• Title/Summary/Keyword: $Sb_2S_3$

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High Temperature Fade Behavior of Brake Friction Materials at Extreme Braking Conditions (실험통계법을 이용한 마찰재의 고온 마찰특성에 대한 고찰)

  • Ko, Kil-Ju;Park, Sang-Jin;Jang, Ho
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2001.11a
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    • pp.117-126
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    • 2001
  • Tribological properties of high temperature fade were investigated by changing relative amounts of ingredients in the brake friction material. Based on a simple experimental formulation containing 10 ingredients, friction materials were tested using a pad-on-disk type friction tester. Twenty-five friction material specimens with different relative amounts of the ingredients were manufactured according to the constrained mixture design .The difference ($\Delta$${\mu}$=${\mu}$$\sub$max/. -${\mu}$$\sub$min/. ) of friction coefficients was measured to represent the high temperature fade. Results from elevated temperature tests showed that five ingredients including cashew, graphite, Sb$_2$S$_3$, ZrSiO$_4$, and Cu fibers played important roles on $\Delta$${\mu}$. In order to find relative importance on fade phenomena among these ingredients, ANOVA(analysis of variance) was performed in this investigation. Thirty-two friction material specimens by changing ${\pm}$50vol.% of these five ingredients were tested to examine the relative importance. Results showed that cashew, graphite '||'&'||' Sb$_2$S$_3$, and cashew '||'&'||' graphite aggravated the fade behavior and Cu fibers improved on fade resistance.

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Experimental Investigation on Friction Performance of Brake Linings with Two Different Solid Lubricants (두 종의 고체윤활제에 따른 마찰재의 마찰성능에 관한 실험적 고찰)

  • Kim, Seong-Jin;Bae, Eun-Gap;Yoon, Ho-Gyu;Jang, Ho
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2001.06a
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    • pp.72-78
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    • 2001
  • An experimental investigation was conducted to examine the tribological behavior of NAO (non-asbestos organic) type brake linings containing different volume ratios of graphite and antimony trisulfide (Sb$_2$S$_3$). In order to investigate the effect of the solid lubricants on brake performance, three different friction tests (pressure, speed, and temperature sensitive tests) were carried out using a scale dynamometer. The test results showed that the friction characteristics were strongly affected by the type and the amount of solid lubricants in the brake lining. It was found that the brake linings with both solid lubricants were better in friction stability due to the complementary role of the two disparate lubricating properties at various pressure and speed conditions. In particular, the brake lining containing higher concentrations of graphite showed better fade resistance than others during high temperature friction test.

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Changes in Nutritional Composition of Gryllus bimaculatus Fermented by Bacillus sp. and Mycelium of Basidiomycetes (고초균 및 버섯 균사체를 이용하여 발효한 쌍별귀뚜라미 발효물의 단백질 및 무기질 성분 변화)

  • Jang, Hyun Wook;Choi, Ji Ho;Park, Shin Young;Park, Bo Ram
    • Journal of the Korean Society of Food Culture
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    • v.34 no.6
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    • pp.785-792
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    • 2019
  • This study examined the changes in the protein and mineral composition of Gryllus bimaculatus fermented with Bacillus substilis and the mycelia of Basidiomycetes. Normal Gryllus bimaculatus (S) and experimental group data obtained after an inoculation of Bacillus substilis (SC) (KACC 19623), Pleurotus eryngii (SP) and Cordyceps millitaris (SC) were compared. The crude protein content of the Gryllus bimaculatus (control) was 75.48%, but it decreased to 64.55, 54.32, and 63.53% after fermentation with SB, SP and SC, respectively (p<0.05). An analysis of the organic elements showed that the contents of the carbon and nitrogen sources were also reduced after fermentation, and the most significant decrease was observed after fermentation with SP. In SDS-PAGE, a 120 kDa and a 48 kDa protein of Gryllus bimaculatus were found. On the other hand, protein bands faded after fermentation with SP and SC, respectively. Moreover, no visible band was observed after fermentation with SB. According to amino acid analysis, the total free amino acid content increased 3.84 and 1.74 times after fermentation with SB and SP, respectively, compared to the corresponding baseline data. In contrast, it decreased by 0.52 times after fermentation with SC. Among the essential amino acids found in crickets fermented with SB, the valine and isoleucine content was 3.57 and 2.64 times higher, respectively, than the recommended daily amount of essential amino acids.

A STUDY ON FRACTURAL BEHAVIOR OF DENTIN-RESIN INTERFACE (상아질-복합레진 접착계면의 파괴거동에 대한 연구)

  • Ryu, Gil-Joo;Choi, Gi-Woon;Park, Sang-Jin;Choi, Kyung-Kyu
    • Restorative Dentistry and Endodontics
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    • v.32 no.3
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    • pp.208-221
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    • 2007
  • The fracture toughness test is believed as a clinically relevant method for assessing the fracture resistance of the dentinal restoratives. The objectives of this study were to measure the fracture toughness $(K_{1C})$ and microtensile bond strength of dentin-resin composite interface and compare their relationship for their use in evaluation of the integrity of the dentin-resin bond. A minimum of six short-rod specimens for fracture toughness test and fifteen specimens for microtensile bond strength test was fabricated for each group of materials used. After all specimens storing for 24 hours in distilled water at $37^{\circ}C$, they were tensile-loaded with an EZ tester universal testing machin. Statistical analysis was performed using ANOVA and Tukey's test at the 95% confidence level, Pearson's coefficient was used to verify the correlation between the mean of fracture toughness and microtensile bond strength. FE-SEM was employed on fractured surface to describe the crack propagation. Fracture toughness value of Clearfil SE Bond (SE) was the highest, followed by Adper Single Bond 2 (SB), OptiBond Solo (OB), ONE-STEP PLUS (0S), ScotchBond Multi-purpose (SM) and there was significant difference between SE and other 4 groups (p < 0.05). There were, however, no significant difference among SB, OB, OS, SM (p > 0.05). Microtensile bond strength of SE was the highest, followed by SB, OB, SM, OS and OS only showed significant lower value (p < 0.05). There was no correlation between fracture toughness and microtensile bond strength values. FE-SEM examination revealed that dentin bonding agent showed different film thickness and different failure pattern according to the film thickness. From the limited results of this study, it was noted that there was statistically no correlation between K1C and ${\mu}TBS$. We can conclude that for obtaining the reliability of bond strength test of dentin bonding agent, we must pay more attention to the test procedure and its profound scrutiny.

REALAP5/MOD3.1를 이용한 Semi-Scale Mod-2A실험의 모사

  • 안성수;장완호;김상녕
    • Proceedings of the Korean Nuclear Society Conference
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    • 1995.10a
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    • pp.462-468
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    • 1995
  • SB-LOCA, RCP Failure 등의 특정사고와 운전중의 과도현상의 발생시, 형성되는 자연대류의 PWR의 열수력학적 거동은 로심 잔열제거의 가능/불가능과 직결되므로 매우 중요한 PWR 안전성평가자료이다. 이러한 자료를 획득하기 위해, EG&G의 감독하에 수행된 Semiscale Experiment Program의 일부인 Semiscale Mod-2A실험들 중에서 S-NC-3과 5-NC-4를 REALAP5/MOD3로 모사하였다. 모사결과는 실험결과와 REALAP5/MODl을 이용한 모사결과와 비교 검토하였다.

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Study of the Relation between Quality and Image of the WholeGarment Knit Structured Patterns for High Sensible knit Design (1) - On mechanical property to armhole connecting part (Machi) - (고감성 니트디자인을 위한 무봉제 니트 조직패턴의 성능과 이미지간의 연구 (1) - 암홀 접속부(마치)의 역학적 특성을 중심으로 -)

  • Lee, Yoo-Jin;Choi, Won-Jung
    • Journal of Fashion Business
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    • v.16 no.1
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    • pp.52-68
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    • 2012
  • To achieve the aim of this study, 9 different types of samples were made to examine mechanical property according to structured pattern and type of Machi of pullover armhole of WholeGarment(seamless knitwear). With respect to samples, from which comparisons are made and anaylzed among basic characteristics of material, tensile strength & elongation and residual elongation due to repeated extension of armhole connecting part, the following conclusions could be obtained. It's revealed that the tensile strength of Machi part as being armhole connecting part of samples is more affected by Machi type than pattern structure. Of Machi types, it showed stronger tensile strength in the order of Normal(Normal Machi)< Machi_B(unilateral Machi)

Electrochemical properties of $TiO_2$/CNTs composite as anode materials for lithium secondary battery system (리튬이차전지용 음극물질 $TiO_2$/CNTs의 전기화학적 특성)

  • Oh, Mi-Hyun;Park, Soo-Gil
    • Proceedings of the KIEE Conference
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    • 2007.07a
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    • pp.1363-1364
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    • 2007
  • The composites such as Sn-CNTs, $SnSb_{0.5}$-CNTs and $CoSb_3$-CNTs have attracted much attention in the past years owing to their good overall properties. In these samples, intermetallic compounds show high specific capacities. Recently, interest in metal oxides such as $Al_{2}O_{3}$, MgO and $TiO_2$ has been largely stimulated by the realization that they can improve the cycling stability of the Li-ion battery electrodes. The reversible capacity of the $TiO_2$/CNTs composite reaches 168 mAh $g^{-1}$ at the first cycle and remains almost constant during long-term cycling. In this study, a nanocomposite of $TiO_2$/CNTs was prepared by sol-gel method and its electrochemical properties as anode materials for Li-ion batteries were studied by galvanostatic cycling, cyclic voltammograms (CV) and electrochemical impedance spectroscopy (EIS).

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Studies on the Preparation of $^{99m}TC$ Labelled Antimony Sulfide Colloid and Hydroxyethyl Starch for Lymphoscintigraphy (림포신티그래피용 $^{99m}TC$를 표지황화안티몬 콜로이드 및 전분의 제조에 관한 연구)

  • Park, Kyung-Bae;Awh, Ok-Doo;Kim, Jae-Rok;Lim, Sang-Moo;Hong, Seong-Woon
    • The Korean Journal of Nuclear Medicine
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    • v.23 no.1
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    • pp.71-83
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    • 1989
  • For the development of $^{99m}Tc-labelled$ antimony sulfide colloid and hydroxyethyl starch, various experiments such as preparation of colloid, control of the distribution of particle size, establishment of labelling conditions, determination of labelling yield and radiochemical purity, examination of stability, and organ imagings of rabbits etc. were carried out. 1) Antimony sulfide colloid was readily prepared by the reaction of aqueous solution of antimony potassium tartrate with hydrogen sulfide generated by treating ferrous sulfide with dilute sulfuric acid. The colloid could be stabilized by adding small amount of polyvinylpyrrolidone. 2) Electron microscopy analysis exhibited the distribution of colloid size in the range of $1\sim15nm$ with a major portion of 9 m. The colloid solution was sterilized by membrane filtration $(0.2{\mu}m)$ and then stored at $4^{\circ}C$. This sterilized colloid was so stable that it was usable at least for one year. 3) The antimony sulfide colloid was labelled by adding sodium $pertechnetate-^{99m}Tc$ solution to the reaction vial, followed by adding hydrochloric acid and then boiled for 30 min. The optimal pH of the reaction mixture was found to be in the range of $1.3\sim1.4$. Instant thin layer chromatography (ITLC) analysis showed high labelling yield of above 99.5%. This labelled colloid maintained high radio-chemical purity of above 99% until 10 hours after labelling. 4) Animal studies showed high uptake of $^{99m}Tc-Sb_2S_3$ colloid at lymph vessels and nodes indicating a suitable agent for lymphoscintigraphy. Satisfactory results were also abtained in other clinical studies. 5) Hydroxyethyl starch (HES $0.6\sim1.0%$) was labelled with $Na^{99m}TcO_4$ in the presence of $SnCl_2$ with high labelling yield of above 99.5%. The optimal pH of the reaction mixture was in the range of $1.8\sim2.0$. $^{99m}Tc-HES$ maintained high radiochemical purity of above 99% until 10 hours after labelling. 6) Animal studies showed that $^{99m}Tc-HES$ migrated more rapidly from the injection sites into the lymph vessels than $^{99m}Tc-Sb_2S_3$ colloid while less amount of the former was uptaken at lymph nodes than that of the latter. Similar phenomenon was also observed in other clinical studies. As a result, $^{99m}Tc-Sb_2S_3$ colloid was found to be more effective lymphoscintigraphic agent than $^{99m}Tc-HES$.

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The Fabrication and Electrical Properties of PMS-PZT Ceramics using a Tape Casting Method (Tape Casting법에 의한 PMS-PZT계 세라믹스 제조 및 전기적 특성)

  • Jung, Hyun-Jae;Na, Eun-Sang;Choi, Sung-Churl
    • Journal of the Korean Ceramic Society
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    • v.38 no.9
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    • pp.860-865
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    • 2001
  • After manufacturing 2mol% CdO substitute $0.05Pb(Mn_{1/3}Sb_{2/3})O_3-0.95Pb(Zr_{0.52}Ti_{0.48})O_3$ piezoelectric ceramics powder as starting material, to manufacture green sheets using Doctor Blade method. The optimum composition of slurry was studied. Moreover, the sintering properties and the dielectric and piezoelectric properties with variation a thickness of the manufactured sheets were investigated. The optimum of slurry was investigated by the rheology with addition of additives, the sintering condition was decided by TGA. And the properties of sheet were investigated through SEM. XRD. The optimum of slurry was the stablest at dispersant 3.0 wt% to solid loading 30vol%. After, at addition of binder/plasticizer(0.75/0.25) 3.0wt%, viscosity was 7.55Pa${\cdot}$s. The dielectric and piezoelectric properties of the sheet were increased a little with the increasing of sintering temperature but were not variable with variation of sheet thickness.

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Effects of Expanders in Manufacture and Microstructure of ZnO Varistor with $Al_2O_3$ (ZnO 바리스터의 제조에서 분산제 영향 및 $Al_2O_3$ 첨가에 따른 미세구조 연구)

  • Soh, J.J.;Han, S.W.;Kim, H.S.
    • Proceedings of the KIEE Conference
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    • 1995.11a
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    • pp.345-347
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    • 1995
  • ZnO varistor with composition of ZnO(90wt%)-$Bi_2O_3$(3wt%)-$Sb_2O_3$(3.61wt%)-$CO_2O_3$(1.16wt%)-NiO (0.88wt%)-$MnO_2$(0.71wt%)-$Cr_2O_3$(0.93wt%) according to $Al_2O_3$ addtive was fabricated by sintering methods. The optimal densification were established for the processing conditions of 8000 rpm 190$^{\circ}C$ spray drying and 1200$^{\circ}C$ 2hrs sintering. Then here investigated how additive compotions and processing variables affected the electrical and the phesical properties of these ZnO varistors.

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