Journal of the Korean Society of Clothing and Textiles (한국의류학회지)

The Korean Society of Clothing and Textiles (한국의류학회)
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Dyeing Properties and Color of Silk Fabrics Dyed with Safflower Yellow Dye

홍화 황색소 견섬유에 대한 염색성과 색상

  • Shin, Youn-Sook (Dept. of Clothing & Textiles/Human Ecology Research Institute, Chonnam National University) ;
  • Son, Kyung-Hee (Dept. of Clothing & Textiles/Human Ecology Research Institute, Chonnam National University) ;
  • Yoo, Dong-Il (Dept. of Textile Engineering, Chonnam National University)
  • 신윤숙 (전남대학교 의류학과/생활과학연구소) ;
  • 손경희 (전남대학교 의류학과/생활과학연구소) ;
  • 류동일 (전남대학교 섬유공학과)
  • Published : 2008.06.30
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Abstract

The objective of this study is to investigate the dyeing properties of safflower yellow dye on silk for the standardization of dyeing process and color reproducibility. Yellow colorants were water-extracted from safflower petals, concentrated, and freeze-dried to obtain colorants powder. The effects of dye concentration, dyeing temperature, and pH of dye bath were studied in terms of dye uptake and shade. Fastness to dry cleaning and light was evaluated. Dye uptake increased with raising temperature and brighter and more vivid yellow shade was obtained when dyed at $30^{\circ}C$. As colorants concentration increased, dye uptake increased progressively and the shade got darker and deeper. Maximum color strength was obtained at pH 3.5. It was speculated that the adsorption of colorants seemed to occur mainly by hydrogen bonding and physical force at pH 5.5 and by ionic bonding as well as hydrogen bonding below isoelectric point(pH 3.8-4.0). The results of reproducibility test showed acceptable color difference in the range of $1.11{\sim}2.01$. Washing fastness was fairly good as 4/5 rating, while light fastness was 2/3 rating.

본 연구는 염색공정의 표준화와 재현성을 확립하기 위해 흥화 황색소의 견섬유에 대한 염색성을 조사하는데 목적 이 있다. 홍화 황색소는 물로 추출한 후 농축, 동결건조하여 분말상태로 만들어 사용하였다. 염색온도 및 시간, 염료농도, 염액의 pH 등에 따른 염착성과 색상 변화에 대해 조사하였으며, 세탁 및 광견뢰도를 평가하였다. 염색온도가 증가함에 따라 염착량은 증가하였으며 $30^{\circ}C$에서 염색할 때 가장 선명한 노랑색을 얻을 수 있었다. 염료농도가 증가함에 따라 염착량이 계속 증가하여 점점 진하고 어두운 노랑색이 되었다. pH 3.5에서 최대염착량을 보였으며, 최적조건에서 색차는 1.11-2.01로서 재현성은 양호하였다. 색소와 견섬유간의 결합은 pH 5.5 부근에서는 주로 수소결합에 의해, 등전점(pH 3.8-4.0) 이하에서는 수소결합과 함께 이온결합이 관여하는 것으로 판단되었다. 세탁(드라이크리닝)견뢰도는 4/5둥급으로 좋은 편이었으나 일광견뢰도는 2/3등급이었다.

Keywords

References

  1. An, K. C. & Kim, J. H. (2001). A study of the dyeability and physical properties of mordanted and finished fabrics dyed with natural dye of safflower. J. of Korean Society of Dyers and Finishers, 13(1), 23-31
  2. Bechtold, T., Mahmud-Ali, A., & Mussak, R. (2007). Natural dyes for textile dyeing: A comparison of methods to assess the quality of Canadian golden rod plant material. Dyes and Pigments, 75(2), 287-293 https://doi.org/10.1016/j.dyepig.2006.06.004
  3. Billmeyer, Jr. F. W. & Saltzman, M. (1981). Principles of color technology (2nd ed.). New York: Wiley Pub. Co.
  4. Cho, K. R. (1997). Study on the natural dyes. J. of Korean Society of Dyers and Finishers, 9(5), 10-18
  5. Cristea, D. & Vilarem, G. (2006). Improving light fastness of natural dyes on cotton yarn. Dyes and Pigments, 70(3), 238-245 https://doi.org/10.1016/j.dyepig.2005.03.006
  6. Jung, S. & Jang, J. (2004). Light fastness of silk fabric dyed with safflower and amur cork tree extract for combining dyeing. J. of Korean Society of Dyers and Finishers, 16(5), 8-18
  7. Kanehira, T. & Saito, K. (2001). Stability of carthamin and safflower yellow B on silk powders under continous irradiation of fluorescent or UV-C light. Lebensmmittel-Wissenschaft und-Technologie, 34, 55-56 https://doi.org/10.1006/fstl.2000.0709
  8. Kim, G. J. & Lee, J. M. (1996). Chemistry of dyeing. Seoul: Hyungsul Pub. Co.
  9. Nam, S. W., Chung, I. M., & Kim, I. H. (1995). Dyeing cotton by natural dyes (I). J. of Korean Society of Dyers and Finishers, 7(2), 47-54
  10. Saito, K. (1990). Possible locality of affinity site(s) on cellulose for preservation of stable red colour of carthamin. Food Chemistry, 36, 243-251 https://doi.org/10.1016/0308-8146(90)90063-A
  11. Saito, S., Kusakari, T., Suda, T., Kasai, T., Kumazawa, T., Onodera, J., & Obara, H. (2005). Efficient synthesis of analogs of safflower yellow B, carthamin, and its precursor: Two yellow and one red dimeric pigments in safflower petals. Tetrahedron, 61, 9630-9636 https://doi.org/10.1016/j.tet.2005.07.080
  12. Shin, Y., Cho, A., & Yoo, D. I. (2007). Improving dyeability of safflower yellow colorants on cellulose fibers. J. Korean Society of Clothing and Textiles, 31(12) 1754-1760 https://doi.org/10.5850/JKSCT.2007.31.12.1754
  13. Shin, Y. & Choi, S. Y. (2007). Imroving UV-cut ability of natural dyed fabrics. J. Korean Home Economics Association, 45(10), 73-81
  14. Trotman, E. R. (1975). Dyeing and chemical technology of textile fibers (5th ed.). London: Charles Griffin & Co. Ltd.
  15. Yoon, J. M., Cho, M. H., Park, J. E., Kim, Y. H., Hahn, T. R., & Paik, Y. S. (2003). Thermal stability of the pigments hydroxysafflor yellow A, safflor yellow B, and precarthamin from safflower. J. of Food Science, 68(3), 839-845 https://doi.org/10.1111/j.1365-2621.2003.tb08252.x

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