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Characteristics of TiO2 Nanotube Gas Sensor Preparedby Hydrothermal Treatment

수열처리에 의한 TiO2 나노 튜브 센서의 가스 검지 특성

  • Seo, Min-Hyun (Department of Sensor and Display Engineering, Kyungpook National University) ;
  • Oh, Sang-Jin (Department of Materials Science & Metallurgy, Kyungpook National University) ;
  • Kida, Tetsuya (Department of Energy and Material Sciences, Kyushu University) ;
  • Shimanoe, Kengo (Department of Energy and Material Sciences, Kyushu University) ;
  • Huh, Jeung-Soo (Department of Materials Science & Metallurgy, Kyungpook National University)
  • Published : 2007.08.27

Abstract

Preparation and morphology control of $TiO_2$ nano powders for gas sensor applications are investigated. $TiO_2$ nanopowders with rutile and anatase structures were prepared by controlling the pH value of a precursor solution without any heat treatment. The mean particle size of $TiO_2$ powders were below 10nm. The prepared $TiO_2$ nano powders were hydrothermal treated by NaOH solution. The sample was washed in HCl solution. As a result and $TiO_2$ nanotubes were formed. The lengths of $TiO_2$ nanotube were $1{\mu}m$ and the diameters were 10nm. Crystal structure and microstructure of $TiO_2$ nanotube were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscope (TEM). As-prepared $TiO_2$ nanotube powders have several advantages of nano particle size and high surface area and could be a prominent candidate for nano-sensors. The sensitivity of $TiO_2$ nanotube sensor was measured for toluene and NO in this study.

Keywords

References

  1. N. Yamazoe, Sensors and Actuators B, 5, 7 (1991) https://doi.org/10.1016/0925-4005(91)80213-4
  2. G Martinelli, M. C. Carotta, Sensors and Actuators B, 7, 717 (1992) https://doi.org/10.1016/0925-4005(92)80391-A
  3. J. D. Choi, G M. Choi, Sensors and Actuators B, 69, 120 (2000) https://doi.org/10.1016/S0925-4005(00)00519-0
  4. D. S. Lee, S. D. Han, J. S. Huh, and D. D. Lee, Sensors and Actuators B, 60, 57 (1999) https://doi.org/10.1016/S0925-4005(99)00244-0
  5. A. Gurlo, M. Ivanovskaya, N. Barsan, M. SchweizerBerberich, U. Weimar, W. Gopel, and A. Dieguez, Sensors and Actuators B, 44, 327 (1997) https://doi.org/10.1016/S0925-4005(97)00199-8
  6. M. R. Prairie, L. P. Evans, B. M. Stange and S. L. Marinez, Envi. Sci. Tech., 27, 1776, (1993) https://doi.org/10.1021/es00046a003
  7. H. Tang, K. Prasad, R. Sanjines, F. Levy, Sensors and Actuators B, 26, 71 (1995) https://doi.org/10.1016/0925-4005(94)01559-Z
  8. A. Curulli, F. Valentini, G Padeletti, M. Viticoli, D. Caschera and GPalleschi, Sensors and Actuators B 111 441 (2005) https://doi.org/10.1016/j.snb.2005.03.044
  9. M. Z. Atashbar, S. Singamaneni, Sensors and Actuators B, 111, 13 (2005) https://doi.org/10.1016/j.snb.2005.07.034
  10. C. C. Tasi, H. Teng. J. Am. Chern. Soc. 18, 367 (2006)