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Evaluation of Material Characteristics with Sintering Temperature in Ti2AlC MAX Phase Material using Spark Plasma Sintering Method

방전플라즈마 소결법을 이용한 Ti2AlC Max Phase 소결체의 소결온도 변화에 따른 재료 특성 평가

  • 이창훈 (부산대학교 융합학부 하이브리드소재응용전공) ;
  • 백경래 (부산대학교 융합학부 하이브리드소재응용전공) ;
  • 정희상 ((주)싸토리우스코리아) ;
  • 정영근 (부산대학교 융합학부 하이브리드소재응용전공) ;
  • 강명창 (부산대학교 융합학부 하이브리드소재응용전공)
  • Received : 2015.06.09
  • Accepted : 2015.06.20
  • Published : 2015.06.28

Abstract

In this study, ternary compound Max Phase $Ti_2AlC$ material was mixed by 3D ball milling as a function of ball milling time. More than 99.5 wt% pure $Ti_2AlC$ was synthesized by using spark plasma sintering method at 1000, 1100, 1200, and $1300^{\circ}C$ for 60 min. The material characteristics of synthesized samples were examined with relative density, hardness, and electrical conductivity as a function of sintering temperature. The phase composition of bulk was identified by X-ray diffraction. On the basis of FE-SEM result, a terraced structures which consists of several laminated layers were observed. And $Ti_2AlC$ bulk material obtained a vickers hardness of 5.1 GPa at the sintering temperature of $1100^{\circ}C$.

Keywords

References

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