Carbon letters

  • 제10권1호
  • /
  • Pages.38-42
  • /
  • 2009
  • /
  • 1976-4251(pISSN)
  • /
  • 2233-4998(eISSN)
한국탄소학회 (Korean Carbon Society)
권호 표지
DOI QR코드

DOI QR Code

Structural Study of the Oxidized High Modulus Carbon Fiber using Laser Raman Spectroscopy

  • Roh, Jae-Seung (School of Advanced Materials and System Engineering, Kumoh National Institute of Technology 1) ;
  • Kim, Suk-Hwan (School of Advanced Materials and System Engineering, Kumoh National Institute of Technology 1)
  • 투고 : 2008.02.04
  • 심사 : 2009.03.04
  • 발행 : 2009.03.30
PDF 다운로드
⟨ 이전 논문 다음 논문 ⟩

초록

This study aims to find a correlation between XRD and Raman result of the oxidized high modulus carbon fibers as a function of its oxidation degrees, and compare with the isotropic carbon fiber reported early. La of the high modulus carbon fiber prepared by oxidation in carbon dioxide gas have been observed using laser Raman spectroscopy. The basic structural parameters of the fibers were evaluated by XRD as well. The La of the original high modulus carbon fibers were measured to be 144 ${\AA}$ from Raman analysis and 135 ${\AA}$ from XRD analysis. La of the 92% oxidized fiber were 168 ${\AA}$ by using Raman and 182 ${\AA}$ by using XRD. There was some correlation between the La value obtained from Raman and XRD. However the La value changes of the high modulus carbon fiber through whole oxidation process showed opposite tendency compare with the isotropic carbon fiber because of the fiber structure basically.

키워드

참고문헌

  1. Endo, M.; Kim, C.; Kasai, T.; Mathews, M. J.; Brown, S. D. M.; Dresselhaus, M. S.; Tamaki, T.; Nishimura, Y. Carbon 1998, 36, 1633. https://doi.org/10.1016/S0008-6223(98)00157-2
  2. Hong, S. H.; Korai, Y.; Mochida, I. Carbon 2000, 38, 805. https://doi.org/10.1016/S0008-6223(99)00175-X
  3. Montes-Moran, M. A.; Young, R. J. Carbon 2002, 40, 845. https://doi.org/10.1016/S0008-6223(01)00212-3
  4. Donnet, J. B.; Bansal, R. C. "Carbon Fibers" 2nd ed., Marcel Decker, New York, 1990, 8.
  5. Dami, T. L.; Manocha, L. M.; Bahl, O. P. Carbon 1999, 29, 51. https://doi.org/10.1016/0008-6223(91)90094-Y
  6. Ismail, M. K. Carbon 1991, 29, 777. https://doi.org/10.1016/0008-6223(91)90017-D
  7. Mahajan, O. P.; Yarzab R.; Walker Jr. P. L. Feul 1978, 57, 643.
  8. Sanchez, A. R.; Elguezabal, A. A.; Torre Saenz, L. L. Carbon 2001, 39, 1367. https://doi.org/10.1016/S0008-6223(00)00253-0
  9. Kasaoka, S.; Sakata, Y.; Kayano, S.; Masuoka, Y. Int. Chem. Eng. 1983, 23, 477.
  10. Hu, Y. Q.; Nikzat, H.; Nawata, M.; Kobayashi, N.; Hasatani, M. Feul 2001, 80, 2111.
  11. Rafsanjani, H. H.; Jashidi, E.; Rostam-Abadi, M. Carbon 2002, 40, 1167. https://doi.org/10.1016/S0008-6223(01)00265-2
  12. Blanco, S. Lu, C.; Rand, B. Carbon 2002, 40, 2002.
  13. Sharma, A.; Kyotani, T.; Tomita, A. Carbon 2000, 38, 1977. https://doi.org/10.1016/S0008-6223(00)00045-2
  14. Kovalevski, V. V.; Buseck, P. R.; Cowley, J. M. Carbon 2001, 39, 243. https://doi.org/10.1016/S0008-6223(00)00120-2
  15. Senneca, O.; Salatino, P.; Masi, S. Fuel 1998, 77, 1483. https://doi.org/10.1016/S0016-2361(98)00056-8
  16. Busyin, R. M.; Rouzaud, J. N.; Ross, J. V. Carbon 1995, 33, 679. https://doi.org/10.1016/0008-6223(94)00155-S
  17. Roh, J. S. Carbon Science 2004, 5, 27
  18. Roh, J. S. Carbon Science 2008, 9, 127
  19. Montes-Moran, M. A.; Young. R. J. Carbon 2002, 40, 845. https://doi.org/10.1016/S0008-6223(01)00212-3
  20. Kuo, C. T.; Wu, J. Y.; Lu, T. R. Materials Chemistry and Physics 2001, 72, 251. https://doi.org/10.1016/S0254-0584(01)00447-3
  21. Lespade, P.; Al-Jishi, R.; Dresselhaus, M. S. Carbon 1982, 20, 427. https://doi.org/10.1016/0008-6223(82)90043-4
  22. Escribano, R.; Sloan, J. J.; Siddique, N.; Sze, N.; Dudev, T. Vibrational Spectroscopy 2001, 26, 179. https://doi.org/10.1016/S0924-2031(01)00106-0
  23. Montes-Moran, Miguel A.; Young, Robert J. Carbon 2002, 40, 845 https://doi.org/10.1016/S0008-6223(01)00212-3
  24. Kamegawa, K.; Nishikubo, K.; Yoshida, H. Carbon 1998, 36, 433. https://doi.org/10.1016/S0008-6223(97)00227-3
  25. Sharma, A.; Kyotani, T.; Tomita, A. Fuel 1999, 78, 1203. https://doi.org/10.1016/S0016-2361(99)00046-0
  26. Yoshizawa, N..; Maruyama, K.; Yamada, Y.; Zielinska-Blajet, M. Fuel 2000, 79, 1461. https://doi.org/10.1016/S0016-2361(00)00011-9
  27. Gondy, D.; Ehrburger, P. Carbon 1997, 35, 1745. https://doi.org/10.1016/S0008-6223(97)00133-4

피인용 문헌

  1. Analysis of the Microstructure and Oxidation Behavior of Some Commercial Carbon Fibers vol.55, pp.5, 2011, https://doi.org/10.5012/jkcs.2011.55.5.819