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Effects of electron beam irradiation on the superconducting properties of YBCO thin films

  • Lee, Y.J. (Korea Atomic Energy Research Institute) ;
  • Choi, J.H. (Korea Atomic Energy Research Institute) ;
  • Jun, B.H. (Korea Atomic Energy Research Institute) ;
  • Joo, J. (Sungkyunkwan University) ;
  • Kim, C.S. (Korea Research Institute of Standards and Science) ;
  • Kim, C.J. (Korea Atomic Energy Research Institute)
  • Received : 2016.11.02
  • Accepted : 2016.12.13
  • Published : 2016.12.31

Abstract

The effects of electron beam (EB) irradiation on the superconducting critical temperature ($T_c$) and critical current density ($J_c$) of YBCO films were studied. The YBCO thin films were irradiated using a KAERI EB accelerator with an energy of 0.2 MeV and a dose of $10^{15}-10^{16}e/cm^2$. A small $T_c$ decrease and a broad superconducting transition were observed as the EB dose increased. The value of $J_cs$ (at 20 K, 50 K and 70 K) increased at doses of $7.5{\times}10^{15}$ and $2.2{\times}10^{16}e/cm^2$. However, $J_cs$ decreased as the dose increased further. The X-ray diffraction (XRD) analysis showed that the c axis of YBCO was elongated and the full width at half maximum (FWHM) increased as the dose increased, which is strong evidence of the atomic displacement by EB irradiation. The transmission electron microscopy (TEM) showed that the amorphous layer formed in the vicinity of the surfaces of the irradiated films. The amorphous phase was often present as an isolated form in the interior of the films. In addition to the formation of the amorphous phase, many striations running along the a-b direction of YBCO were observed. The high magnification lattice image showed that the striations were stacking faults. The enhancement of $J_c$ by EB irradiation is likely to be due to the lattice distortion and the formation of defects such as vacancies and stacking faults. The decrease in $J_c$ at a high EB dose is attributed to the extension of the amorphous region of a non-superconducting phase.

Keywords

References

  1. M. K. Wu, J. R. Ashburn, C. J. Torng, P. H. Hor, R. L. Meng, L. Gao, Z. J. Huang, Y. Q. Wang and C.W. Chu, "Superconductivity at 93 K in a new mixed-phase Y-Ba-Cu-O compound system at ambient pressure," Phys. Rev. Lett., vol. 58, pp. 908-910, 1987. https://doi.org/10.1103/PhysRevLett.58.908
  2. G. W. Crabtree, J. Z. Liu, A. Umezawa, W. K. Kwok, C. H. Sowers, S. K. Malik, B. W. Veal, D. J. Lam, M. B. Brodsky and J. W. Downey, "Large anisotropic critical magnetization currents in single-crystal $YBa_2Cu_3O_{7-{\delta}}$," Phys. Rev. B, vol. 36, pp. 4021-4024, 1987. https://doi.org/10.1103/PhysRevB.36.4021
  3. M. Daeumling, J. M. Seuntjens and D. C. Larbalestier, "Oxygen-defect flux pinning, anomalous magnetization and intra-grain granularity in $YBa_2Cu_3O_{7-{\delta}}$," Nature, vol. 346, pp. 332-335, 1990. https://doi.org/10.1038/346332a0
  4. M. Mironova, D. F. Lee and K. Salama, "TEM and critical current density studies of melt-textured $YBa_2Cu_3O_x$ with silver and $Y_2BaCu_3O_5$ additions," Physica C, vol. 211, pp. 188-204, 1993. https://doi.org/10.1016/0921-4534(93)90741-8
  5. A. Diaz, L. Mechin, P. Berghuis, and J. E. Evetts, "Evidence for vortex pinning by dislocations in $YBa_2Cu_3O_{7-{\delta}}$ low-angle grain boundaries," Phys. Rev. Lett., vol. 80, pp. 3855-3858, 1998. https://doi.org/10.1103/PhysRevLett.80.3855
  6. H. Yamasaki, Y. Nakagawa, A. Sawa, H. Obara and K. Develos, "Flux pinning effects of twin boundaries studied with unidirectionally twinned YBCO films," Physica C, vol. 372-376, pp. 1885-1889, 2002. https://doi.org/10.1016/S0921-4534(02)01001-8
  7. Z. L. Wang, A. Goyal and D.M. Kroeger, "Structural and chemical disorder near the $Y_2BaCuO_5/Yba_2Cu_3O_{7- {\delta}}$ interface and its possible relation to the flux-pinning behavior in melt-textured $YBa_2Cu_3O_{7-{\delta}}$," Phys. Rev. B, vol. 47, pp. 5373-5382, 1993. https://doi.org/10.1103/PhysRevB.47.5373
  8. C. J. Kim and G. W. Hong, "Defect formation, distribution and size reduction of $Y_2BaCuO_5$ in melt-processed YBCO superconductors," Supercond. Sci. Technol., vol. 12, pp. 24-41, 1999. https://doi.org/10.1088/0953-2048/12/1/006
  9. G. Krabbes, G. Fuchs, P. Schatzle, S. Grup, J. W. Park, F. Hardinghaus, G. Stover, R. Hayn, S. L. Drechsler and T. Fahr, "Zn doping of $YBa_2Cu_3O_7$ in melt textured materials: peak effect and high trapped field," Physica C, vol. 330, pp. 181-190, 2000. https://doi.org/10.1016/S0921-4534(99)00616-4
  10. M. Murakami, N. Sakai, T. Higuchi and S. I. Yoo, "Melt-processed light rare earth element-Ba-Cu-O," Supercond. Sci. Technol., vol. 9, pp. 1015-1032, 1996. https://doi.org/10.1088/0953-2048/9/12/001
  11. Y. J. Zhao, W. K. Chu, M. F. Davis, J. C. Wolfe, S. C. Deshmukh and D. J. Economou, "Radiation damages and flux pinning in $YBa_2Cu_3O_7$ thin films," Physica C, vol. 184, pp. 144-148, 1991. https://doi.org/10.1016/0921-4534(91)91511-2
  12. L. Gozzelino, D. Botta, R. Cherubini, A. Chiodoni, R. Gerbaldo, G. Ghigo and F. Laviano, "Proton irradiation induced effects on YBCO films analyzed by magnetooptics," in Magneto-Optical Imaging, vol. 142, T. H. Johansen and D. V. Shantsev, Spinger Netherlands, 2004, pp. 197-204.
  13. F. M. Sauerzopf, H. P. Wiesinger and H. W. Weber, "Analysis of pinning effects in $YBa_2CuO_{7-{\delta}}$ single crystals after fast neutron irradiation," Phys. Rev. B, vol. 51, pp. 6002-6012, 1995. https://doi.org/10.1103/PhysRevB.51.6002
  14. F. M. Sauerzopf, H. P. Wiesinger, H. W. Weber, G. W. Crabtree and J. Z. Liu, "Neutron-irradiation effects on critical current densities in single-crystalline $YBa_2Cu_3O_{7-{\delta}}$," Phys. Rev. B, vol. 43, pp. 3091-3100, 1991. https://doi.org/10.1103/PhysRevB.43.3091
  15. T. Kato, K. Shiraishi and J. Kuniya, "Enhanced critical magnetization currents due to electron irradiation in high-$T_c$ oxide superconductors," Jpn. J. Appl. Phys., vol. 28, pp. 766-768, 1989. https://doi.org/10.1143/JJAP.28.L766
  16. M. A. Kirk and Y. Yan, "Structure and properties of irradiation defects in $YBa_2Cu_3O_{7-x}$," Micron, vol. 30, pp. 507-526, 1999. https://doi.org/10.1016/S0968-4328(99)00051-7
  17. H. Matsui, H. Ogiso, H. Yamasaki, M. Sohma, I. Yamaguchi, T. Kumagai, and T. Manabe, "Influence of middle-energy ion-irradiation on the flux pinning properties of YBCO films: Comparison between different synthesis methods," J. Phys. Conf. Ser., vol. 507, pp. 022019, 2014. https://doi.org/10.1088/1742-6596/507/2/022019
  18. N. M. Strickland, E. F. Talantsev, N. J. Long, J. A. Xia, S. D. Searle, J. Kennedy, A. Markwitz, M. W. Rupich, X. Li and S. Sathyamurthy, "Flux pinning by discontinuous columnar defects in 74 MeV Ag-irradiated $YBa_2Cu_3O_7$ coated conductors," Physica C, vol. 469, pp. 2060-2067, 2009. https://doi.org/10.1016/j.physc.2009.08.009
  19. Y. Mizukami, M. Konczykowski, Y. Kawamoto, S. Kurata, S. Kasahara, K. Hashimoto, V. Mishra, A. Kreisel, Y. Wang, P. J. Hirschfeld, Y. Matsuda and T. Shibauchi, "Disorder-induced topological change of the superconducting gap structure in iron pnictides," Nature, vol. 5, pp. 5657, 2014.
  20. D. X. Chen and R. B. Goldfarb, "Kim model for magnetization of type II superocnductors," J. Appl. Phys., vol. 66, pp. 2486, 1989.
  21. R. Biswal, J. John, P. Mallick, B. N. Dash, P. K. Kulriya, D. K. Avasthi, D. Kanjilal, D. Behera, T. Mohanty, P. Raychaudhuri, and N. C. Mishra, "200 MeV silver ion irradiation induced structural modification in $YBa_2Cu_3O_{7-y}$ thin films at 89 K: An in situ x-ray diffraction study," J. Appl. Phys., vol. 106, pp. 053912, 2009. https://doi.org/10.1063/1.3212537
  22. E. D. Specht, C. J. Sparks, A. G. Dhere, J. Brynestad, O. B. Cavin, and D. M. Kroeger and H. A. Oye, "Effect of oxygen pressure on the orthorhombic-tetragonal transition in the high-temperature superconductor $YBa_2Cu_3O_x$," Phys. Rev. B, vol. 37, pp. 7426, 1988. https://doi.org/10.1103/PhysRevB.37.7426
  23. P. Benzia, E. Bottizzoa, N. Rizzi, "Oxygen determination from cell dimensions in YBCO superconductors," J. Cryst. Growth, vol. 269, pp. 625-629, 2004. https://doi.org/10.1016/j.jcrysgro.2004.05.082
  24. H. L. Edwards, J. T. Markert, and A. L. de Lozanne, "Energy gap and surface structure of $YBa_2Cu_3O_7$ probed by scanning tunneling microscopy," Phys. Rev. Lett., vol. 69, pp. 2946, 1992.
  25. S. Horiuchi, "Arrangements of oxygen atoms in $YBa_2Cu_3O_{6+x}$, superconductors visualized by ultra-high-resolution electron microscopy," Mater. Chem. Phys., vol. 35, pp. 139-144, 1993. https://doi.org/10.1016/0254-0584(93)90189-S
  26. C. D. Dewhurst, W. Lo, Y. H. Shi and D. A. Cardwell, "Homogeneity of superconducting properties in $SmBa_2Cu_3O_{7-{\delta}}$-seeded melt processed YBCO," Mater. Sci. Eng. :B, vol. 53, pp. 169-173, 1998.

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