Journal of Power System Engineering (동력기계공학회지)

The Korean Society for Power System Engineering (한국동력기계공학회)
권호 표지
DOI QR코드

DOI QR Code

Fabrication of Graphene Using Exfoliation Method

박리법을 이용한 그래핀 제조

  • Lee, Jeong-Su (Dapartment of Materials Science and Engineering, Pukyong National University) ;
  • Kim, Bu-Ahn (Dapartment of Materials Science and Engineering, Pukyong National University) ;
  • Moon, Chang-Kwon (Dapartment of Materials Science and Engineering, Pukyong National University)
  • Received : 2014.03.05
  • Accepted : 2014.10.15
  • Published : 2014.12.31
Download PDF
⟨ Previous Next ⟩

Abstract

The effect of various synthesis conditions in the fabrication of graphene using the exfoliation methods has been investigated. Graphite oxide and graphene fabricated by various synthesis conditions were identified by SEM and XRD. Graphite oxide was made from graphite by the chemical oxidation, and graphene was manufactured from graphite oxide by thermal exfoliation method. As a result, it is confirmed that graphite oxide was well formed from graphite, and the graphene could be obtained from graphite oxide. And it was found that the interlayer spacing between the graphene layers depended on the reaction time and particle size, regardless of the reaction temperature from $5^{\circ}C$ to $25^{\circ}C$.

Keywords

References

  1. M. Cakmak, 2011, "Manufacturing of Multifunctional Electrically Conductive/Transparent/Flexible Films", University of Akron, WO pp.1-55
  2. D. B. Lee and C. K. Moon., 2003, "Study on the Evaluation of the interfacial Strength in the Fiber Reinforced Composites", Journal of the Korea Society For Power System Engineering 7, pp.25-33.
  3. B. Lee, H. L. Choi and C. K. Moon., 2008, "A study on the Polymer surface treatment of GF-filter bag for collection of fine Particle like carbon black", Journal of the Korea Society For Power System Engineering 12, pp.55-59.
  4. J. C. Meyer et al., 2007, "On the roughness of single- and bi-layer graphene membranes", Nature 446, pp.60-63. https://doi.org/10.1038/nature05545
  5. K. S. Kim et al., 2009, "Large-scale pattern growth of graphene films for stretchable transparent electrodes" Nature 457, pp.706-710. https://doi.org/10.1038/nature07719
  6. S. Watcharotone et al., 2007, "Simple approach for high-contrast optical imaging and characterization of graphene-based sheets", Nano Letter Vol.7, pp.1888-1892. https://doi.org/10.1021/nl070477+
  7. X. L. Li et al., 2008, "Highly Conducting Graphene Sheets and Langmuir-Blodgett Films", Science 319 pp.1229-1232. https://doi.org/10.1126/science.1150878
  8. O. Niitsoo and A. Couzis, 2011, "Facile synthesis of silver core - silica shell composite nanoparticles", Journal of Colloid Interface Sci. 354, pp.887. https://doi.org/10.1016/j.jcis.2010.11.013
  9. S. Gilje et al., 2007, "A Chemical Route to Graphene for Device Applications", Nano Letter.7, pp.3394-3398. https://doi.org/10.1021/nl0717715
  10. K. S. Novoselov et al., 2005, "Two-dimensional gas of massless Dirac fermions in graphene", Nature 438, pp.197-200. https://doi.org/10.1038/nature04233
  11. Y. B. Zhang, Y. W. Tan, H. L. Stormer and P. Kim, 2005, "Experimental observation of the quantum Hall effect and Berry's phase in graphene.", Nature 438, pp.201-204. https://doi.org/10.1038/nature04235
  12. A. Altland, Physical Review Letter 97 (2006) pp.236-802.
  13. J. Lee et al., 2006, "Electrochemical capacitance of nanocomposite films formed by loading carbon nanotubes with ruthenium oxide", Journal of Power Sources 159, pp.1527-1531. https://doi.org/10.1016/j.jpowsour.2005.11.063
  14. F. Schedin et al., 2007, "Detection of individual gas molecules adsorbed on graphene", Nature Materials 6, pp.652-655. https://doi.org/10.1038/nmat1967
  15. H. C. Schniepp et al., 2006, "Functionalized single graphene sheets derived from splitting graphite oxide", Journal of Physical Chemistry B, Vol. 110, pp.8535-8539.
  16. H. B. Zhang et al., 2010, "Electrically conductive polyethylene terephthalate/graphene nanocomposites prepared by melt compounding", polymer 51, pp.1191-1196 https://doi.org/10.1016/j.polymer.2010.01.027