DOI QR코드

DOI QR Code

A New Stationary Phase Prepared from Ground Silica Monolith Particles by Reversible Addition-Fragmentation Chain Transfer Polymerization

  • Lee, Seung-Mi (Department of Chemistry, Nano Fine Center, and Institute of Basic Research, Inha University) ;
  • Zaidi, Shabi Abbas (Department of Chemistry, Nano Fine Center, and Institute of Basic Research, Inha University) ;
  • Cheong, Won-Jo (Department of Chemistry, Nano Fine Center, and Institute of Basic Research, Inha University)
  • 투고 : 2010.07.19
  • 심사 : 2010.08.31
  • 발행 : 2010.10.20

초록

Silica monolith powders were prepared by a new procedure where ground powders of proper size distribution were obtained without sieving. An initiator was attached to this ground monolith and polystyrene was bound by reversible addition-fragmentation chain transfer polymerization to give a new stationary phase. The separation efficiency of this phase was found better than that of the polystyrene bound phase based on conventional silica particles and that of the C18 bound silica monolith powders.

키워드

참고문헌

  1. Rahman, M. M.; Czaun, M.; Takafuji, M.; Ihara, H. Chem. Eur. J. 2008, 14, 1312-1321. https://doi.org/10.1002/chem.200701302
  2. Nagase, K.; Kobayashi, J.; Kikuchi, A.; Akiyama, Y.; Annaka, M.; Kanazawa, H.; Okano, T. Langmuir 2008, 24, 10981-10987. https://doi.org/10.1021/la801949w
  3. Idota, N.; Kikuchi, A.; Kobayashi, J.; Akiyama, Y.; Sakai, K.; Okano, T. Langmuir 2006, 22, 425-430. https://doi.org/10.1021/la051968h
  4. Coad, B. R.; Steels, B. M.; Kizhakkedathu, J. N.; Brooks, D. E.; Haynes, C. A. Biotechnol. Bioengineer. 2007, 97, 574-587. https://doi.org/10.1002/bit.21283
  5. Nagase, K.; Kobayashi, J.; Kikuchi, A.; Akiyama, Y.; Kanazawa, H.; Okano, T. Langmuir 2008, 24, 511-517. https://doi.org/10.1021/la701839s
  6. Mallik, A. K.; Rahman, M. M.; Czaun, M.; Takafuji, M.; Ihara, H. J. Chromatogr. A 2008, 1187, 119-127. https://doi.org/10.1016/j.chroma.2008.02.011
  7. Hemstrom, P.; Szumski, M.; Irgum, K. Anal. Chem. 2006, 78, 7098-7103. https://doi.org/10.1021/ac0602874
  8. Miller, M. D.; Baker, G. L.; Bruening, M. L. J. Chromatogr. A 2004, 1044, 323-330. https://doi.org/10.1016/j.chroma.2004.04.071
  9. Yoshikawa, C.; Goto, A.; Tsujii, Y.; Ishizuka, N.; Nakanishi, K.; Fukuda, T. J. Polym. Sci. Part A: Polym. Chem. 2007, 45, 4795-4803. https://doi.org/10.1002/pola.22224
  10. Nagase, K.; Kobayashi, J.; Kikuchi, A.; Akiyama, Y.; Kanazawa, H.; Okano, T. Biomacromolecules 2008, 9, 1340-1347. https://doi.org/10.1021/bm701427m
  11. Derouet, D.; Thuc, C. N. H. J. Appl. Polym. Sci. 2008, 109, 2113-2127. https://doi.org/10.1002/app.28290
  12. Fairhurst, R. E.; Chassaing, C.; Venn, R. F.; Mayes, A. G. Biosensors and Bioelectronics 2004, 20, 1098-1105. https://doi.org/10.1016/j.bios.2004.01.020
  13. Sulitzky, C.; Ruckert, B.; Hall, A. J.; Lanza, F.; Unger, K.; Sellergren, B. Macromolecules 2002, 35, 79-91. https://doi.org/10.1021/ma011303w
  14. Roohi, F.; Titirici, M. M. New J. Chem. 2008, 32, 1409-1414. https://doi.org/10.1039/b800851e
  15. Su, S.; Zhang, M.; Li, B.; Zhang, H.; Dong, X. Talanta 2008, 76, 1141-1146. https://doi.org/10.1016/j.talanta.2008.05.015
  16. Czaun, M.; Rahman, M. M.; Takafuji, M.; Ihara, H. Polymer 2008, 49, 5410-5416. https://doi.org/10.1016/j.polymer.2008.10.017
  17. Unsal, E.; Elmas, B.; Caglayan, B.; Tuncel, M.; Patir, S.; Tuncel, A. Anal. Chem. 2006, 78, 5868-5875. https://doi.org/10.1021/ac060506l
  18. Coessens, V.; Pintauer, T.; Matyjaszewski, K. Prog. Polym. Sci. 2001, 26, 337-377. https://doi.org/10.1016/S0079-6700(01)00003-X
  19. Qiu, K.; Li, P. Chinese J. Polym. Sci. 2004, 22, 99-110.
  20. Favier, A.; Charreyre, M. Macromol. Rapid Comm. 2006, 27, 653-692. https://doi.org/10.1002/marc.200500839
  21. Perrier, S.; Takolpuckdee, P. J. Polym. Sci. Pt. A: Polym. Chem. 2005, 43, 5347-5393. https://doi.org/10.1002/pola.20986
  22. Kim, S. S.; Cheong, W. J. Bull. Korean Chem. Soc. 2009, 30, 722-725. https://doi.org/10.5012/bkcs.2009.30.3.722
  23. Hwang, D. G.; Zaidi, S. A.; Cheong, W. J. Bull. Korean Chem. Soc. 2009, 30, 3127-3130. https://doi.org/10.5012/bkcs.2009.30.12.3127
  24. Hwang, D. G.; Zaidi, S. A.; Cheong, W. J. J. Sep. Sci. 2010, 33, 587-593. https://doi.org/10.1002/jssc.200900578
  25. Ko, J. H.; Baik, Y. S.; Park, S. T.; Cheong, W. J. J. Chromatogr. A 2007, 1144, 269-274. https://doi.org/10.1016/j.chroma.2007.01.086
  26. Han, K. M.; Cheong, W. J. Bull. Korean Chem. Soc. 2008, 29, 2281-2283. https://doi.org/10.5012/bkcs.2008.29.11.2281

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