한국환경보건학회지 (Journal of Environmental Health Sciences)

  • 제45권3호
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  • Pages.258-266
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  • 2019
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  • 1738-4087(pISSN)
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  • 2233-8616(eISSN)
한국환경보건학회 (Korean Society of Environmental Health)
권호 표지
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흑연로 원자 흡광 광도법과 유도 결합 플라즈마 질량 분석법을 이용한 혈중 납 농도 비교

Comparison of Blood Lead Concentration Using Graphite Furnace Atomic Absorption Spectrometry (GF-AAs) and Inductively Coupled Plasma-mass Spectrometry (ICP-MS)

  • 강민경 (동아대학교 중금속 노출 환경보건센터) ;
  • 권정연 (동아대학교 중금속 노출 환경보건센터) ;
  • 김병권 (동아대학교 중금속 노출 환경보건센터) ;
  • 임현주 (동아대학교 중금속 노출 환경보건센터) ;
  • 서정욱 (동아대학교 중금속 노출 환경보건센터) ;
  • 김유미 (동아대학교 중금속 노출 환경보건센터) ;
  • 홍영습 (동아대학교 중금속 노출 환경보건센터)
  • Kang, Min-Kyung (Heavy Metal Exposure Environmental Health Center, Dong-A University) ;
  • Kwon, Jung-Yeon (Heavy Metal Exposure Environmental Health Center, Dong-A University) ;
  • Kim, Byoung-Gwon (Heavy Metal Exposure Environmental Health Center, Dong-A University) ;
  • Lim, Hyoun-Ju (Heavy Metal Exposure Environmental Health Center, Dong-A University) ;
  • Seo, Jeong-Wook (Heavy Metal Exposure Environmental Health Center, Dong-A University) ;
  • Kim, Yu-Mi (Heavy Metal Exposure Environmental Health Center, Dong-A University) ;
  • Hong, Young-Seoub (Heavy Metal Exposure Environmental Health Center, Dong-A University)
  • 투고 : 2019.06.07
  • 심사 : 2019.06.20
  • 발행 : 2019.06.30
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초록

Objectives: In this study, blood lead was analyzed using graphite furnace atomic absorption spectrometry (GF-AAs) and inductively coupled plasma mass spectrometry (ICP-MS). We tried to examine the difference and consistency of the analytical values and the applicability of the analytical method. Methods: We selected 57 people who agreed to participate in this study. After confirming the linearity of the calibration standard curves in GF-AAs and ICP-MS, the concentrations of lead in quality control material and samples were measured, and the degree of agreement was compared. Results: The detection limit of the ICP-MS was lower than that of GF-AAs. The coefficient of variation of reference materials was shown to be stable in the ICP-MS and GF-AAs. When the correspondence between the two equipments was verified by bias of the analysis values, a concordance was shown, and approximately 98% of the ideal reference lines were present within ${\pm}40%$ of the deflection. Conclusion: GF-AAs showed high sensitivity to single heavy metal analysis, but it took much time and showed higher detection limit than ICP-MS. Therefore, it would be considered necessary to switch to ICP-MS analysis method, considering that the level of lead exposure is gradually decreasing.

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