치위생과학회지 (Journal of dental hygiene science)

  • 제22권3호
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  • Pages.191-198
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  • 2022
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  • 1598-4478(pISSN)
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  • 2233-7679(eISSN)
한국치위생과학회 (The Korean Society of Dental Hygiene Science)
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X-Ray Diffraction Analysis of Various Calcium Silicate-Based Materials

  • An, So-Youn (Department of Pediatric Dentristry & Wonkwang Bone Regeneration Research Institute, College of Dentistry, Wonkwang University) ;
  • Lee, Myung-Jin (Department of Dental Hygiene, Baekseok University) ;
  • Shim, Youn-Soo (Department of Dental Hygiene, Sunmoon University)
  • 투고 : 2022.09.01
  • 심사 : 2022.09.19
  • 발행 : 2022.09.30
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초록

Background: The purpose of this study was to evaluate the composition of the crystal phases of various calcium silicate-based materials (CSMs): ProRoot white MTAⓇ (mineral trioxide aggregate) (WMTA), Ortho MTAⓇ (OM), Endocem MTAⓇ (EM), Retro MTAⓇ (RM), Endocem ZrⓇ (EN-Z), BiodentineTM (BD), EZ-sealTM (EZ), and OrthoMTA III (OM3). Methods: In a sample holder, 5 g of the powder sample was placed and the top surface of the material was packed flat using a sterilized glass slide. The prepared slides were mounted on an X-ray diffraction (XRD) instrument (D8 Advance; Bruker AXS GmbH, Germany). The X-ray beam 2θ angle range was set at 10~90° and scanned at 1.2° per minute. The Cu X-ray source set to operate at 40 kV and 40 mA in the continuous mode. The peaks in the diffraction pattern of each sample were analyzed using the software Diffrac (version 2.1). Then, the peaks were compared and matched with those of standard materials in the corresponding Powder Diffraction File (PDF-2, JCPDS International Center for Diffraction Data). A powder samples of the materials were analyzed using XRD and the peaks in diffraction pattern were compared to the Powder Diffraction File data. Results: Eight CSMs showed a similar diffraction pattern because their main component was calcium silicate. Eight CSMs showed similar diffraction peaks because calcium silicate was their main component. Two components were observed to have been added as radiopacifiers: bismuth oxide was detected in WMTA, OM, and EM while zirconium oxide was detected in RM, EN-Z, BD, EZ, and OM3. Unusual patterns were detected for the new material, OM3, which had strong peaks at low angles. Conclusion: It was caused by the presence of Brushite, which is believed to have resulted in crystal growth in a particular direction for a specific purpose.

키워드

과제정보

This work was supported by the Sunmoon University University Research Grant of 2022.

참고문헌

  1. Torabinejad M, Hong CU, McDonald F, Pitt Ford TR: Physical and chemical properties of a new root-end filling material. J Endod 21: 349-353, 1995. https://doi.org/10.1016/S0099-2399(06)80967-2
  2. Camilleri J, Pitt Ford TR: Mineral trioxide aggregate: a review of the constituents and biological properties of the material. Int Endod J 39: 747-754, 2006. https://doi.org/10.1111/j.1365-2591.2006.01135.x
  3. Park JW, Hong SH, Kim JH, Lee SJ, Shin SJ: X-Ray diffraction analysis of white ProRoot MTA and Diadent BioAggregate. Oral Surg Oral Med Oral Pathol Oral Radiol Endod 109: 155-158, 2010. https://doi.org/10.1016/j.tripleo.2009.08.039
  4. Islam I, Chng HK, Yap AU: X-ray diffraction analysis of mineral trioxide aggregate and Portland cement. Int Endod J 39: 220-225, 2006. https://doi.org/10.1111/j.1365-2591.2006.01077.x
  5. Belio-Reyes IA, Bucio L, Cruz-Chavez E: Phase composition of ProRoot mineral trioxide aggregate by X-ray powder diffraction. J Endod 35: 875-878, 2009. https://doi.org/10.1016/j.joen.2009.03.004
  6. Torabinejad M, Parirokh M: Mineral trioxide aggregate: a comprehensive literature review--part II: leakage and bio- compatibility investigations. J Endod 36: 190-202, 2010. https://doi.org/10.1016/j.joen.2009.09.010
  7. Parirokh M, Torabinejad M: Mineral trioxide aggregate: a comprehensive literature review--part I: chemical, physical, and antibacterial properties. J Endod 36: 16-27, 2010. https://doi.org/10.1016/j.joen.2009.09.006
  8. Parirokh M, Torabinejad M: Mineral trioxide aggregate: a comprehensive literature review--part III: clinical applications, drawbacks, and mechanism of action. J Endod 36: 400-413, 2010. https://doi.org/10.1016/j.joen.2009.09.009
  9. Song JS, Mante FK, Romanow WJ, Kim S: Chemical analysis of powder and set forms of Portland cement, gray ProRoot MTA, white ProRoot MTA, and gray MTA-Angelus. Oral Surg Oral Med Oral Pathol Oral Radiol Endod 102: 809-815, 2006. https://doi.org/10.1016/j.tripleo.2005.11.034
  10. Taylor HFW: Cement chemistry. 2nd ed. Thomas Telford, London, pp.1-28, 1997.
  11. Camilleri J, Montesin FE, Brady K, Sweeney R, Curtis RV, Ford TR: The constitution of mineral trioxide aggregate. Dent Mater 21: 297-303, 2005. https://doi.org/10.1016/j.dental.2004.05.010
  12. Camilleri J: Hydration mechanisms of mineral trioxide aggregate. Int Endod J 40: 462-470, 2007. https://doi.org/10.1111/j.1365-2591.2007.01248.x
  13. Dunstetter F, de Noirfontaine MN, Courtial M: Polymorphism of tricalcium silicate, the major compound of Portland cement clinker: 1. Structural data: review and unified analysis. Cem Concr Res 36: 39-53, 2006. https://doi.org/10.1016/j.cemconres.2004.12.003
  14. Saghiri MA, Orangi J, Asatourian A, et al.: Calcium silicate-based cements and functional impacts of various constituents. Dent Mater J 36: 8-18, 2017. https://doi.org/10.4012/dmj.2015-425
  15. Retrieved June 1, 2022, from http://www.ezekiel.co.kr/03_ezseal/ezseal.html.
  16. Retrieved June 1, 2022, from http://www.biomta.com/shop/sub/product_5.php
  17. Cutajar A, Mallia B, Abela S, Camilleri J: Replacement of radiopacifier in mineral trioxide aggregate; characterization and determination of physical properties. Dent Mater 27: 879-891, 2011. https://doi.org/10.1016/j.dental.2011.04.012
  18. Darvell BW, Wu RC: "MTA"-an Hydraulic Silicate Cement: review update and setting reaction. Dent Mater 27: 407-422, 2011. https://doi.org/10.1016/j.dental.2011.02.001
  19. Min KS, Chang HS, Bae JM, Park SH, Hong CU, Kim EC: The induction of heme oxygenase-1 modulates bismuth oxide-induced cytotoxicity in human dental pulp cells. J Endod 33: 1342-1346, 2007. https://doi.org/10.1016/j.joen.2007.07.012
  20. Han L, Kodama S, Okiji T: Evaluation of calcium-releasing and apatite-forming abilities of fast-setting calcium silicate-based endodontic materials. Int Endod J 48: 124-130, 2015. https://doi.org/10.1111/iej.12290
  21. Li Q, Deacon AD, Coleman NJ: The impact of zirconium oxide nanoparticles on the hydration chemistry and bio-compatibility of white Portland cement. Dent Mater J 32: 808-815, 2013. https://doi.org/10.4012/dmj.2013-113
  22. Kang SH, Shin YS, Lee HS, et al.: Color changes of teeth after treatment with various mineral trioxide aggregate-based materials: an ex vivo study. J Endod 41: 737-741, 2015. https://doi.org/10.1016/j.joen.2015.01.019
  23. Forbes WF, Gentleman JF: Risk factors, causality, and policy initiatives: the case of aluminum and mental impairment. Exp Gerontol 33: 141-154, 1998. https://doi.org/10.1016/s0531-5565(97)00061-2
  24. Rajasekharan S, Martens LC, Cauwels RG, Verbeeck RM: Biodentine TM material characteristics and clinical applications: a review of the literature. Eur Arch Paediatr Dent 15: 147-158, 2014. https://doi.org/10.1007/s40368-014-0114-3
  25. Camilleri J, Sorrentino F, Damidot D: Investigation of the hydration and bioactivity of radiopacified tricalcium silicate cement, Biodentine and MTA Angelus. Dent Mater 29: 580-593, 2013. https://doi.org/10.1016/j.dental.2013.03.007
  26. Grech L, Mallia B, Camilleri J: Investigation of the physical properties of tricalcium silicate cement-based root-end filling materials. Dent Mater 29: e20-e28, 2013. https://doi.org/10.1016/j.dental.2012.11.007
  27. Xie J, Riley C, Chittur K: Effect of albumin on brushite transformation to hydroxyapatite. J Biomed Mater Res 57: 357-365, 2001. https://doi.org/10.1002/1097-4636(20011205)57:3<357::aid-jbm1178>3.0.co;2-1
  28. Mehdawi I, AbouNeel EA, Valappil S, et al.: Development of remineralizing, antibacterial dental materials. Acta Biomater 5: 2525-2539, 2009. https://doi.org/10.1016/j.actbio.2009.03.030
  29. Tamimi F, Sheikh Z, Barralet J: Dicalcium phosphate cements: brushite and monetite. Acta Biomater 8: 474-487, 2012. https://doi.org/10.1016/j.actbio.2011.08.005