Mass Spectrometry Letters

Korean Society for Mass Spectrometry (한국질량분석학회)
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Simple and Direct Quantitative Analysis for Quinidine Drug in Fish Tissues

  • Received : 2016.11.24
  • Accepted : 2017.02.02
  • Published : 2017.03.30
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Abstract

Analysis of quinidine for fish tissues using single drop microextraction (SDME) coupled with atmospheric pressure matrix assisted laser desorption/ionization mass spectrometry (AP-MALDI-MS) are reported. Optimization conditions; such as extraction solvent, extraction time, pH of the aqueous solution, salt additions (NaCl), stirring rate, matrix type and concentration are investigated. Linear dynamic range (${\mu}M$), limit of detection, relative recovery%, and enrichment factor are 0.08-9.2, 0.05, $94.8{\pm}3.1-98.5{\pm}3.3%$, $4.34{\pm}0.28-4.40{\pm}0.30$, respectively. SDME-AP-MALDI-MS shows good intraday and interday reproducibility.

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References

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