Bulletin of the Korean Chemical Society

Korean Chemical Society (대한화학회)
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A New Stationary Phase Prepared from Ground Silica Monolith Particles by Reversible Addition-Fragmentation Chain Transfer Polymerization

  • Lee, Seung-Mi (Department of Chemistry, Nano Fine Center, and Institute of Basic Research, Inha University) ;
  • Zaidi, Shabi Abbas (Department of Chemistry, Nano Fine Center, and Institute of Basic Research, Inha University) ;
  • Cheong, Won-Jo (Department of Chemistry, Nano Fine Center, and Institute of Basic Research, Inha University)
  • Received : 2010.07.19
  • Accepted : 2010.08.31
  • Published : 2010.10.20
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Abstract

Silica monolith powders were prepared by a new procedure where ground powders of proper size distribution were obtained without sieving. An initiator was attached to this ground monolith and polystyrene was bound by reversible addition-fragmentation chain transfer polymerization to give a new stationary phase. The separation efficiency of this phase was found better than that of the polystyrene bound phase based on conventional silica particles and that of the C18 bound silica monolith powders.

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References

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