한국재료학회지 (Korean Journal of Materials Research)

  • 제22권3호
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  • Pages.150-154
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  • 2012
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  • 1225-0562(pISSN)
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  • 2287-7258(eISSN)
한국재료학회 (Materials Research Society of Korea)
권호 표지
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Microstructure and Mechanical Properties of Ti-35Nb-7Zr-XCPP Biomaterials Fabricated by Rapid Sintering

  • Woo, Kee-Do (Dental Schoolvision of Advanced Materials Engineering, Research Center of Advanced Materials Development (RCAMD), Chonbuk National University) ;
  • Park, Sang-Hoon (Dental Schoolvision of Advanced Materials Engineering, Research Center of Advanced Materials Development (RCAMD), Chonbuk National University) ;
  • Kim, Ji-Young (Dental Schoolvision of Advanced Materials Engineering, Research Center of Advanced Materials Development (RCAMD), Chonbuk National University) ;
  • Kim, Sang-Mi (Dental Schoolvision of Advanced Materials Engineering, Research Center of Advanced Materials Development (RCAMD), Chonbuk National University) ;
  • Lee, Min-Ho (Department of Dental Biomaterials, School of Dentistry, Chonbuk National University)
  • 투고 : 2012.01.19
  • 심사 : 2012.03.01
  • 발행 : 2012.03.27
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초록

Ti-6Al-4V ELI (Extra Low Interstitial) alloy have been widely used as alternative to bone due to its excellent biocompatibility, although it still has many problems such as high elastic modulus and toxicity. Therefore, biomaterials with low elastic modulus and non toxic characteristics have to be developed. A novel ${\beta}$ Ti-35wt%Nb-7wt%Zr-Calcium pyrophosphate (CPP) composite that is a biocompatible alloy without elemental Al or V was fabricated by spark plasma sintering (SPS) at $1000^{\circ}C$ under 70 MPa using high energy mechanical milled (HEMM) powder. The microstructure and phases of the milled powders and the sintered specimens were studied using SEM, TEM, and XRD. Ti-35wt%Nb-7wt%Zr alloy was transformed from ${\alpha}$ phase to ${\beta}$ phase in the 4h-milled powder by sintering. The sintered specimen using the 4h-milled powder showed that all the elements were distributed very homogeneously and had higher density and hardness. ${\beta}$ Ti alloy-CPP composite, which has nanometer particles, was fabricated by SPS using HEMMed powder. During the sintering process, $CaTiO_3$, TixOy, and CaO were formed because of the reaction between Ti and CPP. The Vickers hardness of the composites increases with the increase of the milling time and the addition of CPP. The biocompatibility of the Ti-Nb-Zr alloys was improved by addition of CPP.

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참고문헌

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피인용 문헌

  1. Characterizations on Mechanical Properties and In Vitro Bioactivity of Biomedical Ti–Nb–Zr–CPP Composites Fabricated by Spark Plasma Sintering vol.29, pp.11, 2016, https://doi.org/10.1007/s40195-016-0486-y