Journal of Magnetics

The Korean Magnetics Society (한국자기학회)
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Analysis of Mobile Lead in Soil Using Carboxylated Magnetic Particle

  • Published : 2005.09.01
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Abstract

The analytic possibility of mobile lead contained in soil has been studied using carboxylated magnetic beads. Extraction of heavy metal was performed to contaminated soil that has been collected and supplied for tests. As experiment materials, soil sample, distilled water and magnetic beads were only used. It means that the lead was extracted under neutral condition. In this condition, only the mobile fraction of lead could be extracted by magnetic beads. The mobile lead in the soil was quickly combined with magnetic beads in the mixture process. Then, the magnetic beads were dissolved into acids after collection by external magnetic force, and the lead combined with the beads was eluted and analyzed by Graphite Furnace Atomic Absorption Spectroscopy (GFAAS). In the results of extraction experiments for 3 sandy soils, the efficiency using beads was similar to or higher than that of EDTA (Ethylendiamintetraacetic acid), which is normally used for analyzing mobile heavy metal concentration in soil. With this, it was shown that this method is a more accurate and simple method to analyze mobile lead when analyzing mobile heavy metal concentration in sandy soil, rather than conventional method using EDTA.

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References

  1. A. Saglam, S. Bektas, S. Patir, O. Gene, and A. Denizli, Reactive and Functional Polymers 47, 185 (2001) https://doi.org/10.1016/S1381-5148(00)00054-7
  2. I.-J. Chung, Ph.D. Thesis, Sogang University, Korea (2001) pp. 12-17
  3. F. Scheffer and P. Schachtschabel, Lehrbuch der Bodenkunde, Ferdinand Enke Verlag, (1998) pp. 87-134, 309-371, 471-476
  4. H. Zeien and G. W. Brummer, Mitteilgn. Dtsch. Bodenkundl. Gesellsch. 59(1), 505 (1989)
  5. P. Welp, M. Hamer, G. M. Briimmer, and R. LichtfuB, Mitteilgn, Dtsch. Bodenkundl. Gesellsch. 76, 487 (1995)
  6. I. Maiz, V. Esnaola, and E. Millan, The Sci. Total Environ. 206, 107 (1997)
  7. J. Lewandowski, S. Leitschuh, and V. KoB, Schadstoffe im Boden, Springer Verlag, (1997) pp. 130-135, 258
  8. V. Homburg, Ph.D Thesis, 1991, Bonn University, Germany (1991) pp. 14-16
  9. H. So, H. C. Shin, and Y.-S. Yoo, J. Korean Magnetic Soc., 15(2), 76 (2005)
  10. Oesterreichisches Normungs-institut Wien, Bestimmung von EDTA-extrahierbarem Fe, Mn, Cu, und Zn, OENORM L 1089, (1989) pp. 5
  11. H. Zeien and G. W. Brummer, Mitteilgn. Dtsch. Boden-kundl. Gesellsch. 66(1), 439 (1991)