• Title/Summary/Keyword: $B_4C$ coating

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The Wear Resistance of Electroless Nickel and Electroless Composite(Ni-P-X, X: SiC, $Al_2$O$_3$, Diamond) Coating Layers (무전해 니켈도금과 무전해복합도금(Ni-P-X, X: SiC, $Al_2$O$_3$, Diamond)의 내마모성 비교)

  • Kim, M.;Chang, D. Y.;Jeong, Y. S.;Ro, B. H.;Lee, K. H.
    • Journal of the Korean institute of surface engineering
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    • v.27 no.4
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    • pp.193-206
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    • 1994
  • A wear behavior of electroless (Ni-P-X, X: SiC, $Al_2O_3$, Diamond) composite coating layers, formed under various conditions on commerical grade low carbon steel, has been investigated using Taber abrasion tester and scanning electron microscope. Several factors, which are type of particles, co-deposited content, particle size, distribution of particles and heat-treatment, influenced the wear resistance. The wear resistance of the composited coating layers after heat-treatment at $400^{\circ}C$ for 1 hr was increased 70 times with diamond, 15 times with SiC and 8 times with $Al_2O_3$, compared with the electroless nickel plating layer without heat-treatment.

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High-Temperature Fracture Strength of a CVD-SiC Coating Layer for TRISO Nuclear Fuel Particles by a Micro-Tensile Test

  • Lee, Hyun Min;Park, Kwi-Il;Park, Ji-Yeon;Kim, Weon-Ju;Kim, Do Kyung
    • Journal of the Korean Ceramic Society
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    • v.52 no.6
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    • pp.441-448
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    • 2015
  • Silicon carbide (SiC) coatings for tri-isotropic (TRISO) nuclear fuel particles were fabricated using a chemical vapor deposition (CVD) process onto graphite. A micro-tensile-testing system was developed for the mechanical characterization of SiC coatings at high temperatures. The fracture strength of the SiC coatings was characterized by the developed micro-tensile test in the range of $25^{\circ}C$ to $1000^{\circ}C$. Two types of CVD-SiC films were prepared for the micro-tensile test. SiC-A exhibited a large grain size (0.4 ~ 0.6 m) and the [111] preferred orientation, while SiC-B had a small grain size (0.2 ~ 0.3 mm) and the [220] preferred orientation. Free silicon (Si) was co-deposited onto SiC-B, and stacking faults also existed in the SiC-B structure. The fracture strengths of the CVD-SiC coatings, as measured by the high-temperature micro-tensile test, decreased with the testing temperature. The high-temperature fracture strengths of CVD-SiC coatings were related to the microstructure and defects of the CVD-SiC coatings.

Experimental brush wear pattern and cariostatic effect of Biscover (Biscover의 잇솔질에 따른 마모양상과 항우식 효과)

  • Oh, Eun-Ju;Park, Song-Soo;Jang, Mun-Ju;Jeon, Young-Mi;Kim, Jong-Ghee
    • The korean journal of orthodontics
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    • v.38 no.3
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    • pp.214-222
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    • 2008
  • Objective: The aim of this study was to investigate the experimental brush wear pattern of a light cured surface sealant, Biscover (Bisco, Schaumburg, IL), and to evaluate its cariostatic effect. Methods: Caries-free human premolars were used for the Biscover coating group (n = 90) and the control group (n = 10). The Biscover coating group was randomly assigned to nine subgroups of 10 each and the control group was assigned to two subgroups of 5 each according to the number of brushing strokes. An experimental 3-body wear test was conducted under different strokes of wear test. Tooth-brushing was accomplished with movement of each brush head set at a frequency of 100 rpm under a force of 1.5N, Surface roughness was tested before, and after Biscover coating, and after brushing. Then, each of the 10 teeth of both groups were placed in artificial caries inducing solution for 7 days. All tooth surfaces were assessed using scanning electron microscopy. Results: Biscover coated surfaces showed a smoother texture than enamel surfaces. The roughness was increased after experimental brushing and after 10,800 brushing strokes, the whole layer of Biscover wore out. However, teeth in the Biscover coating group had a cariostatic effect in cariogenic conditions. Conclusions: We suggest that white lesions in orthodontic patients can be suppressed by topical applications of Biscover.

Friction and Wear at Ceramic Coated Surfaces of Aluminum Alloy (알루미늄 합금표면에 코팅된 세라믹재의 마찰마멸 특성)

  • 공호성;권오관;김형선
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.17 no.12
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    • pp.3083-3093
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    • 1993
  • Friction and wear at ceramic coated surfaces of aluminum alloy were experimentally studied using a Ring-on-Block wear test machine. Ceramic materials coated on aluminum alloy surfaces were WC, CrC, $Al_{2}O_{3}$ by a plasma spray; and $Al_{2}O_{3}$,$Al_{2}SiO_{5}$, $Na_{2}B_{4}O_{7}$,$Na_{4}P_{2}O_{7}$, and $Al_{2}O_{3}-ZrO_{2}$ composite coating by an Anodic Spark Depositon. They were tested under the sliding wet contact and compared with aluminum alloys and steels. Test results showed that ceramic coated surfaces, in general, have better anti-wear property than those of aluminum alloys due to increase in the surface hardness ; however, they also showed higher coefficients of friction and changes in wear mechanisms, resulting in brittle fractures.

Assessment of UV Blocking Performance for Development of Converged Technologies of Vision Correcting Spectacle Lenses (시력교정용 안경렌즈의 융복합적 기술개발을 위한 UV차단 성능 평가)

  • Kim, Heung-Soo
    • Journal of the Korea Convergence Society
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    • v.9 no.4
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    • pp.93-98
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    • 2018
  • This study was wanted to confirm ability for UV blocking according to its material. The lenses materials were Acryl, CR-39, NK-55, and MR-8. It was grouped: Group A consisting of anti-scratch hard coated lenses and anti-refractive multi coated lenses, Group B added UV blocking coating on the group A, and Group C consisting of only UV blocking lenses. The results measured UV transmittance, On the UV-A wavelength, Group A showed the UV transmittance of 7.726%, 0.043%, 0.007%, and 0.007% respectively. Group B showed 0.038%, 0.037%, 0.007%, and 0.007%, respectively. The UV-blocking performance of CR-39 has been greatly improved. Group C has shown the best UV blocking function; only 0.005% and 0.004% of UV transmittances.(1.60 and 1.67 index of refraction respectively). For the low power of lenses and sunglasses, the CR-39 lens is the most used. Therefore, to UV blocking from the lens, new materials or UV absorbers or UV coating technology and development of Converged Technologies are required.

Strategic coating of NdFeB magnets with Dy to improve the coercivity of permanent magnets

  • Ucar, Huseyin;Parker, David S.;Nlebedim, I.C.;McCallum, R.W.;McCall, S.K.;Parans Paranthaman, M.
    • Advances in materials Research
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    • v.4 no.4
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    • pp.227-233
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    • 2015
  • We present a method, supported by theoretical analysis, for optimizing the usage of the critical rare earth element dysprosium in $Nd_2Fe_{14}B$ (NdFeB)-based permanent magnets. In this method, we use Dy selectively in locations such as magnet edges and faces, where demagnetization factors are largest, rather than uniformly throughout the bulk sample. A200 nm thick Dy film was sputtered onto a commercial N-38, NdFeB magnets with a thickness of 3 mm and post-annealed at temperatures from $600-700^{\circ}C$. Magnets displayed enhanced coercivities after post-annealing and as much as a 5 % increase in the energy product, while requiring a total Dy content of 0.06 wt. % - a small fraction of that used in the commercial grade Dy-NdFeB magnets. By assuming all Dy diffused into NdFeB magnets, the improvement in energy product corresponds to a saving of over 1% Dy (critical element). Magnets manufactured using this technique will therefore be higher performing which would potentially broaden the application space of these magnets in the traction motors of hybrid and pure electric vehicles, and wind generators.

Optimal Aluminizing Coating on Incoloy 909 (Incoloy 909 합금의 최적 알루미나이징 확산 코팅)

  • Kwon, S.W.;Yoon, J.H.;Joo, Y.K.;Cho, T.Y.;Ahn, J.S.;Park, B.K.
    • Journal of the Korean institute of surface engineering
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    • v.40 no.4
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    • pp.175-179
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    • 2007
  • An Fe-Ni-Co based superalloy Incoloy 909 (Incoloy 909) has been used for gas turbine engine component material. This alloy is susceptible to high temperature oxidation and corrosion because of the absence of corrosion resistant Cr. For the improvement of durability of the component of Incoloy 909 aluminizing-chromate coating by pack cementation process has been investigated at relatively low temperature of about $550^{\circ}C$ to protect the surface microstructure and properties of Incoloy 909 substrate. As a previous study to aluminizing-chromate coating by pack cementation of Incoloy 909, the optimal aluminizing process has been investigated. The size effects of source Al powder and inert filler $Al_O_3$ powder and activator selection have been studied. And the dependence of coating growth rate on aluminizing temperature and time has also been studied. The optimal aluminizing process for the coating growth rate is that the mixing ratio of source Al powder, activator $NH_4Cl$ and filler $Al_O_3$ are 80%, 1% and 19% respectively at aluminizing temperature $552^{\circ}C$ and time 20 hours.

Wear Resistance of c-BN Surface Modified 316L Austenitic Stainless Steel by R.F. Sputtering (R.F. sputtering 방법에 의해 c-BN 표면처리된 316L 오스테나이트계 스테인리스 강의 내마모특성 향상)

  • Lee, Kwang-Min;Jeong, Se-Hoon;Park, Sung-Tae
    • Korean Journal of Materials Research
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    • v.20 no.4
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    • pp.194-198
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    • 2010
  • Cubic boron nitride (c-BN) is a promising material for use in many potential applications because of its outstanding physical properties such as high thermal stability, high abrasive wear resistance, and super hardness. Even though 316L austenitic stainless steel (STS) has poor wear resistance causing it to be toxic in the body due to wear and material chips, 316L STS has been used for implant biomaterials in orthopedics due to its good corrosion resistance and mechanical properties. Therefore, in the present study, c-BN films with a $B_4C$ layer were applied to a 316L STS specimen in order to improve its wear resistance. The deposition of the c-BN films was performed using an r.f. (13.56 MHz) magnetron sputtering system with a $B_4C$ target. The coating layers were characterized using XPS and SEM, and the mechanical properties were investigated using a nanoindenter. The friction coefficient of the c-BN coated 316L STS steel was obtained using a pin-on-disk according to the ASTM G163-99. The thickness of the obtained c-BN and $B_4C$ were about 220 nm and 630 nm, respectively. The high resolution XPS spectra analysis of B1s and N1s revealed that the c-BN film was mainly composed of $sp^3$ BN bonds. The hardness and elastic modulus of the c-BN measured by the nanoindenter were 46.8 GPa and 345.7 GPa, respectively. The friction coefficient of the c-BN coated 316L STS was decreased from 3.5 to 1.6. The wear property of the c-BN coated 316L STS was enhanced by a factor of two.

Characterization of the complex(B+C+N) Diffusion Layers Formed on Tool Steels (공구강에 형성된 복합(B+C+N) 확산층의 특성 연구)

  • Lee, Jong-Hun;Yu, Wi-Do;Im, Yeong-Mok;Gwon, Gi-Hyeon
    • 연구논문집
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    • s.33
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    • pp.175-182
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    • 2003
  • In this study, the wear resistance of the complex powder diffusion treated KS STD 61 has been investigatived. KS STD 61 tool steel was pretreated in quenching and tempering processes to obtain the tempered martensitic microstructure. The samples were packed with complex powder in steel pot($\Phi$90x60mm) and heated in a box furnace. the complex powder diffusion treatment are carried out at $540^{\circ}C$, $520^{\circ}C$, $500^{\circ}C$ for 40min, 1.5hr and 2.5hr. The microstructure, microhardness, wear resistance, and coating layer thickness of the complex powder diffusion treated samples were investigation. The weight loss of as heat treated sample was 0.4mg and that of the complex powder treated at $540^{\circ}C$ for 2.5hr was 0.17mg. These result means that the wear resistance of tool steels can be easily improved by the powder diffusion process at conventional tempering treatment temperature.

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A Study on Combustion Characteristics in each Coating Thickness of Fire Retardant Paints (난연도료의 도포 두께별 연소특성에 관한 연구)

  • Kim, Hong;Park, Hyung-Ju
    • Fire Science and Engineering
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    • v.17 no.4
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    • pp.36-41
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    • 2003
  • This experimental study shows the combustion characteristics for each coating thickness of water and oil paint which are used as fire retardant paints that prevent fire propagation through cables in underground culverts and trays. To evaluate combustion characteristics, smoke density(ASTM E 662) and Limited Oxygen Index(ASTM D 2863) experiment method was used. As the results of this study, the combustion characteristics of fire retardant paints produced the following : (a) The molt suitable coating thickness of fire retardant paint was 1.5∼2.0 mm in water paint and 0.2 mm in oil paint. (b) Flaming method in experiments of smoke density were found to be higher than Non-flaming method. (c) Water paint has the fire retardant effect and characteristics better than oil paint in measurement results of smoke density and oxygen index. (d) The oxygen index of water and oil fire retardant was able to know that it was satisfied a standard (30 or above).