DOI QR코드

DOI QR Code

INFLUENCE OF MECHANICAL ALLOYING ATMOSPHERES ON THE MICROSTRUCTURES AND MECHANICAL PROPERTIES OF 15Cr ODS STEELS

  • Noh, Sanghoon (Nuclear Materials Division, Korea Atomic Energy Research Institute) ;
  • Choi, Byoung-Kwon (Nuclear Materials Division, Korea Atomic Energy Research Institute) ;
  • Kang, Suk Hoon (Nuclear Materials Division, Korea Atomic Energy Research Institute) ;
  • Kim, Tae Kyu (Nuclear Materials Division, Korea Atomic Energy Research Institute)
  • 투고 : 2013.11.07
  • 심사 : 2014.07.10
  • 발행 : 2014.12.25

초록

Mechanical alloying under various gas atmospheres such as Ar, an Ar-$H_2$ mixture, and He gases were carried out, and its effects on the powder properties, microstructure and mechanical properties of ODS ferritic steels were investigated. Hot isostatic pressing and hot rolling processes were employed to consolidate the ODS steel plates. While the mechanical alloyed powder in He had a high oxygen concentration, a milling in Ar showed fine particle diameters with comparably low oxygen concentration. The microstructural observation revealed that low oxygen concentration contributed to the formation of fine grains and homogeneous oxide particle distribution by the Y-Ti-O complex oxides. A milling in Ar was sufficient to lower the oxygen concentration, and this led a high tensile strength and fracture elongation at a high temperature. It is concluded that the mechanical alloying atmosphere affects oxygen concentration as well as powder particle properties. This leads to a homogeneous grain and oxide particle distribution with excellent creep strength at high temperature.

키워드

참고문헌

  1. P . Yvon and F. Carre, "Structural Materials Challenges for Advanced Reactor Systems." J. Nucl. Mater., Vol. 385, pp. 217-222 (2009). https://doi.org/10.1016/j.jnucmat.2008.11.026
  2. S . Ukai, T. Okuda, M. Fujiwara, T. Kobayashi, S. Mizuta and H. Nakashima, "Characterization of High Temperature Creep Properties in Recrystallized 12Cr-ODS Ferritic Steel Claddings." J. Nucl. Sci. Technol., Vol. 39, pp.872-879 (2002). https://doi.org/10.1080/18811248.2002.9715271
  3. T .K. Kim, C.S. Bae, D.H. Kim, J. Jang, S.H. Kim, C.B. Lee and D. Hahn, "Microstructural Observation and Tensile Isotropy of an Austenitic ODS Steel." Nucl. Eng. Technol., Vol. 40, pp.305-310 (2008). https://doi.org/10.5516/NET.2008.40.4.305
  4. H .S. Cho, H. Ohkubo, N. Iwata, A. Kimura. S. Ukai and M. Fujiwara, "Improvement of Compatibility of Advanced Ferritic Steels with Super Critical Pressurized Water Toward a Higher Thermally Efficient Water-cooled Blanket System, " Fusion Eng. Design, Vol. 81, pp.1071-1076 (2006). https://doi.org/10.1016/j.fusengdes.2005.09.056
  5. S . Yamashita, N. Akasaka, S. Ukai and S. Ohnuki, "Microstructural Development of a Heavily Neutron-Irradiated ODS Ferritic Steel (MA957) at Elevated Temperature." J. Nucl. Mater., Vol. 367-370, pp.202-207 (2007). https://doi.org/10.1016/j.jnucmat.2007.03.145
  6. S . Ohtsuka, S. Ukai and M. Fujiwara, "Nano-mesoscopic Structural Control in 9CrODS Ferritic/martensitic Steels." J. Nucl. Mater., Vol. 351, pp.241-246 (2006). https://doi.org/10.1016/j.jnucmat.2006.02.006
  7. Z . Oksiuta and N. Baluc, "Effect of Mechanical Alloying Atmosphere on the Microstructure and Charpy Impact Properties of an ODS Ferritic Steel." J. Nucl. Mater., Vol.386-388, pp.426-429 (2009). https://doi.org/10.1016/j.jnucmat.2008.12.148
  8. N .Y. Iwata, T. Liu, P. Dou, R. Kasada, A. Kimura, T. Okuda, M. Inoue, F. Abe, S. Ukai, S. Ohnuki and T. Fujisawa, "Effect of MA Environment on the Mechanical and Microstructural Properties of ODS Ferritic Steels." J. Nucl. Mater., Vol. 417, pp.162-165 (2011). https://doi.org/10.1016/j.jnucmat.2010.12.058
  9. S . Ukai, M. Harada, H. Okada, M. Inoue, S. Nomura, S. Shikakura, K. Asabe, T. Nishida and M. Fujiwara, "Alloying Design of Oxide Dispersion Strengthened Ferritic Steel for Long Life FBRs Core Materials." J. Nucl. Mater., Vol. 204, pp.65-73 (1993). https://doi.org/10.1016/0022-3115(93)90200-I
  10. S. Ohtsuka, Ukai, M. Fujiwara, T. Kaito and T. Narita, "Improvement of 9Cr-ODS Martensitic Steel Properties by Controlling Excess Oxygen and Titanium Contents." J. Nucl. Mater., Vol. 329-333, pp.372-376 (2004). https://doi.org/10.1016/j.jnucmat.2004.04.043

피인용 문헌

  1. Development of Advanced Radiation Resistant ODS Steel for Fast Reactor System Applications vol.03, pp.03, 2015, https://doi.org/10.4236/wjet.2015.33C019
  2. Mössbauer Spectroscopy Study of Laboratory Produced ODS Steels vol.131, pp.4, 2017, https://doi.org/10.12693/APhysPolA.131.1171
  3. Stability of Y-Ti-O nanoparticles during laser deposition of oxide dispersion strengthened steel powder vol.23, pp.6, 2017, https://doi.org/10.1007/s12540-017-6832-4
  4. Processing Techniques for ODS Stainless Steels pp.1543-1916, 2018, https://doi.org/10.1007/s11663-018-1429-y