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Preparation and characterization of nanoflake composite multi core-shell SrFe12O19/Fe3O4/PEG/PPy

  • 투고 : 2012.04.24
  • 심사 : 2012.06.24
  • 발행 : 2012.06.25

초록

Nanoflake composite multi core-shell $SrFe_{12}O_{19}/Fe_3O_4$/PEG/Polypyrrole was synthesized by in situ polymerization method. In this paper, the fabrication of $SrFe_{12}O_{19}$ nanoflake is as first core by solgel method. Then fabricated a shell layer from magnetic nanoparticles of $Fe_3O_4$, which synthesized by coprecipitation technique, onto the $SrFe_{12}O_{19}$ nanoflake. Polyethylene glycol (PEG) as a polymer layer and as second shell was coated onto the before core-shell. Than core-shell $SrFe_{12}O_{19}/Fe_3O_4$/PEG was used as template for the preparation of $SrFe_{12}O_{19}/Fe_3O_4$/PEG/Polypyrrole composite. Final composite has a conductive property among $4.23{\times}10^{-2}Scm^{-1}$ and magnetic property about $M_s$=2.99 emu/g. Also final composite in soluble at organic solvent such as DMF and DMSO and has a flake structure. Conductivity and magnetic property respectively determine by four-probe instrument and vibrant sample magnetometer (VSM), morphology and article size determined by FE-SEM, TEM and XRD.

키워드

참고문헌

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피인용 문헌

  1. Preparation of nanofiber polythiophene layered on Ba x Sr1−x Fe12O19/Fe3O4/polyacrylic acid core–shell structure and its microwave absorption investigation vol.120, pp.3, 2015, https://doi.org/10.1007/s00339-015-9296-8
  2. Preparation of magnetic and conductive graphite nanoflakes/SrFe12O19/polythiophene nanofiber-nanocomposites and its radar absorbing application vol.17, pp.4, 2016, https://doi.org/10.1007/s12221-016-5669-7