of the changing fraction were steeper for the tumor group than the controls, especially for lactate (P < 0.01). In both pyruvate and lactate, the fraction of the shorter $T_2{^*}$ component was always greater than the longer $T_2{^*}$ component over time. Conclusion: The exchange and redistribution of pyruvate and lactate between different pools was investigated by dual component analysis of the free induction decay signal from hyperpolarized $^{13}C$ experiments. Tumor and control groups showed differences in their fractions rather than the values of longer and shorter $T_2{^*}$ components. Fraction changing dynamics may provide an aspect for extravasation and membrane transport of pyruvate and lactate, and will be useful to determine the appropriate time window for acquisition of hyperpolarized $^{13}C$ images.

• 한국주조공학회지
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• 제14권5호
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• pp.412-418
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• 1994

Efficient algorithm for the solidification simulation by FDM is described from the practical point of views. If a proper time step ${\Delta}t$ is selected, the calculation is accelerated by implicit algorithm with the temperature recovery method of latent heat method. The implicit routine in the calculation is processed by SOR method(relaxation factor＝1.5, truncation error＝$10^{-4}$). The calculation is more accelerated by linear-interpolated explicite algorithm with a time step larger than the minimum value of the time step. This explicit method, which is applicable to the practical casting simulation problems, produces almost same results with about 40% faster calculation speed compared with the conventional explicit method.

• Investigative Magnetic Resonance Imaging
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• 제6권1호
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• pp.35-40
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• 2002

목적 : 새로운 개념의 macromolecular MR 조영제를 개발하여 자기이완적 특성 및 조직특이성 조영제로서의 가능성을 탐색해 보고자 하였다. 대상 및 방법 : Phthalocyanine (PC)을 상자성 원소의 배위자로 선택하였다. 2.01g (5.2 mmol)의 Phthalocyanine을 0.37 g(1.4mmo1)의 Mn chloride와 $310^{\circ}C$에서 36시간동안 반응시킨 후 혼합물을 크로마토그래피(CHC13/CH3OH 98/2 v/v, Rf, 0.76)로 정제하여 1.04 g (46%)의 MnPC (분자량 2000)를 얻었다. 0.1 mM로 희석시킨 MnPC를 1.5T(64MHz) MR 장비를 이용하여 T1/T2 자기이완율을 측정하였다. MnPC의 MR 영상 특성을 알아보기위해 1.5T MRI에서 스핀반향 기법(TR/TE= 500/14 msec)과 경사에코 기법중 FLASH 기법(TR/TE=80/4 msec, flip angle=60)을 사용하여 매 10분 간격으로 최고 4시간까지 연속적으로 토끼의 간에서 영상을 획득하였다. 농도별 차이를 알아보기위해 MnPC를 20 mM, 50 mM, 100 mM로 희석하여 사용하였다. 결과 : MnPC의 1.5 T(64 MHz)에서의 자기이완율은 Rl : 7.28 $mM^{-1}S^{-1}$, R2=55.56 $mM^{-1}S^{-1}$으로 small molecular weight 조영제인 Gd-DTPA의 Rl(=4.8 $mM^{-1}S^{-1}$), R2(=5.2 $mM^{-1}S^{-1}$) 값과 비교할 때 T1/T2 자기이완율이 매우 컸다. 스핀반향과 FlASH 기법 모두에서 조영증강은 조영제 주사후 약 10분 정도에 최고치에 달한 후 약 2시간 정도까지 유지하였다. MnPC는 small molecular weight의 간특이성 조영제들인 Gd-EOB-DTPA, Gd-BOPTA 및 MnDPDP과 비교할 때 조명증강을 유지하는 시간이 훨씬 더 긴 특성을 보였다. MnPC는 시간 경과에 따라 담도로 배출되었다. 결론 : 새로운 종류의 macromolecular MR agent인 MnPC를 자체 개발하였고 자기이완율을 측정한 결과 T1/T2 효과가 기존의 small molecular Gd-chelate에 비해 매우 큼을 알 수 있었다. MnPC는 간세포에 흡수된 후 담도계로 배출되는 간특이성 조영제임을 확인하였다.

• 한국학교보건학회지
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• 제14권1호
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• pp.145-160
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• 2001

The main purpose of this study is to identify the effects of a structured nursing intervention program on dysmenorrhea in middle school girls. This study employed two methods of research at the same time: a quasi-experiment pre- and post-test to use for comparison. Subjects were middle school girls assigned to the research program: 40 girls in the second grade, 40 girls in the third grade at K Girls' Middle School and H Girls' Middle School located in J city. The data were collected for 68 days from August 23 to October 30, 1999. The data were collected by observation technique and by a self-administered questionnaire. The instruments used for this study were as follows: the "Face Interval Pain Scale" menstrual pain instrument developed by McGreth(1987) and the "Menstrual Distress Questionnaire" dysmenorrhea instrument developed by Moos(1968). The dysmenorrhea knowledge instrument was developed by the researcher and refered to above. The research procedure was as follows: after preliminary examination, the experimental groups were provided educational programs with O.H.P. films developed by the researcher and with the videotape "first meeting" supported by P&G company and produced by EBS. The groups followed the educational programs twice for two weeks. At the beginning of menstruation, these subjects could choose one among the following choices: * Jacobson's progressively muscle relaxation method and massage treatment * Jacobson's progressively muscle relaxation method and hot bag treatment * Jacobson's progressively muscle relaxation method, a pain killer treatment, and massage treatment * Jacobson's progressively muscle relaxation method, a pain killer treatment, and hot bag treatment The dysmenorrhea of the control group were measured during the same period. The analysis of the collected data was done using an SPSS-PC+, descriptive statistic including real numbers, percentage, averages, standard deviations and t-test, $x^2$ test, and ANCOVA. The results of this study were as follows. (1) The knowledge level of the girls provided with the planned nursing intervention program was higher when compared to these who did not follow the educational programs. (2) The original difference in the dysmenorrhea level having been controled, the dysmenorrhea level made, nevertheless, a statistical difference between the experimental group and the control group(F=63.8, p=.00). Observed pain on quantity measurement of dysmenorrhea showed significant difference depending on the treatment(t=4.6, p=.00). In conclusion, those in the planned nursing intervention program had a higher knowledge level and fewer symptoms than the control group. Accordingly, the nursing intervention program for dysmenorrhea developed by the researcher can be effectively applied in nursing practice and can be the foundation for this kind of program.

• Investigative Magnetic Resonance Imaging
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• 제2권1호
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• pp.67-72
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• 1998

자기공명 영상의 의학적 이용에서 T2이완시간의 화소별 영상화(T2 이완 영상)는 병변의 정량적 진단도구로서 제안된 바 있다. NMR의 물리/화학적 이용에서 T2 이완시간의 측정으로서 CPMG(Carr-Pucell-Meiboom-Gill) 펄스열이 가장 효과적으로 인정되고, 쓰이고 있으나, 선형자계를 가하는 MR 영상화 장비에서는 측정된 다른 TE의 영상들을 이용한 T2 이완시간의 영상화 자체에 대한 복잡한 계산을 영상기기에서 수행에 문제가 있고, 일반적으로 최대 4개의 CPMG 에코를 영상화하는 펄스열이 제공되어 있다. 좀더 정확한 T2 이완영상화를 위하여 적어도 8개의 다른 반향시간 TE를 가진 영상들을 필용로 하므로, MR 영상화 장비사에서 제공된 펄스열을 이용하면, 적어도 두번 이상의 영상화를 하여야한다. 이는 TR을 2500msec로 할 때 적어도 15분 정도의 시간이 걸리며, 이 동안 환자의 약간의 움직임, 특히 각 4개 단위의 영상화 사이에 움직임에 의한 임의적 잡음이 계산될 T2 영상에 큰 영향을 미친다. 이 연구에서는 시뮬레이션에 의하여 1, 5, 10% 의 이론적인 임의 잡음을 포함한 영상들을 이용하여 잡음이 T2 영상의 작성에 미치는 영향을 연구하였다. 그리고 4개 에코 펄스열을 이용하여 세 번의 영상화로 12개의 영상을 얻고, 이들로부터 4개, 8개의 다른 TE를 가진 영상들을 선택하여 T2 영상을 계산하였다. 그리고 이 연구에서 개발된 8에코 CPMG펄스열로 한 번에 얻은 8개의 영상을 이용한 T2 이완 영상과 결과를 비교하였다. 잡음이 클수록 실제치보다 T2가 길었고, 8-에코 펄스열은 영상화하는 동안에 환자의 움직임을 줄여서 더 정확한 T2 이완 영상을 만들수 있었다.

• 한국조명전기설비학회:학술대회논문집
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• 한국조명전기설비학회 2004년도 춘계학술대회 논문집
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• pp.502-505
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• 2004

The purpose of this experiment is to modify diagnosis criterion of isothermal relaxation current(IRC) measurement equipment which is using for distribution cable diagnosis. We're using this system for several years in the field instead of DC leakage current measurement and lots of cables were replaced. But we have to investigate on the reliability of this equipment for our cables because we didn't carried out condition assessment of extracted cables after field diagnosis by this equipment. It is important thing for cable maintenance. If the replacement criterion is improper we can not prevent failures or will waste budget on account of replacement of the sound cables. In this papar we selected field installed cables and injected silicone fluid to the cables for insulation rehabilitation. In order to prove reliability of the diagnosis equipment we compared diagnosis results and AC breakdown strength according to operating time after silicone treatment. This is the results of the field test for 1 year.

• 대한전기학회논문지:전기물성ㆍ응용부문C
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• 제53권5호
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• pp.258-263
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• 2004

The purpose of this experiment is to modify diagnosis criterion of isothermal relaxation current(IRC) measurement equipment which is using for distribution cable diagnosis. We're using this system for several years in the field instead of DC leakage current measurement and lots of cables were replaced. But we have to investigate on the reliability of this equipment for our cables because we didn't carried out condition assessment of extracted cables after field diagnosis by this equipment. It is important thing for cable maintenance. If the replacement criterion is improper we can not prevent failures or will waste budget on account of replacement of the sound cables. In this paper we selected field installed cables and injected silicone fluid to the cables for insulation rehabilitation. In order to prove reliability of the diagnosis equipment we compared diagnosis results and AC breakdown strength according to operating time after silicone treatment. This is the results of the field test for 1 year.