• Title/Summary/Keyword: $Q_{10}$ coefficient

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Comparison of sample preparation methods for quantification of febantel, an anthelmintic agent, and its metabolites in rockfish (Sebastes schlegeli) muscle using liquid chromatography-tandem mass spectrometry (LC-MS/MS를 이용한 조피볼락 근육에서 구충제 febantel 및 그 대사체들의 정량분석을 위한 시료 전처리 방법의 비교 분석)

  • Lim, Jae-Woong;Kwon, Inyeong;Kim, Taeho;Kim, Wi-Sik;Kang, So Young
    • Journal of fish pathology
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    • v.34 no.2
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    • pp.261-269
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    • 2021
  • This study presents the evaluation of sample extraction and purification procedure for the determination of residues of febantel and its metabolites, fenbendazole, oxfendazole and oxfendazole sulfone in rockfish (Sebastes schlegeli) muscle using liquid chromatography-tandem mass spectrometry. Residues of febantel and its metabolites in rockfish muscle were analyzed using each different sample preparation method from Korean Food Standards Codex (KFSC), Food Safety and Inspection Service (FSIS, USA), and the modified FSIS method using QuEChERS kit (FSIS-Q), respectively. Each method was compared for mean recoveries and repeatabilities. Since FSIS-Q showed higher repeatabilities (coefficient of variation, CV of 2.4%~10.9%) than those of FSIS method (CV of 4.6%~17.5%), recoveries from FSIS-Q were compared with those from KFSC method. FSIS-Q showed significantly higher recoveries of 83.1%~110.1% (P < 0.05) than those from KFSC method of 64.7%~107.4%. In addition, FSIS-Q showed a good linearity over the range of 2.5~200 ㎍/kg, and excellent sensitivities with limit of detection of 0.46~0.71 ㎍/kg and limit of quantification of 1.08~2.15 ㎍/kg. Although all the sample preparation methods turned out to be able to meet CODEX guideline for all the compounds, FSIS method and FSIS-Q validated in this study could be applied to screening and quantification for residues of febantel and its metabolites in rockfish muscle with efficient preparation procedures.

EXTINCTION AND NON-EXTINCTION OF SOLUTIONS TO A FAST DIFFUSIVE p-LAPLACE EQUATION WITH A NONLOCAL SOURCE

  • Han, Yuzhu;Gao, Wenjie;Li, Haixia
    • Bulletin of the Korean Mathematical Society
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    • v.51 no.1
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    • pp.55-66
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    • 2014
  • In this paper, the authors establish the conditions for the extinction of solutions, in finite time, of the fast diffusive p-Laplace equation $u_t=div({\mid}{\nabla}u{\mid}^{p-2}{\nabla}u)+a{\int}_{\Omega}u^q(y,t)dy$, 1 < p < 2, in a bounded domain ${\Omega}{\subset}R^N$ with $N{\geq}1$. More precisely, it is shown that if q > p-1, any solution vanishes in finite time when the initial datum or the coefficient a or the Lebesgue measure of the domain is small, and if 0 < q < p-1, there exists a solution which is positive in ${\Omega}$ for all t > 0. For the critical case q = p-1, whether the solutions vanish in finite time or not depends crucially on the value of $a{\mu}$, where ${\mu}{\int}_{\Omega}{\phi}^{p-1}(x)dx$ and ${\phi}$ is the unique positive solution of the elliptic problem -div(${\mid}{\nabla}{\phi}{\mid}^{p-2}{\nabla}{\phi}$) = 1, $x{\in}{\Omega}$; ${\phi}(x)$=0, $x{\in}{\partial}{\Omega}$. This is a main difference between equations with local and nonlocal sources.

Synthesis of Forsterite with High Q and Near Zero TCf for Microwave/Millimeterwave Dielectrics

  • Ohsato, Hitoshi;Ando, Minato;Tsunooka, Tsutomu
    • Journal of the Korean Ceramic Society
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    • v.44 no.11
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    • pp.597-606
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    • 2007
  • With the advent of ubiquitous age, the high quality dielectric materials have been required for the wireless communications available to the millimeterwave as well as microwave frequencies. The utilizable region for the frequency has been expanding to the millimeter-wave region because of the shortage of radio frequency (RF) resources. These high frequencies would be expected for ultra high speed LAN, ETS and car anti-collision system on the intelligent transport system (ITS) and so on. Silicates are good candidates for microwave/millimeterwave dielectrics, because of their low dielectric constant ${\epsilon}_r$ and high quality factor (High Q). Forsterite ($Mg_2SiO_4$) is one of the silicates with low ${\epsilon}_r$ of 6.8 and Q f of 240000 GHz. In this paper, we reviewed following three categories for synthesis of forsterite: (1) Synthesis of high Q forsterite (2) Adjust the temperature coefficient of resonant frequency $TC_f$ (3) Diffusion of $SiO_{4^-}$ and Mg-ions on the formation of forsterite.

Evaluation of side resistance for drilled shafts in rock sections

  • Hsiao, Cheng-Chieh;Topacio, Anjerick J.;Chen, Yit-Jin
    • Geomechanics and Engineering
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    • v.21 no.6
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    • pp.503-511
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    • 2020
  • This study evaluated the side resistance of drilled shafts socketed into rock sections. Commonly used analysis methods for side resistance of piles in rocks are examined by utilizing a large number of load test data. The analysis of the unit side resistance of pile foundations embedded into rock sections is based on an empirical coefficient (α) and the uniaxial compressive strength (qu) or its root (${\sqrt{q_u}}$). The Davisson criterion was used to interpret the resistance capacity from the load test results to acquire the computed relationships. The α-${\sqrt{q_u}}$ relationship is proven to be reliable in the prediction of friction resistance. This study further analyzed the relationship by including the effect of rock quality designation (RQD) on the results. Analysis results showed that the analysis model of α-${\sqrt{q_u}}$-RQD provided better prediction and reliability considering the RQD classification. Based on these analyses, the side resistance of drilled shafts socked into rocks is provided with statistical data to support the analysis.

Prediction of Thermal Decomposition Temperature of Polymers Using QSPR Methods

  • Ajloo, Davood;Sharifian, Ali;Behniafar, Hossein
    • Bulletin of the Korean Chemical Society
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    • v.29 no.10
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    • pp.2009-2016
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    • 2008
  • The relationship between thermal decomposition temperature and structure of a new data set of eighty monomers of different polymers were studied by multiple linear regression (MLR). The stepwise method was used in order to variable selection. The best descriptors were selected from over 1400 descriptors including; topological, geometrical, electronic and hybrid descriptors. The effect of number of descriptors on the correlation coefficient (R) and F-ratio were considered. Two models were suggested, one model having four descriptors ($R^2$ = 0.894, $Q^2_{cv}$ = 0.900, F = 172.1) and other model involving 13 descriptors ($R^2$ = 0.956, $Q^2_{cv}$ = 0.956, F = 125.4).

A Study for the Viscous Flow of Sodium Chloride Through a Cuprophane Membrane

  • Jee Jong-Gi;Kwun Oh Cheun;Jhon Mu Shik;Ree Taikyue
    • Bulletin of the Korean Chemical Society
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    • v.3 no.1
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    • pp.23-30
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    • 1982
  • For the study of transport phenomena of an aqueous NaCl solution through a cuprophane membrane, a new apparatus was constructed. The volumc flow rate Q, the permeability coefficient U, and the permeability constant K were measured or determined by using this apparatus. The experimental temperature range was 5 to $35^{\circ}C$, and the applied pressure increments were 10 to 40 psi. By assuming that the cuprophane membrane is composed of n parallel cylindrical capillaries of circular cross-section and that the flow of the solution through the capillaries follows the Poiseulle law, the mean radius r of the capillaries and the number n of the latter in the membrane were evaluated. By using a reasonable assumption concerning the radius ${\eta}'$ of the species diffusing through the membrane, it was concluded that the contribution of the diffusive flow to the total flow rate Q is less than 10%. Thus, the Q was treated as the rate due to the viscous flow, and the viscosity ${\eta}_m$ of the solution in the membrane phase was evaluted, and it was found that ηm is nearly equal to ${\eta}_b$, the bulk viscosity of the solution. From this fact, it was concluded that in the capillaries, no change occurs in the physical state of the NaCl solution. The value of ( = 4.27 kcal/mole) and ${\Delta}Sm^{\neq}$(4.28 eu) were obtained for the viscous flow. A possible explanation was given.

A Stochastic Analysis of the Water Quality with Discharge Variation in Upper Nakdong River Basin (낙동강 상류 유역에서의 유량변동에 따른 수질의 통계학적 분석)

  • Choi, Hyun Gu;Han, Kun Yeun;Choi, Seung Yong
    • Journal of Environmental Impact Assessment
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    • v.20 no.6
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    • pp.833-843
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    • 2011
  • The purpose of this study is to analysis pollutant loading of upper Nakdong River basin according to the variation of discharge. The correlation between discharge and pollutant concentration and between discharge and pollutant loading were analyzed by statistical method, respectively. Regression equation of pollutant loading and discharge was represented as $L=_aQ^b$ in which L = pollutant loading(kg/day), and b = regression coefficients, and Q = discharge($m^3/day$). The correlation coefficient of study area was in range of 0.8428 to 0.9935. The SS was the highest b value 1.2856~1.7730 among water quality parameters because the pollutant loading of SS was much affected by flow. Additionally, the applicability of the regression equations was verified by comparing predicted results with observed value. The correlation coefficient of verification was in range of 0.8983 to 0.9987 and NSEC was in range of 0.7018 to 0.9960. Therefore the pollutant loading was good correlated with discharge. The main result will be used as basic data for water quality management and design of environment fundamental facilities.

3D-QSAR Studies of Tetraoxanes Derivatives as Antimalarial Agents Using CoMFA and CoMSIA Approaches

  • Liang, Taigang;Ren, Luhui;Li, Qingshan
    • Bulletin of the Korean Chemical Society
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    • v.34 no.6
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    • pp.1823-1828
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    • 2013
  • Tetraoxanes (1,2,4,5-tetraoxanes) have been reported to exhibit potent antimalarial activity. In the present study, the three dimensional-quantitative structure activity relationship (3D-QSAR) studies were performed on a series of tetraoxanes derivatives using comparative molecular field analysis (CoMFA) and comparative molecular similarity indices analysis (CoMSIA) techniques. The best predictive CoMFA model with atom fit alignment resulted in cross-validated coefficient ($q^2$) value of 0.719, non-cross-validated coefficient ($r^2$) value of 0.855 with standard error of estimate (SEE) 0.335. Similarly, the best predictive CoMSIA model was derived with $q^2$ of 0.739, $r^2$ of 0.847 and SEE of 0.344. The generated models were externally validated using test sets. The final QSAR models as well as the information gathered from 3D contour maps should be useful for the design of novel tetraoxanes having improved antimalarial activity.

Analysis of Magnetically Coupled Wireless Power Transmission Efficiency according to Material (주변 물질에 따른 자계결합 무선 전력 전송 시스템의 전송 효율 변화 연구)

  • Oh, TaekKyu;Lee, Bomson
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.25 no.3
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    • pp.304-310
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    • 2014
  • This paper presents the analysis of the coupling coefficient(k), Q value of the resonator, and the optimum loaded resistance at Rx for the magnetically coupled wireless power transmission using two loops(resonators). In addition, the metamaterial, conductor, and the relay methods have been used in order to improve the limitation problem of transmission efficiency by using the figure of merit. We have achieved the increase of transmission efficiency about 11~60 % using the proposed methods by analyzing and comparing the results based on EM simulations.

Accuracy Assessment of Global Land Cover Datasets in South Korea

  • Son, Sanghun;Kim, Jinsoo
    • Korean Journal of Remote Sensing
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    • v.34 no.4
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    • pp.601-610
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    • 2018
  • The national accuracy of global land cover (GLC) products is of great importance to ecological and environmental research. However, GLC products that are derived from different satellite sensors, with differing spatial resolutions, classification methods, and classification schemes are certain to show some discrepancies. The goal of this study is to assess the accuracy of four commonly used GLC datasets in South Korea, GLC2000, GlobCover2009, MCD12Q1, and GlobeLand30. First, we compared the area of seven classes between four GLC datasets and a reference dataset. Then, we calculated the accuracy of the four GLC datasets based on an aggregated classification scheme containing seven classes, using overall, producer's and user's accuracies, and kappa coefficient. GlobeLand30 had the highest overall accuracy (77.59%). The overall accuracies of MCD12Q1, GLC2000, and GlobCover2009 were 75.51%, 68.38%, and 57.99%, respectively. These results indicate that GlobeLand30 is the most suitable dataset to support a variety of national scientific endeavors in South Korea.