• Title/Summary/Keyword: ${\alpha}$-particle

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PRELIMINARY STUDY ON THE ALPHA TRACK ANALYSIS OF SPHERICAL URANIUM METAL PARTICLES

  • Pyo Hyung-Yeol;Kim Jong-Yun;Lee Myung-Ho;Park Yong-Jun;Jee Kwang-Yong;Kim Won-Ho
    • Nuclear Engineering and Technology
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    • 제38권4호
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    • pp.353-358
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    • 2006
  • Alpha track analysis for the determination of the trace amount of alpha emitting nuclides in a very small particle was performed as an efficient and powerful technique during safeguard inspection. Metal particles with well-defined spherical shape, size and isotopic compositions as a reference material were used to correlate the number of tracks or track diameter with an isotopic composition eventually to identify the uranium enrichment in the environmental swipe samples. Slopes in the number of tracks versus the exposure time curve provide a simple insight into the uranium enrichment of an unknown particle. Low enriched uranium metal particles result in slopes still steeper than the depleted or natural uranium metal particles. In addition, a linear relationship between track diameter and particle size Is thought to be a useful first stage analytical tool as an efficient and convenient inspection guide. The significance of the simple linear model was also judged using the usual statistical tests.

분쇄마찰매체 효소반응계에서 생전분 효소당화를 위한 Glucoamylase와 Alpha-Amylase의 보완작용 (Synergistic Effect of Glucoamylase and $\alpha$-Amylase in Enzymatic Hydrolysis of Raw Corn Starch in an Agitated Bead Reaction System)

  • 이용현;박동찬
    • 한국미생물·생명공학회지
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    • 제18권4호
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    • pp.352-359
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    • 1990
  • 분쇄마찰매체효소반응계에서 glucoamylase와 Alpha-amylase의 보완작용에 의한 옥수수 생전분의 효소당화 mechanism을 규명코자, 분리.정제된 상기 효소의 혼합 비율에 따른 당화양상 및 생성당 조성, 전분입자 구조, 생전분입자의 particle size 분포, X-ray 회절양샹의 변화 등을 관찰하였다. 분쇄마찰매체 효소반응계에서도 효소를 분리하여 사용하였을 때보다 glucoamylase와 $\alpha$-amylase를 혼합사용할 경우 당화율이 크게 향상되었으며, 고순도의 glucose 생산에 적합한 두 효소의 혼합비율은 약 1:1-1:2(unit) 로 판명되었다.

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선택적 CO 산화 반응을 위한 Ru/$\alpha-Al_2O_3$ 촉매 고분산 제조 방법에 관한 연구 (Preparation of Highly Dispersed Ru/$\alpha-Al_2O_3$ Catalyst for Preferential CO Oxidation)

  • 엄현지;구기영;정운호;이영우;윤왕래
    • 한국수소및신에너지학회논문집
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    • 제21권5호
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    • pp.390-397
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    • 2010
  • 0.5wt% Ru/$\alpha-Al_2O_3$ catalysts are prepared by deposition-precipitation method for the preferential CO oxidation In order to investigate the effect of pH on the Ru dispersion and particle size, the pH of precursor solution is adjusted to between 5.5 and 9.5. 0.5wt% Ru/$\alpha-Al_2O_3$ catalyst prepared at the pH of 6.5 has high Ru dispersion of 17.9% and small particle size of 7.7nm. In addition, 0.5wt% Ru/$\alpha-Al_2O_3$ catalyst prepared at the pH 6.5 is easily reduced at low temperatures below $150^{\circ}C$ due to high dispersion of $RuO_2$ particle and shows high CO conversion over 90% in the wide temperature range between $100^{\circ}C$ and $160^{\circ}C$. Moreover, the deposition-precipitation is a feasible method to improve the Ru dispersion as compared to the impregnation method. The 0.5wt% Ru/$\alpha-Al_2O_3$ catalyst prepared by deposition-precipitation exhibits higher CO conversion than 0.5wt% Ru/$\alpha-Al_2O_3$ catalysts prepared by impregnation due to higher metal dispersion and better reducibility at low temperature.

대기 중 유기염소계 살충제의 가스-입자 분배 (Gas-particle Partitioning of Organochlorine Pesticides in Atmosphere)

  • 최민규;천만영
    • 한국대기환경학회지
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    • 제23권4호
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    • pp.457-465
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    • 2007
  • This study was performed to estimate the gas-particle partitioning of organochlorine pesticides (OCPs) in atmosphere, the samples were collected by PUF high volume air sampler for two years from June, 2000 to June, 2002. The gas phase fraction of ${\alpha/\gamma}-HCH$, heptachlor epoxide, ${\alpha/\gamma}-chlordane$ and trans-nonachlor was over 90%. But the gas phase fraction of ${\beta}-HCH$, p,p'-DDE, endosulfan sulfate, p,p'-DDD and p,p'-DDT was range of 20% through 80%, which means the gas phase fraction of OCPs components described above is sensitive to temperature. The correlation between the gas phase fraction and molecular weight of each OCPs component was not found in this research. The slope of regression line between gas-particle partitioning coefficient(${\log}K_p$) and subcooled liquid vapor(${\log}{P^o}_L$), gal-particle partitioning coefficient(${\log}K_p$) and octanol-air partitioning coefficient(${\log}K_{oa}$) which show -0.54 and 0.43 was not steep. So the equilibrium state between gas and particle was not reached and in this state the particulate fraction was low.

Application of CR-39 Microfilm for Rapid Discrimination Between Alpha-Particle Sources

  • Dwaikat, Nidal;Al-Karmi, Anan M.
    • Nuclear Engineering and Technology
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    • 제49권4호
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    • pp.881-885
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    • 2017
  • This work presents a new technique for discriminating between alpha particles of different energy levels. In a first study, two groups of alpha particles emitted from radium-226 and americium-241 sources were successfully separated using a CR-39 microfilm of appropriate thickness. This thickness was adjusted by chemical etching before and after irradiation so that lower-energy particles were stopped within the detector, while higher-energy particles were revealed on the back side of the detector. The number of tracks on the front side of the microfilm represented all alpha particles incident on that side from the two sources. However, the number of tracks on the back side of the microfilm represented only the long-range alpha particles of higher energy that arrived at that side. Therefore, by subtracting the number of tracks on the back side from the number of tracks on the front side, one could easily determine the number of tracks for the short-range alpha particles of lower energy that remained embedded in the microfilm. Discrimination of the two energy levels is thus achieved in a simple, fast, and reliable process.

Tribology of Clay Bonded Silicon Carbide

  • Lee, Kyunghee;Kim, Honggi
    • The Korean Journal of Ceramics
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    • 제2권4호
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    • pp.226-230
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    • 1996
  • A small amount of fine particle graphite was added to $\alpha$-SiC and $\beta$-SiC having certain particle distributions, and they were mixed clay and frit. After forming, they were sintered at 140$0^{\circ}C$ for 3 hours. Tribological properties of sintered $\alpha$-SiC-$\beta$-SiC-graphite-clay (frit) system showed that kinetic friction coefficient was 0.108, specific wear rate was 1.3${\times}10^-8\;mm^2$.$kgf^1$, and torque was 0.01kgf.cm at the wrench torque of 100 kgf.cm.

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DYNAMICAL MAGNETIC PROPERTIES OF IRON-NITRIDE MAGNETIC FLUIDS

  • Mamiya, H.;Nakatani, I.
    • 한국자기학회지
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    • 제5권5호
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    • pp.815-818
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    • 1995
  • Ac susceptibility of iron-nitride magnetic fluids with various particle number densities was measured. Therelaxation time increases rapidly as the temperature decreases or the inter-particle interaction increases. The analysis of the data suggests that the activation energy is proportional to ${(k_{B}T/J_{typ})}^{\alpha}$ with $\alpha$~-0.24 in the lower temperature range in which the thermal energy is comparable to the magnetic dipole interaction.

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SENSITIVITY ANALYSIS TO EVALUATE THE TRANSPORT PROPERTIES OF CdZnTe DETECTORS USING ALPHA PARTICLES AND LOW-ENERGY GAMMA-RAYS

  • Kim, Kyung-O;Ahn, Woo-Sang;Kwon, Tae-Je;Kim, Soon-Young;Kim, Jong-Kyung;Ha, Jang-Ho
    • Nuclear Engineering and Technology
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    • 제43권6호
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    • pp.567-572
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    • 2011
  • A sensitivity analysis of the methods used to evaluate the transport properties of a CdZnTe detector was performed using two different radiations (${\alpha}$ particle and gamma-ray) emitted from an $^{241}Am$ source. The mobility-lifetime products of the electron-hole pair in a planar CZT detector ($5{\times}5{\times}2\;mm^3$) were determined by fitting the peak position as a function of biased voltage data to the Hecht equation. To verify the accuracy of these products derived from ${\alpha}$ particles and low-energy gamma-rays, an energy spectrum considering the transport property of the CZT detector was simulated through a combination of the deposited energy and the charge collection efficiency at a specific position. It was found that the shaping time of the amplifier module significantly affects the determination of the (${\mu}{\tau}$) products; the ${\alpha}$ particle method was stabilized with an increase in the shaping time and was less sensitive to this change compared to when the gamma-ray method was used. In the case of the simulated energy spectrum with transport properties evaluated by the ${\alpha}$ particle method, the peak position and tail were slightly different from the measured result, whereas the energy spectrum derived from the low-energy gamma-ray was in good agreement with the experimental results. From these results, it was confirmed that low-energy gamma-rays are more useful when seeking to obtain the transport properties of carriers than ${\alpha}$ particles because the methods that use gamma-rays are less influenced by the surface condition of the CZT detector. Furthermore, the analysis system employed in this study, which was configured by a combination of Monte Carlo simulation and the Hecht model, is expected to be highly applicable to the study of the characteristics of CZT detectors.

복합교반법에 의한 금속복합재료의 제조공정에 따른 강화재의 분산성 검토 (Investigation of Reinforced Distribution in Fabrication Process of Metal Matrix Composites by Combined Stirring Process)

  • 이동건;강충길
    • Composites Research
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    • 제14권5호
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    • pp.1-11
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    • 2001
  • 본 논문은 금속복합재료를 반용융상태로 재가열하여 Thixoforming을 하는데 필요한 소재를 제공하기 위한 장비 설계와 제조방법 등에 관한 내용을 소개하고 있다. 장비 설계에서 기지재내에 강화재가 균일하게 분산되도록 하기 위하여 강화재의 연속주입 방법과 강화재의 온도를 제어하는 방법을 소개하고 있다. 일정한 양의 강화재를 기지재료 내에 분산시키는 것은 균일 혼합을 위하여 필요한 기술이다. 또한 분산시 강화재의 수분제거를 위하여 강화재의 온도를 제어하면서 연속적으로 강제분산시키는 것은 균일분산을 위하여 필요하다. 기지재의 초정 $\alpha$의 크기가 강화재의 분산성에 크게 영향을 미치기 때문에 기지재의 초기 온도가 초정$\alpha$의 크기에 미치는 영향 등을 검토하여 복합재료 빌렛트의 제조조건에 이용하였다.

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2π 비례계수기에 의한 α-A12O3 단결정의 TSEE와 TSL 현상에 관한 연구 (The Study of TSEE and TSL Phenomena on α-A12O3 Single Crystals Using the 2π Proportional Counter)

  • 두하영;심상현
    • 한국안광학회지
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    • 제9권1호
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    • pp.69-73
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    • 2004
  • ${\alpha}-Al_2O_3$ 단결정의 TSEE와 TSL을 $2{\pi}$비례계수기를 사용하여 측정하였다. ${\alpha}-Al_2O_3$ 단결정을 실온에서 500K 온도범위에서 X선과 자외선(UV)을 조사하였다. X선 조사 후에 3개의 TSEE와 3개의 TSL 봉우리가 관찰되었다. ${\alpha}-Al_2O_3$ 단결정의 TSEE와 TSL 그로우곡선은 여기 원의 종류에 관계없이 잘 대용되고 있음을 보여 주었다. 이 연구에서 우리는 $2{\pi}$ 비례계수기가 ${\alpha}$-입자의 에너지 스펙트럼 분석장치 뿐만 아니라 TSEE와 TSL의 측정에도 유익함을 알 수 있었다.

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