• 제목/요약/키워드: ${\chi}$-phase

검색결과 391건 처리시간 0.027초

고속액체크로마토그라피에 의한 백지근 중 Byakangelicin의 정량 (Determination of Byakangelicin in Angelicae dahuricae Radix by High Performance Liquid Chromatography)

  • 신국현;강삼식;지형준
    • 생약학회지
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    • 제21권3호
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    • pp.239-241
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    • 1990
  • A new method for quantitative determination of byakangelicin in Angelicae dahuricae Radix by high performance liquid chromatography was established. A reversed-phase system with a ${\mu}Bondapak$ $C_{18}$ column using THF : dioxane : MeOH : HAc : 5% $H_3PO_4$ : $H_2O$=72.5 : 62.5 : 25 : 10 : 1 : 329 as a mobile phase was developed. Byakangelicin together with ter-O-byakangelicin and oxypeucedanin methanolate, and isooxypeucedanin as an internal reference were detected at 350 nm and the analysis was successfully carried out within 30 min.

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Light Induced Structural Transition in $B_7$ phase of Bent-shaped Liquid Crystals containing Azo dye

  • Kim, Hee-Kyung;Shin, S.T.;Lee, C.K.;Jang, Chi-Woong;Lim, Tong-Kun
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2002년도 International Meeting on Information Display
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    • pp.494-497
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    • 2002
  • The influence of isomeric state of doped azo dye on the $B_7$ phase of bent-shaped liquid crystal (LC) is studied. It was found that modulating the isomeric trans-cis state of azo dye can change the molecular arrangement of the bent-shaped LCs. To identify these phenomena the observations of microscopic texture, electro-optic response, second harmonic wave generation (SHG) and switching current were carried out..

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고속액체크로마토그라피에 의한 현삼근(玄蔘根) 중 p-Methoxycinnamic acid의 정량 (Determination of p-Methoxycinnamic Acid in Scrophulariae Radix by High Performance Liquid Chromatography)

  • 이상현;지형준;신국현
    • 생약학회지
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    • 제30권3호
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    • pp.328-331
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    • 1999
  • A new method for quantitative determination of p-methoxycinnamic acid in Scrophulariae radix by high performance liquid chromatography was established. A reversed-phase system with SPHERI-5 RP-18 5 micron $(250\;{\times}\;4.6\;mm)$ column using TFA (0.05%) and acetonitrile as a mobile phase was developed. p-Methoxycinnamic acid and N-(p-methoxycinnamoyl)-p-aminophenol as an internal reference were detected at 310 nm and the analysis was successfully carried out within 50 min.

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기체크로마토그래피-질량분석검출기와 고체상미량추출법을 이용한 물 중의 MTBE 미량분석

  • 전치완;이정화;정영욱
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 2005년도 총회 및 춘계학술발표회
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    • pp.195-198
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    • 2005
  • A solid-phase microextraction and gas chromatography-mass spectrometry for the extraction and analysis of methyl-tert-butyl ether has been described. methyl-tert-butyl ether was extracted from aqueous solution using SPME fiber coated polydimethylsiloxane and analysed by GC-MS with capillary column. Extraction parameters and chromatographic separation conditions were optimized. The applied method represented good analytical performance in terms of precision (3-8%, RSD) and accuracy(93-102%, mean recovery) with a method detection limit of 0.03 ppb.

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저압하에서 2-methyl-2-propanol-2-butanone계의 기액평형치의 추산 (The prediction of vapor-liquid equilibrium data for 2-methyl-2-propanol-2-butanone system at low pressure)

  • 심홍섭;류종하
    • 한국산업융합학회 논문집
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    • 제7권1호
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    • pp.97-105
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    • 2004
  • The Vapor-liquid equilibrium data for the binary system of 2-methyl-2-propanol-2-butanone are measured at subatmospheric pressure of 100, 200, 300, 400, 500, 600, 700 and 760 torr. This study shows that the relations between logarithmic values of relative valatility(log ${\alpha}$)and liquid phase composition(${\chi}$) in the above binary systems are expressed as a linear function. When the linear relationships of between logarithmic values of relative volatilities and liquid phase compositions in the binary systems of various pressure intersect at a point, this empirical equation can be applied to the systems of this kind. From these relations the vapor-liquid equilibrium data are estimated and compared with the measured values to be in a good agreement with in accuracy ${\pm}0.0021$ for the various pressure.

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진폭변조방식을 이용한 Phase Sensitive RF Modulator/Demodulator의 설계 및 제작 (Design and Implementation of phase sensitive RF Modulator/Demodulator using Amplitude Modulation)

  • 김준우;정재호;문치웅;오창현;이윤
    • 대한의용생체공학회:학술대회논문집
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    • 대한의용생체공학회 1995년도 춘계학술대회
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    • pp.167-170
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    • 1995
  • A quadrature-channel MODEM using amplitude modulation was constructed. To test the MODEM, 6.4 MHz sinusoidal wave 1 KHz triangular wave were modulated, then the modulated signal was fed into the demodulator, to reconstruct the triangular wave.

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PLD를 이용한 5상 스텝모터의 마이크로스텝 구동회로의 집적화와 성능향상에 관한 연구 (A Study on the Characteristic Improvement of PLD-used Microstep Driver for 5 Phase Hybrid Stepping Motor)

  • 안호균;박승규;남징락;지대영;송치훈;김형문
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2000년도 하계학술대회 논문집 B
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    • pp.1143-1145
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    • 2000
  • In this paper, it presents the design and implementation of a Microstep control IC using Programmable Logic Device(PLD). A Microstep driver is implemented with a 5-phase hybrid stepping motor, which has a Pentagon winding, power MOSFETs, and some devices to improve the system characteristics. The Microstep driving method is used for high performance motion control, low vibration and low noise in motor control system. The improvement of the electrical and mechanical driving characteristic of a step motor is achieved by applying microstep driver.

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Correlation Equation for Retention Factor and Resolution of Ibuprofen in SFC

  • Han, Soon-Koo;Jin, Yin-Zhe;Row, Kyung-Ho
    • Bulletin of the Korean Chemical Society
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    • 제25권12호
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    • pp.1807-1811
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    • 2004
  • Supercritical fluid chromatography (SFC) was considered for separating racemic ibuprofen. The chromatographic column (3.9 ${\times}$ 150 mm) was packed with Kromasil$^{\circledR}$ CHI-TBB, and the mobile phase was supercritical carbon dioxide with modifier of IPA. The experimental variables were the content of IPA, and temperature and pressure of supercritical mobile phase. To determine the separation condition, the empirical equation of retention factor and resolution was proposed. In the case of retention factor, the empirical equation was in the form, $k\;=\;a{\rho}\;+b/F\;+\;c\;({\rho}/F)\;+\;d$. The empirical equation for resolution was proposed as a linear form, $R\;=\;a{\rho}\;+\;bF\;+\;c$.

배플 형상에 따른 교반기 내부 고체입자 분포의 비정상상태 해석 (TRANSIENT SIMULATION OF SOLID PARTICLE DISTRIBUTION WITH VARIOUS DESIGN PARAMETERS OF THE BAFFLE IN A STIRRED TANK)

  • 김치겸;이승재;원찬식;허남건
    • 한국전산유체공학회지
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    • 제14권4호
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    • pp.1-6
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    • 2009
  • In the present study, numerical simulations were performed in a stirred solid/liquid system by using Eulerian multi-phase model. The transient flow field of liquid and distribution of solid particles were predicted in the stirred tank with pitched paddle impeller and baffles. The Frozen rotor method is adopted to consider the rotating motion of the impeller. The effects of number and width of baffles on the mixing time and the quality of solid suspension in the stirred tank are presented numerically. The result shows that the mixing time decreases as the width and number of baffles increase. The present numerical methodology can be applied to optimizing mixing condition of industrial mixer.

환형관내 고-액 2상 유동의 압력손실 변화특성에 대한 연구 (A Study on the pressure loss of sloid-liquid 2 phase flow in an annulus)

  • 우남섭;한상목;황영규;윤치호;김영주
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2007년도 춘계학술대회B
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    • pp.2720-2724
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    • 2007
  • Field measurements have revealed that the pressure drop over a borehole during drilling of a slim oil well or a well with a long reach can depend significantly on the rotation speed of the drill pipe. An accurate prediction of the annular frictional pressure drop is therefore important for conditions where the annular clearance is small. An experimental study was carried out to study solid-liquid two phase flow in a slim hole annulus. Annular velocities of carrier fluids varied from 0.2 m/s to 1.5 m/s. The carrier fluids which were utilized included tap water and CMC water solutions. Pressure drops and average flow rates were measured for the parameters such as inner-pipe rotary speed, carrier fluid velocity, hole inclination and particle injection rate. For both water and CMC solutions, the higher the concentration of the solid particles is, the larger the pressure gradients become.

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