• Corrosion Science and Technology
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• v.19 no.1
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• pp.37-42
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• 2020

Even though 304 low-carbon (304L) stainless steel was developed to enhance the resistance to intergranular corrosion and stress corrosion cracking, it is occasionally subject to degradation in harsh environments. The degree of sensitization (DOS) of 304L stainless steel was studied as a function of sensitization using a double-loop electrochemical potentiokinetic reactivation (DL-EPR) method. Sensitizing heat treatment was performed in an Ar atmosphere at 500℃, 600℃, and 700℃, with heat treatment times varying from 0 to 96 h. DOS was measured by the ratio of the peak current density value of the forward scan to that of the reverse scan. After the EPR experiment, the specimen surface was observed by scanning electron microscopy and energy dispersive spectroscopy. The DOS of the specimens heat-treated at 600℃ increased with heat treatment times up to 48 h and then decreased due to a self healing effect. The DOS was higher in specimens heat-treated at 600℃ than those at 500℃ or 700℃. Corrosion of the sensitized specimens occurred mainly at the δ-γ phase boundary. The corrosion morphology at the δ-γ phase boundary changed with sensitizing heat-treatment conditions due to differences in chromium activity in γ austenite and δ ferrite.

• Bulletin of the Korean Chemical Society
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• v.30 no.11
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• pp.2675-2679
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• 2009

This paper reports the example of headspace mulberry paper bag micro solid phase extraction (HS-MPB-$\mu$-SPE) as a new sampling method for the determination of volatile flavor composition of coriander seeds. Adsorption efficiencies between two configurations of mulberry paper bag were compared, and several parameters affecting the HS-MPB-$\mu$-SPE were investigated and optimized. The optimized technique uses an adsorbent (Tenax TA, 0.1 mg) contained in a mulberry paper bag of front configuration where fine surface was outside, and minimal amount of organic solvent (0.6 mL). Linalool and $\gamma$-terpinene were found as abundant flavor compounds from coriander seeds. The limit of detection (LOD) and the limit of quantitation (LOQ) for linalool of major flavor in coriander seeds were 10.3 ng/mL and 34.4 ng/mL, respectively. The proposed method showed good reproducibility and good recovery. The HS-MPB-$\mu$-SPE is very simple to use, inexpensive, requires small sample amounts and solvent consumption. Because the solvent for extraction is reduced to only a very small volume, there is minimal waste or exposure to toxic organic solvent and no further concentration step.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1999.11a
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• pp.59-62
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• 1999

Inception and propagation of electrical tree and properties of Partial discharge(PD) pulses accompanying with tree as a function of needle tip radius in low density polyethylene were discussed. To study on these characteristics in different tip radius, we used specimens with needle-plane electrode system made of LDPE, observed inception and propagation of electrical tree by optical microscope with computer and investigated the characteristics of the phase resolved PD pulses accompanying with propagation of electrical tree. The PD quantities detected and analysed were PD magnitude, mean phase angle, average discharge, and the statistical characteristics of the PD pulses. As the tip radius ${\gamma}$ increases, tree inception stress E$\sub$i/ converges to constance value. This result suggests that tree inception stress E$\sub$i/ increases due to stress relaxation when the tip radius is small. Branch-type electrical tree was formed When E$\sub$i/ is 640-750[kV/mm]. bush-type electrical tree when E$\sub$i/ is 370∼400[kV/mm], branch-like electrical tree when E$\sub$i/ is 370-400[kV/mm].

• Korean Journal of Materials Research
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• v.12 no.7
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• pp.517-521
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• 2002

Europium-activated $Ga_2$$O_3$ phosphor powders were prepared by Pechini method from the mixed aqueous solutions of gallium(III) nitrate, europium(III) nitrate, ethylene glycol and citric acid. The phase formation process and particle shape of the powders obtained were investigated by means of TG/DTA, XRD and SEM. It was found that the powders were amorphous or ${\gamma}$-$Ga_2$$O_3$-like phase up to $500^{\circ}C$ and then transformed into $\beta$- $Ga_2$$O_3$ phase above $600 ^{\circ}C$. The powders calcined below $1000^{\circ}C$ were spherical and nanometer-sized. Photoluminescence spectra measured at room temperature showed that the highest luminescence intensity was obtained for the sample synthesized under the conditions of 2 mol% Eu concentration and heat treatment at $1000^{\circ}C$.

• Atmosphere
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• v.29 no.2
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• pp.227-239
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• 2019

This paper reviews various bulk-type cloud microphysics parameterizations (BCMPs). BCMP, predicting the moments of size distribution of hydrometeors, parameterizes the grid-resolved cloud and precipitation processes in atmospheric models. The generalized gamma distribution is mainly applied to represent the hydrometeors size distribution in BCMPs. BCMP can be divided in three different methods such as single-moment, double-moment, and triple-moment approaches depending on the number of prognostic variables. Single-moment approach only predicts the hydrometeors mixing ratio. Double-moment approach predicts not only the hydrometeors mixing ratio but also the hydrometeors number concentration. Triple-moment approach predicts the dispersion parameter of hydrometeors size distribution through the prognostic reflectivity, together with the number concentrations and mixing ratios of hydrometeors. Triple-moment approach is the most time expensive method because it has the most number of prognostic variables. However, this approach can allow more flexibility in representing hydrometeors size distribution relative to single-moment and double-moment approaches. At the early stage of the development of BMCPs, warm rain processes were only included. Ice-phase categories such as cloud ice, snow, graupel, and hail were included in BCMPs with prescribed properties for densities and sedimentation velocities of ice-phase hydrometeors since 1980s. Recently, to avoid fixed properties for ice-phase hydrometeors and ad-hoc category conversion, the new approach was proposed in which rimed ice and deposition ice mixing ratios are predicted with total ice number concentration and volume.

• Korean Journal of Remote Sensing
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• v.40 no.2
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• pp.141-150
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• 2024

Ground subsidence in urban areas is mainly caused by anthropogenic factors such as excessive groundwater extraction and underground infrastructure development in the subsurface composed of soft materials. Global Navigation Satellite System data with high temporal resolution have been widely used to measure surface displacements accurately. However, these point-based terrestrial measurements with the low spatial resolution are somewhat limited in observing two-dimensional continuous surface displacements over large areas. The synthetic aperture radar interferometry (InSAR) technique can construct relatively high spatial resolution surface displacement information with accuracy ranging from millimeters to centimeters. Although constellation operations of SAR satellites have improved the revisit cycle, the temporal resolution of space-based observations is still low compared to in-situ observations. In this study, we evaluate the extraction of a time-series of surface displacement in Incheon Metropolitan City, South Korea, using the small baseline subset technique implemented using the commercial software, Gamma. For this purpose, 24 COSMO-SkyMed X-band SAR observations were collected from July 12, 2011, to August 27, 2012. The time-series surface displacement results were improved by reducing random phase noise, correcting residual phase due to satellite orbit errors, and mitigating nonlinear atmospheric phase artifacts. The perpendicular baseline of the collected COSMO-SkyMed SAR images was set to approximately 2-300 m. The surface displacement related to the ground subsidence was detected approximately 1 cm annually around a few Incheon Subway Line 2 route stations. The sufficient coherence indicates that the satellite orbit has been precisely managed for the interferometric processing.

• Microbiology and Biotechnology Letters
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• v.44 no.1
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• pp.89-97
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• 2016

Obesity is caused by excess accumulation of body fat and contributes to various pathological disorders such as diabetes, hypertension, cardiovascular disease, and cancer. In this study, we investigated the effect of a 30% ethanol extract of Fructus Rosae laevigata (RLE) on adipogenesis in 3T3-L1 adipocytes, measured by triglyceride accumulation and expression of adipogenesis-related transcription factors during differentiation of pre-adipocytes into adipocytes. RLE decreased the intracellular triglyceride contents (assessed by Oil Red-O staining) in a dose-dependent manner. It also downregulated the expression of adipogenic transcription factors and inhibited cell proliferation during the mitotic clonal expansion phase of adipocyte differentiation by inducing G1 phase arrest. We investigated the alterations in the levels of G1 phase arrest-related proteins. The expression of p21 protein significantly increased, while the levels of Cyclin E, Cdk2, and phospho-Rb decreased in a dose-dependent manner in 3T3-L1 cells treated with RLE. These results suggest that RLE inhibits the differentiation of 3T3-L1 adipocytes by suppressing the expression of adipogenic transcription factors and inducing G1 phase arrest in the early stages of adipocyte differentiation.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.24 no.2
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• pp.65-69
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• 2014

Crystallographic phases of Plasma electrolytic oxidized Al alloy, A1100, A5052, A6061, A6063, A7075, were investigated. Two types of electrolyte $Na_2Si_2O_3$ and Na2P2O7 were also compared. Bipolar pulse, $2000{\mu}sec$ with $400{\mu}sec+420V$ impulse and $300{\mu}sec$ - impulse were applied for 20 min. ${\alpha}-alumina$, ${\gamma}-alumina$, ${\eta}-alumina$, $Al_{4.95}Si_{1.05}O_{9.52}$, and $(Al_{0.9}Cr_{0.1})_2O_3$ were mainly observed. Si, component of electrolyte, were moved into the PEO layer by bipolar pulse. Glassy phase was also observed at the surface of $Na_2Si_2O_3$ electrolyte treated PEO layer, and increased with the Mg content of Al alloy. It is concluded that at first glassy phase was formed by the micro plasma, and the high temperature of plasma turns glassy phase to several crystalline phases. And we could expect that many other crystalline phase could be formed by PEO process.

• Journal of the Institute of Electronics Engineers of Korea TC
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• v.38 no.4
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• pp.11-17
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• 2001

In this paper, we propose a polarity decision carrier recovery algorithm for high order QAM(Quadrature Amplitude Modulation), which has robust and large frequency acquisition performance in the high order QAM modem. The proposed polarity decision PD(Phase Detector) output and its variance characteristic are mathematically derived and the simulation results are compared with conventional DD(Decision-Directed) method. While the conventional DD algorithm has linear range of $3.5^{\circ}{\sim}3.5^{\circ}$, the proposed polarity decision PD algorithm has linear range as large as $-36^{\circ}{\sim}36^{\circ}$ at ${\gamma}-17.9$. The conventional DD algorithm can only acquire offsets less than ${\pm}10\;KHz$ in the case of the 256 QAM while an analog front-end circuit generally can reduce the carrier-frequency offset down to only ${\pm}100\;KHz$. Thus, in this case additional AFC or phase detection circuit for carrier recovery is required. But by adopting the proposed polarity decision algorithm, we can find the system can acquire up to ${\pm}300\;KHz$at SNR = 30dB without aided circuit.

• Mass Spectrometry Letters
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• v.6 no.1
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• pp.13-16
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• 2015

This study demonstrated the stabilizing role of a cyclodextrin on Keggin $[PW_{12}O_{40}]^{3-}$ via hydrogen bonding complexation unveiled by ESI-MS. The distinctive fragmentation pathways of the $\{PW_{12}\}/{\gamma}$-CD complexes from that of discrete $[PW_{12}O_{40}]^{3-}$ showed that the so-called "weak" non-covalent interactions can effectively change the dissociation chemistry of POM in the gas phase. The influence of different types of solvents and organic additives such as ${\gamma}$-CD on the stability of Keggin $[PW_{12}O_{40}]^{3-}$ was also addressed firstly by ESI-MS.