• Title/Summary/Keyword: ${\eta}$ phase

Search Result 80, Processing Time 0.024 seconds

Variation of Alloying Element Distribution and Microstructure due to Microsegregation in Ni-base Superalloy GTD 111 (니켈기 초내열 합금 GTD 111에서 편석에 의한 합금원소 분포 및 미세조직 변화)

  • Choi, Baig-Gyu;Kim, In-Soo;Do, Jeong-Hyeon;Jung, Joong-Eun;Jo, Chang-Yong
    • Journal of Korea Foundry Society
    • /
    • v.35 no.6
    • /
    • pp.170-177
    • /
    • 2015
  • Segregation during solidification and homogenization during thermal exposure in GTD 111 were investigated. The microstructures of as-cast, standard heat-treated, and thermally exposed specimens were observed by SEM. A compositional analysis of each specimen was conducted by EDS. The dendrite core was enriched in W and Co, though lower levels of Ti and Ta were observed. An unexpected phase, in this case like the ${\eta}$ phase, was observed due to segregation near the ${\gamma}-{\gamma}^{\prime}$ eutectic in the standard heat-treated specimen. Segregation also induced microstructural evolution near the ${\gamma}-{\gamma}^{\prime}$ eutectic during the standard heat treatment. A quantitative analysis and microstructural observations showed that the thermal exposure at a high temperature enhanced the chemical homogeneity of the alloy.

A Study for Absolutely Distance Measurement System of Wavelength Variable Type by Using Pinciple of the Michelson Interometer (마이켈슨 간섭계의 원리를 이용한 파장변화형 절대 거리측정기의 기초 연구)

  • 김철한;신영록;양윤석;김한근;사공건
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 2000.07a
    • /
    • pp.651-653
    • /
    • 2000
  • In this study, a distance-measurement system was proposed by using principle of the Michelson Interferometer and a fundamental research was carried out. In case of the rnichelson interferometer, relativity distance was measured by relativity-difference of two course of light. But wavelength of light source were changed in this system in order to use interference phenomenon of michelson interferometer in measuring absolutely distance. Wavelength of input signal were changed periodically and were interfered electrically. So absolute distance can be calculated by using $\Delta\lambda$ and measuring $\eta\Delta$ in electric interference. Nose by a external factor was small in this system because a absolutely distance was measured by phase difference. And a dispersion of noise was small in pulse-echo response because a error was occurred in range of phase difference of signal. Also very wide range can be measured by only single system because informations of distance were acquisited in wavelength level.

  • PDF

Elliptic Feature of Coherent Fine Scale Eddies in Turbulent Channel Flows

  • Kang Shin-Jeong;Tanahashi Mamoru;Miyauchi Toshio
    • Journal of Mechanical Science and Technology
    • /
    • v.20 no.2
    • /
    • pp.262-270
    • /
    • 2006
  • Direct numerical simulations (DNS) of turbulent channel flows up to $Re_{\tau}=1270$ are performed to investigate an elliptic feature and strain rate field on cross sections of coherent fine scale eddies (CFSEs) in wall turbulence. From DNS results, the CFSEs are educed and the strain rate field around the eddy is analyzed statistically. The principal strain rates (i.e. eigenvalues of the strain rate tensor) at the CFSE centers are scaled by the Kolmogorov length $\eta$ and velocity $U_k$. The most expected maximum (stretching) and minimum (compressing) eigenvalues at the CFSE centers are independent of the Reynolds number in each $y^+$ region (i. e. near-wall, logarithmic and wake regions). The elliptic feature of the CFSE is observed in the distribution of phase-averaged azimuthal velocity on a plane perpendicular to the rotating axis of the CFSE $(\omega_c)$. Except near the wall, phase-averaged maximum $(\gamma^{\ast}/\gamma_c^{\ast})$ and minimum $(\alpha^{\ast}/\alpha_c^{\ast})$ an eigenvalues show maxima on the major axis around the CFSE and minima on the minor axis near the CFSE center. This results in high energy dissipation rate around the CFSE.

Risk analysis of offshore terminals in the Caspian Sea

  • Mokhtari, Kambiz;Amanee, Jamshid
    • Ocean Systems Engineering
    • /
    • v.9 no.3
    • /
    • pp.261-285
    • /
    • 2019
  • Nowadays in offshore industry there are emerging hazards with vague property such as act of terrorism, act of war, unforeseen natural disasters such as tsunami, etc. Therefore industry professionals such as offshore energy insurers, safety engineers and risk managers in order to determine the failure rates and frequencies for the potential hazards where there is no data available, they need to use an appropriate method to overcome this difficulty. Furthermore in conventional risk based analysis models such as when using a fault tree analysis, hazards with vague properties are normally waived and ignored. In other word in previous situations only a traditional probability based fault tree analysis could be implemented. To overcome this shortcoming fuzzy set theory is applied to fault tree analysis to combine the known and unknown data in which the pre-combined result will be determined under a fuzzy environment. This has been fulfilled by integration of a generic bow-tie based risk analysis model into the risk assessment phase of the Risk Management (RM) cycles as a backbone of the phase. For this reason Fault Tree Analysis (FTA) and Event Tree Analysis (ETA) are used to analyse one of the significant risk factors associated in offshore terminals. This process will eventually help the insurers and risk managers in marine and offshore industries to investigate the potential hazards more in detail if there is vagueness. For this purpose a case study of offshore terminal while coinciding with the nature of the Caspian Sea was decided to be examined.

An Analysis of Characteristics for the Non-catalytic Esterification of Palm Fatty Acid Distillate (PFAD) (팜지방산 디스틸레이트의 무촉매 에스테르화 반응특성 연구)

  • Hong, Seok Won;Cho, Hyun Jun;Yeo, Yeong-Koo
    • Korean Chemical Engineering Research
    • /
    • v.52 no.3
    • /
    • pp.395-401
    • /
    • 2014
  • In this work, the reaction characteristics for the non-catalytic esterification of palm fatty acid distillate were analyzed. The esterification reaction was assumed as the pseudo homogeneous $2^{nd}$ order reversible reaction and 'reaction effectiveness factor (${\eta}$)' was used to take accounts into evaporation and reaction of water and methanol, which take place simultaneously in the liquid phase. The nonlinear programming was used to derive appropriate kinetic parameters, the reaction rate constant and mass transfer coefficient, minimizing the error between experimental data and the numerical values. Based on these parameters, the apparent activation energy was calculated to be 43.98 kJ/mol.

The Evaluation of Mechanical Property of WC-8%Co Alloys by Coercive Force and Magnetic Saturation (항자력과 자기포화도에 의한 WC-8%Co 초경합금의 기계적 성질 평가)

  • Ahn, Dong-Gil
    • Journal of the Korean Society for Nondestructive Testing
    • /
    • v.20 no.5
    • /
    • pp.438-444
    • /
    • 2000
  • The prediction of mechanical properties for WC-Co alloys by evaluation of coercive force and magnetic saturation were studied in relation to their microstructure. The WC-8%Co alloys were prepared using different WC particle size, carbon content and various sintering temperature by PM process. The magnetic properties such as coercive force and magnetic saturation of sintered WC-Co alloys were critically dependent upon their final composition and microstructure. Slight changes of carbon contents and small variation of WC grain size result in marked changes of magnetic properties, hardness and transverse rupture strength of sintered WC-Co alloys. It was found that the coercive force and hardness were increased by fine WC grain size of sinterd alloys, and the coercive force was proportional to hardness. With decreasing total carbon content below the stoichiometric value in WC-8%Co alloys the volume fraction of $\eta$ phase increased steadily, while the magnetic saturation and transverse rupture strength decreased. The magnetic saturation was inversely proportional to the coercive force of WC-Co alloys.

  • PDF

Bioactivity of Calcium Phosphate Ceramic Coatings on Metallic Implants

  • Kim, Cheol-Sang;Ducheyne, P.
    • Journal of Biomedical Engineering Research
    • /
    • v.11 no.1
    • /
    • pp.5-12
    • /
    • 1990
  • Calcium phosphate ceramics have been applied intensively to orthopaedic and dental implants by virtue of their osteoconductive nature. In an attempt to enhance the bone implant intergrity and Eta utility, these ceramics are deposited onto the porous surface of metallic implants. The coating procedure and the ensuing phase transformations of the ceramic alter the mechanical properties and surface chemistry of the ceramic layers as well as those of the substrate. These structural and compositional differences are directly related to the interaction mechanisms at the surface-active ceramicbone interface. Material and processing induced influences on dissolution, electrokinetic behavior, ceramic-metallic substrate interface and boRe growth enhancement are presented.

  • PDF

Microstructure Features of Large Grains in WC-Co Alloys

  • Delanoe, A.;Lay, S.;Missiaen, J.M.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
    • /
    • 2006.09a
    • /
    • pp.650-651
    • /
    • 2006
  • This paper presents a study of large grains by transmission electron microscopy in two WC-Co alloys, one W rich and one C rich. In the W rich alloy, some large grains are found in contact with the $\eta$ phase. The C content influences the morphology of large grains: they are flatter in the C rich alloy with smoother interfaces. Whatever the C content, they contain few dislocations compared to matrix grains except often in a small area. Small WC grains are often found inside the large grains. They have likely been engulfed during the growth of the large grains owing to the low boundary energy.

  • PDF

A STUDY ON THE FRACTURE OF DENTAL AMALGAM (치과용 아말감의 파절에 관한 연구)

  • Huh, Hyeon-Do;Um, Chung-Moon
    • Restorative Dentistry and Endodontics
    • /
    • v.9 no.1
    • /
    • pp.101-106
    • /
    • 1983
  • It was the purpose of this study to investigate the fracture mode of dental amalgam by observing the crack propagation, and to relate this to the microstructure of the amalgam. Caulk 20th Century Regular, Caulk Spherical, Dispersalloy, and Tytin amalgam alloys were used for this study. After each amalgam alloy and Hg measured exactly by the balance was triturated by the mechanical amalgamator (Capmaster, S.S. White), the triturated mass was inserted into the cylindrical metal mold which was 4 mm in diameter and 12 mm in height and was pressed by the Instron Universal Testing Machine at the speed of 1mm/min with 120Kg. The specimen removed from the mold was stored in the room temperature for a week. This specimen was polished with the emery papers from #100 to #200 and finally on the polishing cloth with 0.06${\mu}Al_2O_3$ powder suspended in water. The specimen was placed on the Instron testing machine in the method similar to the diametral tensile test and loaded at the crosshead speed of 0.05mm/min. The load was stopped short of fracture. The cracks on the polished surface of specimen was examined with scanning electron microscope (JSM-35) and analyzed by EPMA (Electron probe microanalyzer). The following results were obtained. 1. In low copper lathe-cut amalgam, the crack went through the voids and ${\gamma}_2$ phase, through the ${\gamma}_1$ phase around the ${\gamma}$ particles. 2. In low copper spherical amalgam, it was observed that the crack passed through the ${\gamma}_2$ and ${\gamma}_1$ phase, and through the boundary between the ${\gamma}_1$ and ${\gamma}$ phase. 3. In high copper dispersant (Dispersalloy) amalgam, the crack was found to propagate at the interface between the ${\gamma}_1$ matrix and reaction ring around the dispersant (Ag-Cu) particles, and to pass through the Ag-Sn particles. 4. In high copper single composition (Tytin) amalgam, the crack went through the ${\gamma}_1$ matrix between ${\eta}$ crystals, and through the unreacted alloy particle (core).

  • PDF

Study of Hydrolysis of Al Powder and Compaction of Nano Alumina by Spark Plasma Sintering(SPS) (Al 분말의 수화 반응과 스파크 플라즈마 열처리법으로 제조된 알루미나 성형체 연구)

  • Uhm Y. R.;Lee M. K.;Rhee C. K.
    • Journal of Powder Materials
    • /
    • v.12 no.6 s.53
    • /
    • pp.422-427
    • /
    • 2005
  • The $Al_2O_3$ with various phases were prepared by simple ex-situ hydrolysis and spark plasma sintering (SPS) process of Al powder. The nano bayerite $(\beta-Al(OH)_3)$ phase was derived by hydrolysis of commercial powder of Al with micrometer size, whereas the bohemite (AlO(OH)) phase was obtained by hydrolysis of nano Al powder synthesized by pulsed wire evaporation (PWE) method. Compaction as well as dehydration of both nano bayerite and bohemite was carried out simultaneously by SPS method, which is used to fabricate dense powder compacts with a rapid heating rate of $100^{\circ}C$ per min. under the pressure of 50MPa. After compaction treatment in the temperature ranges from $100^{\circ}C\;to\; 1100^{\circ}C$, the bayerite and bohemite phases change into various alumina phases depending on the compaction temperatures. The bayerite shows phase transition of $Al(OH)_3{\to}{\eta}-Al_2O_3{\to}{\theta}-Al_2O_3{\to}\alpha-Al_2O_3$ sequences. On the other hand, the bohemite experiences the phase transition from AlO(OH) to ${\gamma}-Al_2O_3\;at\;350^{\circ}C.$ It shows AlO(OH) ${\gamma}-Al_2O_3{\to}{\delta}-Al_2O_3{\to}{\alpha}-Al_2O_3$ sequences. The ${\gamma}-Al_2O_3$ compacted at $550^{\circ}C$ shows a high surface area $(138m^2/g)$.