Synthesis of Ag Nanopowder for Low Temperature Heat Treatment Prepared by Liquid Phase Reduction Method

액상환원법에 의한 저온 열처리용 Ag 나노분말의 합성

  • Lee, Jong-Kook (Department of Advanced Materials Engineering, Chosun University) ;
  • Choi, Nam-Kyu (Department of Advanced Materials Engineering, Chosun University) ;
  • Song, Dae-Sung (Department of Advanced Materials Engineering, Chosun University) ;
  • Yang, Gon-Seung (Department of Advanced Materials Engineering, Chosun University) ;
  • Seo, Dong-Seok (School of Materials Science and Engineering, Seoul National University)
  • 이종국 (조선대학교 신소재공학과) ;
  • 최남규 (조선대학교 신소재공학과) ;
  • 송대성 (조선대학교 신소재공학과) ;
  • 양권승 (조선대학교 신소재공학과) ;
  • 서동석 (서울대학교 재료공학부)
  • Received : 2005.06.09
  • Accepted : 2005.07.26
  • Published : 2005.07.30

Abstract

Silver nanoparticles were synthesized by liquid phase reduction method from aqueous silver nitrate solution and borohybride as a reduction agent. The morphology, particle size and shape were influenced by the reaction conditions such as the concentration of $AgNO_3$, a reduction agent and addition of surfactant. The particle size decreased with decreasing the concentration of silver nitrate and using a borohydride. The obtained Ag particles showed the spherical shape with the range of 10-20 nm.

Keywords

Acknowledgement

Supported by : 조선대학교

References

  1. S. D. Park, H. G. Kang, Y. H. Park and J. D. Mun, J. Microelectrics and packaging Soc., 40 (1999) 25
  2. M. Skurski, M. Smith, R. Draudt, D. amey; S. Horowiz and M. Champ, Int. J. Microcircuits and Electronic Packaging, 21 (1998) 355
  3. K. Nagashima, T. Himeda and A. Kanto, J. Mater. Sci., 26 (1991) 2477 https://doi.org/10.1007/BF01130198
  4. M. Furusawa, T, Hashimoto, M. Ishida, T. Shimoda, H. Hasei, T. Hirai, H. Kiguchi, H. Aruga, M. Oda, N. Saito, H. Iwashige, N. Abe, S. Fukuta and K. Betsui, SID'02 Digest, (2002) 752
  5. K. S. Chou and C. Y. Ren, Mater. Chem. and Phys., 64 (2000) 241
  6. T. Fujimoto, 'New Introduction to Surface Active Agents', Sanyo Chemical Industries Ltd. 1984
  7. M. S. Kim, Specialty Chemical Symposium, (1991) 79
  8. Y. Xuan and Q. Li, Int. J. Heat Fluid Fl. 21 (2000) 58 https://doi.org/10.1016/S0142-727X(99)00067-3
  9. S. Kundu, S. K. Chosh, M. Mandai and T. Pal, Bull. Mater. Sci., 6 (2002) 577
  10. N. Shirtcliffe, U. Nickel and S. Schneider, J. Collid Interface Sci., 211 (1999) 122 https://doi.org/10.1006/jcis.1998.5980
  11. A. M. Ahern and R. I. Garrell, Anal. Chem., 59 (1987) 2816 https://doi.org/10.1021/ac00150a021
  12. C. C. Vukovic and J. M. Nedeljkovic, Langmuir, 9 (1993) 980 https://doi.org/10.1021/la00028a017