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Synthesis of Core/shell Structured Ag/C Nano Particles and Properties on Annealing Conditions

전기선폭발법을 이용한 core/shell 구조 Ag/C 나노 입자의 제조 및 열처리조건에 따른 특성

  • Jun, S.H. (Nuclear Nano Materials Development LAB., Korea Atomic Energy Research Institute(KAERI)) ;
  • Uhm, Y.R. (Nuclear Nano Materials Development LAB., Korea Atomic Energy Research Institute(KAERI)) ;
  • Rhee, C.K. (Nuclear Nano Materials Development LAB., Korea Atomic Energy Research Institute(KAERI))
  • 전수형 (한국원자력연구원, 원자력재료연구부) ;
  • 엄영랑 (한국원자력연구원, 원자력재료연구부) ;
  • 이창규 (한국원자력연구원, 원자력재료연구부)
  • Received : 2010.05.28
  • Accepted : 2010.07.12
  • Published : 2010.08.28

Abstract

Multi shell graphite coated Ag nano particles with core/shell structure were successfully synthesized by pulsed wire evaporation (PWE) method. Ar and $CH_4$ (10 vol.%) gases were mixed in chamber, which played a role of carrier gas and reaction gas, respectively. Graphite layers on the surface of silver nano particles were coated indiscretely. However, the graphite layers are detached, when the particles are heated up to $250^{\circ}C$ in the air atmosphere. In contrast, the graphite coated layer was stable under Ar and $N_2$ atmosphere, though the core/shell structured particles were heated up to $800^{\circ}C$. The presence of graphite coated layer prevent agglomeration of nanoparticles during heat treatment. The dispersion stability of the carbon coated Ag nanoparticles was higher than those of pure Ag nanoparticles.

Keywords

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