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Polarization Phase-shifting Technique for the Determination of a Transparent Thin Film's Thickness Using a Modified Sagnac Interferometer

  • Kaewon, Rapeepan (King Mongkut's University of Technology Thonburi, Faculty of Engineering, Department of Electronic and Telecommunication Engineering) ;
  • Pawong, Chutchai (Rajamangala University of Technology Krungthep, Faculty of Science and Technology, Physics Division) ;
  • Chitaree, Ratchapak (Mahidol University, Faculty of Science, Department of Physics) ;
  • Bhatranand, Apichai (King Mongkut's University of Technology Thonburi, Faculty of Engineering, Department of Electronic and Telecommunication Engineering)
  • Received : 2018.06.22
  • Accepted : 2018.08.08
  • Published : 2018.10.25

Abstract

We propose a polarization phase-shifting technique to investigate the thickness of $Ta_2O_5$ thin films deposited on BK7 substrates, using a modified Sagnac interferometer. Incident light is split by a polarizing beam splitter into two orthogonal linearly polarized beams traveling in opposite directions, and a quarter-wave plate is inserted into the common path to create an unbalanced phase condition. The linearly polarized light beams are transformed into two circularly polarized beams by transmission through a quarter-wave plate placed at the output of the interferometer. The proposed setup, therefore, yields rotating polarized light that can be used to extract a relative phase via the self-reference system. A thin-film sample inserted into the cyclic path modifies the output signal, in terms of the phase retardation. This technique utilizes three phase-shifted intensities to evaluate the phase retardation via simple signal processing, without manual adjustment of the output polarizer, which subsequently allows the thin film's thickness to be determined. Experimental results show that the thicknesses obtained from the proposed setup are in good agreement with those acquired by a field-emission scanning electron microscope and a spectroscopic ellipsometer. Thus, the proposed interferometric arrangement can be utilized reliably for non-contact thickness measurements of transparent thin films and characterization of optical devices.

Keywords

References

  1. V. H. Flores Munoz, N.-I. T. Arellano, D. I. Serrano Garcia, A. Martínez Garcia, G. Rodriguez Zurita, and L. Garcia Lechuga, "Measurement of mean thickness of transparent samples using simultaneous phase shifting interferometry with four interferograms," Appl. Opt. 55, 4047-4051 (2016). https://doi.org/10.1364/AO.55.004047
  2. R.-S. Chang, Z.-Y. Peng, D.-F. Chen, and C.-Y. Han, "Parallel polarization phase-shifting interferometry with a multi-loop Sagnac configuration," Optik 127, 10122-10126 (2016). https://doi.org/10.1016/j.ijleo.2016.08.006
  3. S. Sarkar and K. Bhattacharya, "Polarization phase shifting cyclic interferometer for surface profilometry of non-birefringent phase samples," J. Mod. Opt. 60, 185-189 (2013). https://doi.org/10.1080/09500340.2013.765051
  4. R. P. Shukla, D. V. Udupa, N. C. Das, and M. V. Mantravadi, "Non-destructive thickness measurement of dichromated gelatin films deposited on glass plates," Opt. Laser Technol. 38, 552-557 (2006). https://doi.org/10.1016/j.optlastec.2004.11.020
  5. C. Pawong, R. Chitaree, and C. Soankwan, "The rotating linearly polarized light from a polarizing Mach-Zehnder interferometer: Production and applications," Opt. Laser Technol. 43, 461-468 (2011). https://doi.org/10.1016/j.optlastec.2010.06.020
  6. G. E. Sommargren, "Up/down frequency shifter for optical heterodyne interferometry," J. Opt. Soc. Am. 65, 960-961 (1975). https://doi.org/10.1364/JOSA.65.000960
  7. J. Shamir and Y. Fainman, "Rotating linearly polarized light source," Appl. Opt. 21, 364-365 (1982). https://doi.org/10.1364/AO.21.000364
  8. D. A. Jackson, A. D. Kersey, P. A. Leilabady, and J. D. C. Jones, "High frequency non-mechanical optical linear polarisation state rotator," J. Phys. E 19, 146-148 (1986). https://doi.org/10.1088/0022-3735/19/2/011
  9. C. Pawong, R. Chitaree, and C. Soankwan, "Investigation of the use of rotating linearly polarized light for characterizing SiO2 thin film on Si substrate," in Proc. IEEE Asia Communications and Photonics (China, Nov. 2011), 83081I (2011).
  10. R. M. A. Azzam, "Polarization Michelson interferometer as a global polarization state generator and for measurement of the coherence and spectral properties of quasimonochromatic light," Rev. Sci. Instrum. 64, 2834-2837 (1993). https://doi.org/10.1063/1.1144370
  11. S. Chakraborty and K. Bhattacharya, "Real-time edge detection by cyclic-path polarization interferometer," Appl. Opt. 53, 727-730 (2014). https://doi.org/10.1364/AO.53.000727
  12. V. H. Flores Munoz, N. I. Toto-Arellano, B. Lopez-Ortiz, A. Martinez Garcia, and G. Rodriguez-Zurita, "Measurement of red blood cell characteristic using parallel phase shifting interferometry," Opt. - Int. J. Light Electron. Opt. 126, 5307-5309 (2015). https://doi.org/10.1016/j.ijleo.2015.09.019
  13. B. Bhaduri, "Cyclic-path digital speckle shear pattern interferometer: use of polarization phase-shifting method," Opt. Eng. 45, 105604-1-105604-6 (2006). https://doi.org/10.1117/1.2361194
  14. X. Liu, Y. Gao, and M. Chang, "A new lateral shearing interferometer for precision surface measurement," Opt. Lasers Eng. 47, 926-934 (2009). https://doi.org/10.1016/j.optlaseng.2009.03.019
  15. L. R. Watkins, "Automatic null ellipsometry with an interferometer," Appl. Opt. 48, 6277-6280 (2009). https://doi.org/10.1364/AO.48.006277
  16. L. R. Watkins, "Interferometric ellipsometer," Appl. Opt. 47, 2998-3001 (2008). https://doi.org/10.1364/AO.47.002998
  17. F.-W. Sheu and S.-Y. Liu, "Using a Mach-Zehnder interferometer to measure the phase retardations of wave plates," in Proc. Education and Training in Optics and Photonics, EMB1 (2007).
  18. C. Zhao, J. Tan, J. Tang, T. Liu, and J. Liu, "Confocal simultaneous phase-shifting interferometry," Appl. Opt. 50, 655-661 (2011). https://doi.org/10.1364/AO.50.000655
  19. K. Bhattacharya, "Generation of phase-modulated periodic optical signals by use of a polarization interferometer," Appl. Opt. 40, 261-267 (2001). https://doi.org/10.1364/AO.40.000261
  20. S. Sarkar, N. Ghosh, S. Chakraborty, and K. Bhattacharya, "Self-referenced rectangular path cyclic interferometer with polarization phase shifting," Appl. Opt. 51, 126-132 (2012). https://doi.org/10.1364/AO.51.000126
  21. L. Wang, L. Liu, Z. Luan, J. Sun, and Y. Zhou, "Polarization phase-shifting Jamin shearing interferometer," Opt. - Int. J. Light Electron. Opt. 121, 358-361 (2010). https://doi.org/10.1016/j.ijleo.2008.07.023
  22. R. P. Tatam, J. D. C. Jones, and D. A. Jackson, "Optical polarisation state control schemes using fibre optics or Bragg cells," J. Phys. E 19, 711-717 (1986). https://doi.org/10.1088/0022-3735/19/9/013
  23. J. C. Manifacier, J. Gasiot, and J. P. Fillard, "A simple method for the determination of the optical constants n, k and the thickness of a weakly absorbing thin film," J. Phys. E 9, 1002-1004 (1976). https://doi.org/10.1088/0022-3735/9/11/032
  24. M. Horprathum, P. Chindaudom, P. Limnonthakul, P. Eiamchai, N. Nuntawong, V. Patthanasettakul, A. Pokaipisit, and P. Limsuwan, "Dynamic in situ spectroscopic ellipsometric study in inhomogeneous TiO2 thin-film growth," J. Appl. Phys. 108, 013522-1-013522-7 (2010). https://doi.org/10.1063/1.3457839
  25. E. Franke, C. L. Trimble, M. J. DeVries, J. A. Woollam, M. Schubert, and F. Frost, "Dielectric function of amorphous tantalum oxide from the far infrared to the deep ultraviolet spectral region measured by spectroscopic ellipsometry," J. Appl. Phys. 88, 5166-5174 (2000). https://doi.org/10.1063/1.1313784