Korean Journal of Veterinary Service (한국동물위생학회지)

The Korean Society of Veterinary Service (한국동물위생학회)
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Feasibility of monitoring of fluoroquinolones residual through feather analysis in broilers

육계에서 깃털을 이용한 플루오르퀴놀론계 잔류 모니터링 가능성 조사

  • Kim, Jae-Ho (Gyeonggi Province Northern Animal Hygiene Laboratory Office) ;
  • Kim, Mi-Hee (Gyeonggi Province Northern Animal Hygiene Laboratory Office) ;
  • Ahn, Gil-Ho (Gyeonggi Province Northern Animal Hygiene Laboratory Office)
  • 김재호 (경기도북부동물위생시험소) ;
  • 김미희 (경기도북부동물위생시험소) ;
  • 안길호 (경기도북부동물위생시험소)
  • Received : 2020.06.03
  • Accepted : 2020.06.24
  • Published : 2020.09.30
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Abstract

This study was conducted to analyze feasibility of monitoring of fluoroquinolnes residual through feather analysis in broilers. The calibration curve showed good linearity (r2≥0.99) within the concentration range of 1~100 ㎍/kg. The limit of detection (LOD) and limit of quantification (LOQ) were validated at ≤0.66 and ≤1.99 ㎍/kg in broiler feather, respectively. The recoveries in feather samples ranged from 94.6 to 114.4% (5.1-15.8% RSD) at the 5 to 20 ㎍/kg spiking levels. The proposed new analytical method proved to be suitable and effective for fluoroquinolnes determination. We also monitored fluoroquinolones residue in 36 samples (broiler that were slaughtered in Gyonggi-do) using this method. Among tested feather samples, enrofloxacin and ciprofloxacin were detected in all samples. In muscle samples, enrofloxacin was detected in 20 (55.6%) samples and ciprofloxacin was not detected.

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References

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