Korean Journal of Environmental Agriculture (한국환경농학회지)

The Korean Society of Environmental Agriculture (한국환경농학회)
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Variation of Fatty Acid Composition and Content in Domestic and Imported Solar-Salt by GC-MS

국산과 수입산 천일염의 지방산 분석

  • Kim, Su-Yeon (Functional Food and Nutrition Division, National Academy of Agricultural Science(NAAS), Rural Development Administration (RDA)) ;
  • Kim, Jung-Bong (Functional Food and Nutrition Division, National Academy of Agricultural Science(NAAS), Rural Development Administration (RDA)) ;
  • Kim, Heon-Woong (Functional Food and Nutrition Division, National Academy of Agricultural Science(NAAS), Rural Development Administration (RDA)) ;
  • Kim, Se-Na (Functional Food and Nutrition Division, National Academy of Agricultural Science(NAAS), Rural Development Administration (RDA)) ;
  • Kim, So-Young (Functional Food and Nutrition Division, National Academy of Agricultural Science(NAAS), Rural Development Administration (RDA)) ;
  • Cho, Young-Sook (Functional Food and Nutrition Division, National Academy of Agricultural Science(NAAS), Rural Development Administration (RDA)) ;
  • Kim, Jae-Hyun (Functional Food and Nutrition Division, National Academy of Agricultural Science(NAAS), Rural Development Administration (RDA)) ;
  • Weon, Hang-Yun (Agricultural Microbiology Team, NAAS, RDA) ;
  • Ham, Kyung-Sik (Dept. of Food Biotechnology Research Center, Mokpo National University)
  • 김수연 (농촌진흥청 국립농업과학원 농식품자원부) ;
  • 김정봉 (농촌진흥청 국립농업과학원 농식품자원부) ;
  • 김헌웅 (농촌진흥청 국립농업과학원 농식품자원부) ;
  • 김세나 (농촌진흥청 국립농업과학원 농식품자원부) ;
  • 김소영 (농촌진흥청 국립농업과학원 농식품자원부) ;
  • 조영숙 (농촌진흥청 국립농업과학원 농식품자원부) ;
  • 김재현 (농촌진흥청 국립농업과학원 농식품자원부) ;
  • 원항연 (농촌진흥청 국립농업과학원 농업생물안전부) ;
  • 함경식 (국립목포대학교 식품공학과 및 천일염생명과학연구소)
  • Received : 2011.11.29
  • Accepted : 2011.12.26
  • Published : 2011.12.31
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Abstract

BACKGROUND: Inorganic component is made up largely of salt, because the criteria are difficult to split into domestic and imported ingredients, organic examined the fatty acid composition is to see a possible use as a marker using gas chromatography-mass spectrometry (GC-MS). The 14 domestic samples and 8 imported samples were collected from China, India and other countries were investigated on item of 37 fatty acids. METHODS AND RESULTS: The major components were six species, myristic acid ($C_{14:0}$), palmitic acid ($C_{16:0}$), palmitoleic acid ($C_{16:1}$), stearic acid ($C_{18:0}$), oleic acid ($C_{18:2,n9}$), linoleic acid ($C_{18:2,n6}$) among detected twenty fatty acids including 9 unknowns. The content of palmitic acid were highest as 25.2 to 50.8% of total fatty acids contents. Domestic has seen the most amount of salt in the Taepyeong salts $250.8{\mu}g$/100g, imports $135.2{\mu}g$/100g salt in Chinese Weifang salts showed the lowest content. CONCLUSION(s): The total fatty acid content has seen the most amount of salt in 352.3 ug/100g Christmas island salts showed the lowest content of $164.0{\mu}g$/100g, as a result it is difficult to distinguish the domestic salts and imported by the composition of fatty acid.

Keywords

References

  1. Gamazo-vazquez, J., Garcia-Falcon, M.S., Simal-Gandara, J., 2003. Control of contamination of olive oil by sunflower seed oil in bottling plants by GC-MS of fatty acid methyl esters, Food control. 14, 463-467. https://doi.org/10.1016/S0956-7135(02)00102-0
  2. Ha, J.O., Park, K.Y., 1998. Composition of mineral contents and external structure of various salts, J. Korean Soc. Food Sci. Nutr. 27, 413-418.
  3. Hwang, S.H., 1988. A study on the heavy metal contents of common salts in Korean, Korean J. Environ. Hith. Soc. 14, 73-86.
  4. Jo, E.J., Shin, D.H., 1998. Study on the chemical compositions of sun-dried, refined and processed salt produced in Chonbuk area, J. Fd. Hyg. Safety. 13, 360-364.
  5. Jung, K.O., Lee, K.Y., Rhee, S.K., Park, K.Y., 2002. Effects of various kinds of salt on the tumor formation, NK cell activity and lipid peroxidation in Sarcoma-180 cell transplanted mice, J. Korean Assoc. Cancer Prevention. 7, 134-142.
  6. Kim, J.B., Kim K.H., Hwang, S.K., Kim, Y.H., Cho, K.J., Hwang, Y.S., Park, R.D., 2001. The Composition of useful medium chain fatty acid in eight plant species, J. Kor. Soc. Agric. Chem. Biotechnol. 44, 20-23.
  7. Kim, J.B., Kim, K.H., Hong, S.B., Park, J.S., Lee, J.Y., Kim, S.S., Bae, S.C., Cho, K.J., Lee, D.J., 2007. Screening of GLA (γ-lnolenic acid) from fungi by gas chromatography and mass spectroscopy, The korean journal of mycology. 35, 96-100. https://doi.org/10.4489/KJM.2007.35.2.096
  8. Korea Food and Drug Administration., 2004. Food Standards Codex. Korean Foods Industry Association, Seoul, Korea.
  9. Lee, K.D., Park, J.W., Choi, C.R., Song, H.W., 2005. A gas chromatography/electron ionization-mass spectrometryselected ion monitoring method for determining the fatty acid pattern in food after formation of fatty acid methyl esters, J. Agric. Food Chem. 53, 8896-8903. https://doi.org/10.1021/jf051468u
  10. Metcalfe, L.D., Schmitz, A.A., Pelka, J.R., 1966. Rapid preparation of fatty acid esters from lipids for gas chromatographic analysis, Anal. Chem. 38, 514-515. https://doi.org/10.1021/ac60235a044
  11. Mochida, M., Kitamori, Y., Kawamura, K., 2002. Fatty acids in the marine atmosphere:Factors governing their concentrations and evaluation of organic films on sea-salt particles, J. Geophys. Res. 107, D17, 4325. https://doi.org/10.1029/2001JD001278
  12. Park, J.W., Kim, S.J., Kim, S.H., Kim, B.H., Kang, S.G., Nam, S.H., Jung S.T., 2000. Determination of mineral and heavy metal contents of various salts, Korean J. Food Sci. Technol. 32, 1442-1445.
  13. Petrovic, M., Kezic, N., Bolanca, V., 2010. Optimization of the GC method for routine analysis of the fatty acid profile in several food samples, Food Chem. 122, 285-291. https://doi.org/10.1016/j.foodchem.2010.02.018
  14. Saraf, A., Park, J.H., Milton, D.K., Larsson, L., 1999. Use of quadrupole GC-MS and ion trap GC-MS-MS for determining 3-hydroxy fatty acids in settled house dust: relation to endotoxin activity, J. Environ. Monit. 1, 163-168. https://doi.org/10.1039/a809019j
  15. Shin, T.S., Park, C.K., Lee, S.H., Han, K.H., 2005. Effect of age on chemical composition in sun-dried, refined, and processed salt produced in Chonbuk area, Korean J. Food Sci. Technol. 37, 312-317.
  16. Slover, H.T., Lanza, E., 1979. Quantitative analysis of food fatty acids by capillary gas chromatography, J. Am. Oil Chem. Soc. 56, 933-943. https://doi.org/10.1007/BF02674138

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