DOI QR코드

DOI QR Code

Effect of Hydrofluoric Acid Etching on Shear Bond Strength between Resin Cement and Zirconia cores

표면 불산처리가 레진시멘트와 지르코니아 하부구조물의 전단결합강도에 미치는 영향

  • Received : 2018.08.20
  • Accepted : 2018.10.01
  • Published : 2018.10.28

Abstract

The purpose of this study was to evaluate the influence of hydrofluoric acid etching treatment on the bonding strength of yttria-stabilized tetragonal zirconia polycrystal(Y-TZP). Four groups of zirconia-resin cement specimens were prepared; 1) ZGS group (zirconia, no treatment), 2) ZGSH group (zirconia, hydrofluoric acid etching treatment) 3) H-ZGS group (Hybrid zirconia, no treatment) 4) H-ZGSH group (Hybrid zirconia, hydrofluoric acid etching treatment). The shear bond strength between zirconia and porcelain was measured using a Instron Universal Testing Machine(Model DBBP-500, Instron Corporation, Kyonggi, Korea). Data were statistically analyzed using independent t-test and two-way ANOVA(${\alpha}=0.05$). The ceramic-resin cement bonding strength was affected by hydrofluoric acid etching treatment(p<0.05). Digital microscope examination of the fracture surface showed mixed failures with adhesive and cohesive types in hydrofluoric acid etching treatment with treated zirconia and hybrid zirconia groups.

이 연구의 목적은 불화 수소산 에칭 처리가 안정화된 정방 정계 지르코니아 다결정 (Y-TZP)의 결합 강도에 미치는 영향을 평가하는 것이었다. 4 그룹의 지르코니아 - 수지 시멘트 시편을 준비 하였다. 1) ZGS 그룹 (zirconia, no treatment) 2) ZGSH 그룹 (zirconia, hydrofluoric acid etching treatment) 3) H-ZGS 그룹 (Hybrid zirconia, no treatment) 4) H-ZGSH 그룹 (Hybrid zirconia, hydrofluoric acid etching treatment). 지르코니아와 도재 사이의 전단 결합 강도는 Instron Universal Testing Machine (ModelBBP-500, Instron Corporation, Kyunggi, Korea)을 사용하여 측정 하였다. 독립표본 t-test와 two-way ANOVA (${\alpha}=0.05$)를 사용하여 데이터를 통계적으로 분석했다. 세라믹 - 수지 시멘트 결합강도는 불화 수소산 에칭 처리에 영향을 받았다 (p <0.05). 파단 표면의 디지털 현미경 검사는 불화 수소산 에칭 처리한 표면처리 된 지르코니아 및 하이브리드 지르코니아 그룹에서 접착성 및 응집성 파절이 동시에 발생하는 결함을 보였다.

Keywords

References

  1. M. J. Kim, S. H. Oh, J. H. Kim, S. W. Ju, D. G. Seo, S. H. Jun, J. S. Ahn, and J. J. Ryu, "Wear Evaluation of the Human Enamel Opposing Different Y-TZP Dental Ceramics and Other Porcelains," J Dent, Vol.40, No.6, pp.979-988, 2012. https://doi.org/10.1016/j.jdent.2012.08.004
  2. L. Borchers, M. Stiesch, F. W. Bach, J. C. Buhl, C. Hubsch, T. Kellner, P. Kohorst, and M. Jendras, "Influence of Hydrothermal and Mechanical Conditions on the Strength of Zirconia," Acta Biometer, Vol.6, No.7, pp.4547-4552, 2010. https://doi.org/10.1016/j.actbio.2010.07.025
  3. P. F. Manicone, P. Rossi Iommetti, and L. Raffaelli, "An Overview of Zirconia Ceramics : Basic Properties and Clinical Application," J Dent, Vol.35, No.6, pp.819-826, 2007. https://doi.org/10.1016/j.jdent.2007.07.008
  4. A. M. Diaz-Arnold, M. A. Vargas, and D. R. Haselton, "Current status of luting agents for fixed prosthodontics," J Prosthet Dent, Vol.81, No.2, pp.135-141, 1999. https://doi.org/10.1016/S0022-3913(99)70240-4
  5. Y. Kokubo, C. Ohkubo, M. Tsumita, A. Miyashita, P. Vult von Steyern, and S. Fukushima, "Clinical marginal and internal gaps of Procera AllCeram crowns," J Oral Rehabil, Vol.32, No.7, pp.526-530, 2005. https://doi.org/10.1111/j.1365-2842.2005.01458.x
  6. S. Reich, M. Wichmann, E. Nkenke, and P. Proeschel, "Clinical fit all-ceramic three-unit fixed partial denture, generated with three different CAD/CAM systems," Eur J Oral Sci, Vol.113, No.2, pp.174-179, 2005. https://doi.org/10.1111/j.1600-0722.2004.00197.x
  7. F. Beuer, H. Aggstaller, D. Edelhoff, W. Gernet, and J. Sorensen, "Marginal and internal fits of fixed dental prostheses zirconia retainers," Dent Mater, Vol.25, No.1, pp.94-102, 2009. https://doi.org/10.1016/j.dental.2008.04.018
  8. F. J. Burke, G. J. Fleming, D. Nathanson, and P. M. Marquis, "Are adhesive technologies needed to support ceramics? An assessment of the current evidence," J Adhes Dent, Vol.4, No.1, pp.7-22, 2002.
  9. I. Sailer, A. Feher, F. Filser, L. J. Gauckler, H. Luthy, and C. H. Hammerle, "Five-year clinical results of zirconia frameworks for posterior fixed partial dentures," Int J Prosthodont, Vol.20, No.3, pp.383-388, 2007.
  10. J. Y. Thompson, B. R. Stoner, J. R. Piascik, and R. Smith, "Adhesion/cementation to zirconia and other non-silicate ceramics: where are we now," Dent Mater, Vol.27, No.1, pp.71-82, 2011. https://doi.org/10.1016/j.dental.2010.10.022
  11. D. M. Qeblawi, C. A. Munoz, J. D. Brewer, and E. A. Monaco Jr, "The Effect of Zirconia Surface Treatment on Flexural Strength and Shear Bond Strength to a Resin Cement," J Prosthet Dent, Vol.103, No.2, pp.210-220, 2010. https://doi.org/10.1016/S0022-3913(10)60033-9
  12. T. Kosmac, C. Oblak, P. Jevnikar, N. Funduk, and L. Marion, "The Effect of Surface Grinding and Sandblasting on Flexural Strength and Reliability of Y-TZP Zirconia Ceramic," Dental Mater, Vol.15, No.3, pp.426-433, 1999. https://doi.org/10.1016/S0109-5641(99)00070-6
  13. J. H. Phark, S. Duarte Jr, M. Blatz, and A. Sadan, "An in Vitro Evaluation of the Long-term Resin Bond to a New Densely Sintered High-purity Zirconium-oxide Ceramic Surface," J Prosthet Dent, Vol.101, No.1, pp.29-38, 2009. https://doi.org/10.1016/S0022-3913(08)60286-3
  14. F. Zarone, R. Sorrentino, F. Vaccaro, T. Traini, and S. Russo, "Acid Etching Surface Treatment of Feldspathic, Alumina and Zirconia Ceramics : A Micromorphological SEM Analysis," Int Dent South Afr, Vol.8, No.1, pp.20-26, 2006.
  15. P. Derand and T. Derand, "Bond strength of luting cements to zirconium oxide ceramics," Int J Prosthodont, Vol.2, No.2, pp.131-135, 2000.
  16. K. Tada, T. Sato, and M. Yoshinari, "Influence of surface treatment on bond strength of veneering ceramics fused to zirconia," Dent Mater J, Vol.2, No.3, pp.287-296, 2012.