Advances in nano research

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Examining the performance of PAI/ZnO synthesized with diamine and nano particles

  • Jianwei Shi (School of Chemistry and Chemical Engineering, Yangtze Normal University) ;
  • Xiaoxu Teng (School of Chemistry and Chemical Engineering, Yangtze Normal University)
  • Received : 2022.03.25
  • Accepted : 2022.08.18
  • Published : 2023.02.25
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Abstract

A ZnO/poly (amide-imide) hybrid nanocomposite film with different weight percentages of Zinc oxide (ZnO) nanoparticles is synthesized and characterized in this paper. A two-step reaction successfully synthesized a new kind of heteroaromatic diamine with bulky pendant groups. In order to produce 3, 5-dinitro-3, 3-bis (4-(4-Nitrophenoxy) phenyl) -2- benzofuran-1-one, 3, 3'-bis (4-hydroxyphenyl) benzofuran-1-one and 3'-bis (4-hydroxyphenyl) benzofuran-1-one were combined with 3'-bis (3-hydroxyphenyl) benzofuran-1-one. The obtained dinitro was then reduced by zinc dust and hydrochloric acid. The reaction of 4, 4* carbonyl diphthalic anhydride with amino acid L-alanine in acetic acid leads to the production of very high yields of chiral diacid monomer. As a result of the direct polymerization of these monomers, new optically active polymers were formed (amide-imide). In order to synthesize poly (amide-imide)/ZnO nanocomposites with different weight percentages (2, 4, 6, 8, and 10%), PAI and ZnO nanoparticles were combined using ultrasonication SEM, Fourier transform infrared spectroscopy, X-ray diffraction and thermal gravimetry were used to characterize the PAI films.

Keywords

Acknowledgement

This work was supported by the National Natural Science Foundation of China (21808017), the Science and Technology Research Project of Chongqing Education Board (CXQT21037 and KJQN201901428) and Fuling Science and Technology Commission Project (FLKJ, 2021ABB1041). The Natural Science Foundation Project of Chongqing CSTC (2022NSCQ-MSX0304).

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