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Optimization of Ni2+ adsorption on 13X zeolite using box-behnken design

  • Jafari, Shoeib (Department of Chemistry, Islamic Azad University, Science and Research Branch) ;
  • Bandarchian, Farideh (Department of Chemistry, Islamic Azad University, Central Tehran Branch)
  • 투고 : 2017.03.16
  • 심사 : 2017.11.01
  • 발행 : 2017.09.25

초록

In this study, the elimination of $Ni^{2+}$ using 13X sorbent due to an electrostatic interaction was reported. The significant factors including pH, time and 13X sorbent amount were investigated using Box-Behnken design (BBD). In the optimum experimental conditions, the linear rang and limit of detection of the proposed method were 0.1-20 and $0.102mg\;L^{-1}$, respectively. The precision as RSD% was 1.3% for concentration of $2mg\;L^{-1}$. Concerning the excellent recoveries in a short time with highly efficient sample clean-up and removal, this method may be a very powerful and innovative future sample removal technique. To the best of our knowledge, this is the first report on using BBD for optimizing the parameters affected the removal of $Ni^{2+}$ by 13X zeolite sorbent.

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