• Title/Summary/Keyword: $\mu$ synthesis

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Synthesis and Properties of $Al_2O_3-SiC$ Composites from Alkoxides (알콕사이드로부터 $Al_2O_3-SiC$ 복합재료의 제조 및 특성)

  • 이홍림;김규영
    • Journal of the Korean Ceramic Society
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    • v.30 no.2
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    • pp.123-130
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    • 1993
  • Dispersed type Al2O3-SiC composite powders were synthesized from Al-isopropoxide (Al(i-OC3H7)3) and Si(OC2H5)4 precursors by hydrolysis of mixed alkoxides and carbothermal reaction method. The characteristics of the synthesized (dispersed type) Al2O3-SiC composite powders were investigated using XRD, SEM, TEM, BET and particle size analyzer. Carbothermal reaction to produce Al2O3-SiC composite was completed in 10h at 135$0^{\circ}C$ on 3~4㎤/s (0.21~0.28cm/s) of H2 flow rate and about 1/1 of carbon/oxides(=SiO2+Al2O3) molar ratio. The synthesized powders were observed to have the mean particle size range of 0.4~1.26${\mu}{\textrm}{m}$ and showed finer particle size with increasing SiC content.

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Synthesis of Ultrafine Calcium Carbonate powders by nozzle Spouting Method (분사법에 의한 초미립 경질 탄산 칼슘 분말의 합성)

  • Ahn, Ji-Whan;Park, Charn-Hoon;Kim, Jeong-Heo;Lee, Jong-Kook;Kim, Hwan
    • Journal of the Korean Ceramic Society
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    • v.33 no.11
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    • pp.1276-1284
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    • 1996
  • Ultrafine calcim carbonate powders with the size of 0.05~0.1 ${\mu}{\textrm}{m}$ and the calcite phase were prepared by the nozzle spouting method which was conducted by spouting calcium hydroxide slurry in reactor filled with CO2 gas. Well dispersed ultra-fine particles were synthesized in condition of high Ca(OH)2 concentration of the slurry ( 0.5wt%) synthesized calcium carbonate powder was shown the large particle size with agglo-meration.

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Synthesis of diamond thin films from $H_2-CH_4$ gas mixture by rf PACVD (고주파 플라즈마 CVD에 의한 $H_2-CH_4$ 계로부터 다이아몬드 박막의 합성)

  • Lee, Sang-Hee;Klm, Dae-Il;Park, Sang-Hyun;Kim, Bo-Youl;Lee, Jong-Tae;Woo, Ho-Whan;Han, Sang-Ok;Lee, Duck-Chool
    • Proceedings of the KIEE Conference
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    • 1998.07d
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    • pp.1514-1515
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    • 1998
  • Diamond thin films were deposited on n-type (100) Si wafers from $H_2-CH_4$ gas mixture by rf PACVD. Prior to deposition, mechanical scratching was done to improve density of nucleation sites with diamond paste of 3${\mu}m$. The microstructure of deposited diamond thin films was studied by using the following conditions : discharge power of 500W, $H_2$ flow rate of 50sccm, reaction pressure of 20torr, and $CH_4/H_2$ ratio of 0.3$\sim$1%. The deposited diamond thin films showed that the crystallite was increased at the lower methane concentration. The deposited thin films were characterized by Scanning Electron Microscopy. Raman Spectroscopy and Fourier-Transform Infrared Spectroscopy.

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SIMD Multiply-accumulate Unit Design for Multimedia Data Processing (멀티미디어 처리에 적합한 SIMD 곱셈누적 연산기의 설계)

  • 홍인표;정재원;정우경;이용석
    • Proceedings of the IEEK Conference
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    • 2000.11b
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    • pp.349-352
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    • 2000
  • In this paper, a SIMD 64bit MAC (Multiply -Accumulate) unit is designed. It is composed of two 32bit MAC unit which supports SIMD 16bit operations. As a result, It can process two 32bit MAC operations or four 16bit operations in one cycle. Proposed MAC unit is described in Verilog HDL. After functional verification is performed, MAC unit is synthesized and optimized with 0.35$\mu\textrm{m}$ standard cell library. The synthesis result shows that this MAC unit can operate at 80㎒ of clock frequency in 85$^{\circ}C$, 3.0V, worst case process and 125㎒ of clock frequency at 25$^{\circ}C$, 3.3V, typical case process. It achieves 320Mops of performance, and is suitable for embedded DSP processors.

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A DSP Architecture for High-Speed FFT in OFDM Systems

  • Lee, Jae-Sung;Lee, Jeong-Hoo;SunWoo, Myung-H.;Moh, Sang-Man;Oh, Seong-Keun
    • ETRI Journal
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    • v.24 no.5
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    • pp.391-397
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    • 2002
  • This paper presents digital signal processor (DSP) instructions and their data processing unit (DPU) architecture for high-speed fast Fourier transforms (FFTs) in orthogonal frequency division multiplexing (OFDM) systems. The proposed instructions jointly perform new operation flows that are more efficient than the operation flow of the multiply and accumulate (MAC) instruction on which existing DSP chips heavily depend. We further propose a DPU architecture that fully supports the instructions and show that the architecture is two times faster than existing DSP chips for FFTs. We simulated the proposed model with a Verilog HDL, performed a logic synthesis using the 0.35 ${\mu}m$ standard cell library, and then verified the functions thoroughly.

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Synthesis and Characterization of Substituted Pyridine Complexes of Molybdenum (Ⅰ). Substituted Pyridinium Salts of Oxopentaisothiocyanatomolybdates(Ⅴ) (몰리브덴의 피리딘계 착물합성과 그 성질 (제1보). 옥소이소티오시아나토몰리브덴 (Ⅴ) 의 치환 피리딘늄염)

  • Sang Oh Oh;Chang Su Kim
    • Journal of the Korean Chemical Society
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    • v.25 no.3
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    • pp.177-182
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    • 1981
  • Benzoylpyridinium and lutidinium salts containing$ [MoO(NCS)_5]^{2-}$ have been synthesized. The complexes have been characterized by spectroscopic, magnetic susceptibility and conductivity studies. Benzoylpyridinium and lutidinium oxopentaisothiocyanatomolybdates(Ⅴ) arise from d-d and charge transfer transitions. The magnetic moments of the complexes are close to the spin-only values. The complex anions are mononuclear containing N-bonded $NCS^-$ ligand.

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Design and Implementation of High Speed Pulse Motor Controller Chip (고속 펄스 모터 콘트롤러 칩의 설계 및 구현)

  • 김원호;이건오;원종백;박종식
    • Journal of Institute of Control, Robotics and Systems
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    • v.5 no.7
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    • pp.848-854
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    • 1999
  • In this paper, we designed and implemented a precise pulse motor controller chip that generates the pulse needed to control step motor, DC servo and AC servo motors. This chip generates maximum pulse output rate of 5Mpps and has the quasi-S driving capability and speed and moving distance override capability during driving. We designed this chip with VHDL and executed a logic simulation and synthesis using Synopsys tool. The pre-layout simulation and post-layout simulation was executed by Compass tool. This chip was produced with 100 pins, PQFP package by 0.8${\mu}{\textrm}{m}$ gate array process and implemented by completely digital logic. We developed the test hardware board of performance and the CAMC(Computer Aided Motor Controller) Agent softwate to test the performance of the pulse motor controller chip produced. CAMC Agent enables user to set parameters needed to control motor with easy GUI(Graphic User Interface) environment and to display the output response of motor graphically.

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A new template matching algorithm and its ASIC chip implementation (Template matching을 위한 새로운 알고리즘 및 ASIC 칩 구현)

  • 서승완;선우명훈
    • Journal of the Korean Institute of Telematics and Electronics C
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    • v.35C no.1
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    • pp.15-24
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    • 1998
  • This paper proposes a new template matching algorithm and its chip design. The CC and SAD algorithms require the massive amount of computation. Hence, several algorithms using quantization schemes have been proposed to reduce the amount of computation and its hardware cost. the proposed algorithm called the EMPPM improves at least 22% of the noise margin compared with the MPPM algorithm. In addition, the proposed architecture can reduce the gate count by more than 60% of that used in the SAD algorithm without usig quantization schemes and 28% of the MPPM algorithm. The VHDL models have been simulated by using the CADANCETEX>$^{TM}$ and logic synthesis has been performed by using the SYNOPSYSTEX>$^{TM}$ with $0.6\mu\textrm{m}$ SOG(sea-of-gate) cell library. The implemented chip consists of 35,829 gates, operates at 100 MHz (worst case 53 MHz) and performs the template maching with the speed of 200 Mpixels/sec.

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Tsaokoarylone, a Cytotoxic Diarylheptanoid from Amomum tsao-ko Fruits

  • Moon, Surk-Sik;Cho, Soon-Chang;Lee, Ji-Young
    • Bulletin of the Korean Chemical Society
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    • v.26 no.3
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    • pp.447-450
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    • 2005
  • The crude methanol extract of the fruits of Amomum tsao-ko (Zingiberaceae) showed cytotoxic activity. Bioactivity-guided separation led to the isolation of a diarylheptanoid, tsaokoarylone [7-(4-hydroxy-3-methoxyphenyl)-1-(4-hydroxyphenyl)-hepta-4E,6E-dien-3-one] (2). 2 showed cytotoxicity at 4.9 and 11.4 $\mu$g/mL ($IC_{50}$) against human nonsmall cell lung cancer A549 and human melanoma SK-Mel-2, respectively, determined by SRB colorimetric method. During purification-(4-hydroxyphenyl)-4-hydroxyhexan-2-one (4) together with three known diarylheptanoids was also isolated. Their structures were determined from interpretation of spectroscopic data (IR, UV, MS, and NMR) and synthesis confirmed the structure of 2.

Synthesis of New 4-(tert-Octyl)phenol Derivatives and Their Anticancer Activity against Human Prostate and Lung Cancer Cell Lines

  • Che, Haiyan;Fang, Yuanying;Gurung, Santosh K.;Luo, Jun;Yoon, Deok Hyo;Sung, Gi-Ho;Kim, Tae Woong;Park, Haeil
    • Bulletin of the Korean Chemical Society
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    • v.35 no.7
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    • pp.2038-2042
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    • 2014
  • 4-(tert-Octyl)phenol derivatives bearing the D-mannitol substructure (6a, 6b, 7) were prepared from $\small{D}$-mannitol and evaluated their anticancer activity against human lung (A549) and prostate (Lncap, Du145, PC3) cancer cell lines. Among derivatives tested, the bis(tert-octyl)phenoxy compound 7 exhibited strongest proliferation inhibitory activities against human cancer cell lines tested, especially high sensitivity to human Du145 prostate cancer cells ($IC_{50}=7.3{\mu}M$).