EFFECT OF HARDNESS CHANGES AND MICROSTRUCTURAL DEGRADATION ON CREEP BEHAVIOR OF A Mod.9Cr-1Mo STEEL

  • PARK K. S. (Department of Mechnical Engineering and Materials Science, Yokohama National University) ;
  • CHUNG H. S. (School of Mechanical and Aerospace Engineering, Gyeongsang National University) ;
  • LEE K. J. (Division of Information Commmunication, Yangsan College) ;
  • JUNG Y. G. (School of Mechnical Engineering, Kumoh National Institute of Technology) ;
  • KANG C. Y. (Division of Materials Science and Engineering, Bukyung National University) ;
  • ENDO T. (Department of Mechnical Engineering and Materials Science, Yokohama National University)
  • Published : 2005.02.01

Abstract

Interrupted creep tests for investigating the structural degradation during creep were conducted for a Mod.9Cr-1Mo steel in the range of stress from 71 to 167 MPa and temperature from 873 to 923 K. The change of hardness and tempered martensitic lath width was measured in grip and gauge parts of interrupted creep specimens. The lath structure was thermally stable in static conditions. However, it was not stable during creep, and the structural change was enhanced by creep strain. The relation between the change in lath width and creep strain was described quantitatively. The change in Vickers hardness was expressed by a single valued function of creep LCR(life consumption ratio). Based on the empirical relation between strain and lath width, a model was proposed to describe the relation between change in hardness and creep LCR. The comparison of the model with the empirical relation suggests that about 65% of hardness loss is due to the decrease of dislocation density accompanied by the movement of lath boundaries. The role of precipitates on subboundaries was discussed in connection with the abnormal subgrain growth appearing in low stress regime.

Keywords

References

  1. ASME Boiler and Pressure Vessel Code, Case 1934. Seamless Modified 9Cr-1Mo Section I
  2. ASTM A213-83
  3. Bursik, O., J., Kucharova, K and Sklenicka, V. (1998). Microstructural developent during high temperature creep of 9%Cr steel. Mater. Sci. Eng., A245, 39
  4. Cerri, E., Evangelista, E., Spigarelli, S. and Bianchi, P. (1998). Evolution of microstructure in a modified 9Cr1Mo steel during short term creep. Mater. Sci. Eng., A245,285
  5. Endo, T. and Shi, J. (1994). Strength of materials. Ed. by H. Oikawa, K. Maruyama, S. Takeuchi and M. Yamaguchi, JIM, 665
  6. Excell, S. F. and Warrington, D. H. (1972). Sub-grain boundary migration in aluminium. Phil. Mag. 26, 1121
  7. Fukutomi, H. and Horiuchi, R. (1979). Stress induced migration of <112> symmetric tilt boundaries. J. Japan Inst. Metals, 43, 1025 https://doi.org/10.2320/jinstmet1952.43.11_1025
  8. Fukutomi, H. and Horiuchi, R. (1981). Stress induced migration of <112> and <100> symmetric tilt boundaries. J. Japan Inst. Metals, 45, 574 https://doi.org/10.2320/jinstmet1952.45.6_574
  9. Hillert, M. (1965). On the theory of normal and abnormal grain growth. Acta Met., 13, 227 https://doi.org/10.1016/0001-6160(65)90200-2
  10. Kouon Henkei Tokusei Deta Shyu. (1992). ISH, Tokyo, 117
  11. Kushima, H., Kimura, K. and Abe, F. (1999). Degradation of Mod.9Cr-1Mo Steel during long-term creep deformation. Tetsu-to Hagane, 85, 841
  12. Masuyama, F. and Nishimura, N. (1994). Srength of Materials. Ed. by H. Oikawa, K. Maruyama, S. Takeuchi and M. Yamaguchi. JIM, 657
  13. Nishizawa, T., Ohmura, I. and Ishida, K. (1977). Examination of the Zener relationship between grain size and particle dispersion. Mater. Trans. JIM, 38, 950
  14. Park, K. S., Masuyama, F. amd Endo, T. (2001). Creep modeling for life evaluation of heat-resistant steel with a martensitic structure. ISIJ International, 41, S 86-90 https://doi.org/10.2355/isijinternational.41.86
  15. Park, K. S., Masuyama, F. and Endo, T. (1998). Shortterm creep behavior analysis of a Mod.9Cr-IMo steel. Tetsu-to Hagane, 84, 526-533 https://doi.org/10.2355/tetsutohagane1955.84.7_526
  16. Park, K. S., Masuyama, F. and Endo, T. (1999). Constitutive equation describing creep curve of a statically aged Mod.9Cr-IMo steel. J. Japan Inst. Metals, 63, 597 https://doi.org/10.2320/jinstmet1952.63.5_597
  17. Park, K. S., Masuyama, F. and Endo, T. (1999). Improvement of $\Omega$ method to estimate creep behavior of a Mod.9Cr-lMo steel. Tetsu-to Hagane, 85,492
  18. Prager, M. (1994). Strength of materials. Ed. by H. Oikawa, K. Maruyama, S. Takeuchi and M. Yamaguchi, JIM,571
  19. Read, W. T., Jr. (1953). Dislocations in Crystls. McGrawHill. New York. 155
  20. Sandstrom, R. and Konyr, A. (1972). Modelfor Tertiarycreep in Mo-and CrMo-Steels. ICM3. Cambridge. UK. 2.275
  21. Sawada, K., Maruyama, K., Hasegawa, Y. and Muraki, T. (1999). Creep and Fracture of Engineering Materials and Structures. Ed. by T. Sakuma, K. Yagi, Trans Tech Publications. Swiss. 109-114
  22. Sawada, K., Maruyama, K., Komine, R. and Nagae, Y. (1997). Microstructural changes during creep and life assessment of Mod.9Cr-1Mo steel. Tetsu-to-Hagane, 83,466-471 https://doi.org/10.2355/tetsutohagane1955.83.7_466
  23. Sawada, K., Takeda, M., Maruyama, K., Komine, R. and Nagae, Y. (1998). Residual creep life assessment by change of martensitic lath structure in modified 9Cr-1Mo steels. Tetsu-to-Hagane, 84, 580 https://doi.org/10.2355/tetsutohagane1955.84.8_580
  24. Suzuki, K., Kumai, S., Kushima, H., Kimura, K. and Abe, F. (2000). Heterogeneous recovery and precipitation of Z phase during long term creep deformation of modified 9Cr-1Mo steel. Tetsu-to Hagane, 86, 550